GB1054576A - - Google Patents
Info
- Publication number
- GB1054576A GB1054576A GB1054576DA GB1054576A GB 1054576 A GB1054576 A GB 1054576A GB 1054576D A GB1054576D A GB 1054576DA GB 1054576 A GB1054576 A GB 1054576A
- Authority
- GB
- United Kingdom
- Prior art keywords
- adsorbent
- alumina
- micron
- activated
- hydroxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
- B01J20/08—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04 comprising aluminium oxide or hydroxide; comprising bauxite
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
- B01J20/282—Porous sorbents
- B01J20/284—Porous sorbents based on alumina
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
- B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
- B01J20/3204—Inorganic carriers, supports or substrates
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
- B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
- B01J20/3234—Inorganic material layers
- B01J20/3236—Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/90—Plate chromatography, e.g. thin layer or paper chromatography
- G01N30/92—Construction of the plate
- G01N30/93—Application of the sorbent layer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/49—Materials comprising an indicator, e.g. colour indicator, pH-indicator
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
- B01J2220/54—Sorbents specially adapted for analytical or investigative chromatography
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
1,054,576. Alumina adsorbent. E. MERCK, A. G. Oct. 29. 1964 [Dec. 14. 1963], No. 44225/64. Heading C1A. [Also in Division B1] A chromatographic adsorbent comprises 1- 25% hydrated aluminium oxide or hydroxide of particle size below 1 micron, preferably 0À001-0À1 micron, and a balance of adsorbent alumina of particle size at least 1 micron. The fine material may be the amorphous hydroxide gel obtained by precipitation from Al salt solutions with NH 3 or NaOH, or a transition alumina obtained by heating the gel at 50- 1250 C. The adsorbent alumina may have a surface area of 50-400 m<SP>2</SP>/g. It may be basic (pH 8-11 in suspension), neutral (pH 6-8) or acidic (pH 3-6), and the pH of the fine aluminium oxide or hydroxide may be adjusted to the same value, e.g. by acid washing. Fluorescent substances, e.g. Mn-activated Zn silicate, Mg tungstate, or Cd halogen phosphate, Sn-activated Ca phosphate, Mn- or Mn/Pbactivated Ca silicate, Sb- or Sb/Mn-activated Ca halogen phosphate, Na 3-hydroxy-pyrene- 5, 8, 10-trisulphonate, Na3,5-dihydroxypyrene- 8, 10-disulphonate, or morin, may be added. The adsorbent is used in thin layer chromatography and for preparative separations using layers 0À5-5 mm. thick.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEM59256A DE1229756B (en) | 1963-12-14 | 1963-12-14 | Adsorbent suitable for plate chromatography, especially for preparative thin-layer chromatography |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1054576A true GB1054576A (en) |
Family
ID=7309477
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1054576D Active GB1054576A (en) | 1963-12-14 |
Country Status (7)
Country | Link |
---|---|
BE (1) | BE656988A (en) |
CH (1) | CH483856A (en) |
DE (1) | DE1229756B (en) |
DK (1) | DK112413B (en) |
GB (1) | GB1054576A (en) |
NL (1) | NL6414438A (en) |
SE (1) | SE306627B (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2423782A1 (en) * | 1978-04-17 | 1979-11-16 | Merck Patent Gmbh | FLUORESCENCE INDICATORS FOR USE IN CHROMATOGRAPHY AND SORPTION AGENTS CONTAINING THESE INDICATORS |
-
0
- GB GB1054576D patent/GB1054576A/en active Active
-
1963
- 1963-12-14 DE DEM59256A patent/DE1229756B/en active Pending
-
1964
- 1964-09-02 CH CH1143164A patent/CH483856A/en unknown
- 1964-12-09 DK DK603364AA patent/DK112413B/en unknown
- 1964-12-11 BE BE656988D patent/BE656988A/xx unknown
- 1964-12-11 NL NL6414438A patent/NL6414438A/xx unknown
- 1964-12-14 SE SE15098/64A patent/SE306627B/xx unknown
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2423782A1 (en) * | 1978-04-17 | 1979-11-16 | Merck Patent Gmbh | FLUORESCENCE INDICATORS FOR USE IN CHROMATOGRAPHY AND SORPTION AGENTS CONTAINING THESE INDICATORS |
Also Published As
Publication number | Publication date |
---|---|
DK112413B (en) | 1968-12-09 |
CH483856A (en) | 1970-01-15 |
NL6414438A (en) | 1965-06-15 |
BE656988A (en) | 1965-06-11 |
SE306627B (en) | 1968-12-02 |
DE1229756B (en) | 1966-12-01 |
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