GB1054576A - - Google Patents

Info

Publication number
GB1054576A
GB1054576A GB1054576DA GB1054576A GB 1054576 A GB1054576 A GB 1054576A GB 1054576D A GB1054576D A GB 1054576DA GB 1054576 A GB1054576 A GB 1054576A
Authority
GB
United Kingdom
Prior art keywords
adsorbent
alumina
micron
activated
hydroxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Publication of GB1054576A publication Critical patent/GB1054576A/en
Active legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • B01J20/08Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04 comprising aluminium oxide or hydroxide; comprising bauxite
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/282Porous sorbents
    • B01J20/284Porous sorbents based on alumina
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/32Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204Inorganic carriers, supports or substrates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/32Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234Inorganic material layers
    • B01J20/3236Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/90Plate chromatography, e.g. thin layer or paper chromatography
    • G01N30/92Construction of the plate
    • G01N30/93Application of the sorbent layer
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00Aspects relating to sorbent materials
    • B01J2220/40Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/49Materials comprising an indicator, e.g. colour indicator, pH-indicator
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00Aspects relating to sorbent materials
    • B01J2220/50Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/54Sorbents specially adapted for analytical or investigative chromatography

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

1,054,576. Alumina adsorbent. E. MERCK, A. G. Oct. 29. 1964 [Dec. 14. 1963], No. 44225/64. Heading C1A. [Also in Division B1] A chromatographic adsorbent comprises 1- 25% hydrated aluminium oxide or hydroxide of particle size below 1 micron, preferably 0À001-0À1 micron, and a balance of adsorbent alumina of particle size at least 1 micron. The fine material may be the amorphous hydroxide gel obtained by precipitation from Al salt solutions with NH 3 or NaOH, or a transition alumina obtained by heating the gel at 50- 1250‹ C. The adsorbent alumina may have a surface area of 50-400 m<SP>2</SP>/g. It may be basic (pH 8-11 in suspension), neutral (pH 6-8) or acidic (pH 3-6), and the pH of the fine aluminium oxide or hydroxide may be adjusted to the same value, e.g. by acid washing. Fluorescent substances, e.g. Mn-activated Zn silicate, Mg tungstate, or Cd halogen phosphate, Sn-activated Ca phosphate, Mn- or Mn/Pbactivated Ca silicate, Sb- or Sb/Mn-activated Ca halogen phosphate, Na 3-hydroxy-pyrene- 5, 8, 10-trisulphonate, Na3,5-dihydroxypyrene- 8, 10-disulphonate, or morin, may be added. The adsorbent is used in thin layer chromatography and for preparative separations using layers 0À5-5 mm. thick.
GB1054576D 1963-12-14 Active GB1054576A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEM59256A DE1229756B (en) 1963-12-14 1963-12-14 Adsorbent suitable for plate chromatography, especially for preparative thin-layer chromatography

Publications (1)

Publication Number Publication Date
GB1054576A true GB1054576A (en)

Family

ID=7309477

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1054576D Active GB1054576A (en) 1963-12-14

Country Status (7)

Country Link
BE (1) BE656988A (en)
CH (1) CH483856A (en)
DE (1) DE1229756B (en)
DK (1) DK112413B (en)
GB (1) GB1054576A (en)
NL (1) NL6414438A (en)
SE (1) SE306627B (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2423782A1 (en) * 1978-04-17 1979-11-16 Merck Patent Gmbh FLUORESCENCE INDICATORS FOR USE IN CHROMATOGRAPHY AND SORPTION AGENTS CONTAINING THESE INDICATORS

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2423782A1 (en) * 1978-04-17 1979-11-16 Merck Patent Gmbh FLUORESCENCE INDICATORS FOR USE IN CHROMATOGRAPHY AND SORPTION AGENTS CONTAINING THESE INDICATORS

Also Published As

Publication number Publication date
DK112413B (en) 1968-12-09
CH483856A (en) 1970-01-15
NL6414438A (en) 1965-06-15
BE656988A (en) 1965-06-11
SE306627B (en) 1968-12-02
DE1229756B (en) 1966-12-01

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