GB1021197A - Process for the manufacture of lactams - Google Patents
Process for the manufacture of lactamsInfo
- Publication number
- GB1021197A GB1021197A GB760064A GB760064A GB1021197A GB 1021197 A GB1021197 A GB 1021197A GB 760064 A GB760064 A GB 760064A GB 760064 A GB760064 A GB 760064A GB 1021197 A GB1021197 A GB 1021197A
- Authority
- GB
- United Kingdom
- Prior art keywords
- phosphoric acid
- acid
- concentration
- nitric acid
- treatment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000003951 lactams Chemical class 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 16
- 235000011007 phosphoric acid Nutrition 0.000 abstract 8
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 7
- 229910000147 aluminium phosphate Inorganic materials 0.000 abstract 7
- 229910017604 nitric acid Inorganic materials 0.000 abstract 5
- 239000012535 impurity Substances 0.000 abstract 3
- 150000002923 oximes Chemical class 0.000 abstract 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 2
- 229910052801 chlorine Inorganic materials 0.000 abstract 2
- 239000000460 chlorine Substances 0.000 abstract 2
- 238000000605 extraction Methods 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- 239000004793 Polystyrene Substances 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 239000003729 cation exchange resin Substances 0.000 abstract 1
- 229940023913 cation exchange resins Drugs 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000005187 foaming Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 abstract 1
- 239000011368 organic material Substances 0.000 abstract 1
- 229920002223 polystyrene Polymers 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 238000004064 recycling Methods 0.000 abstract 1
- 239000011347 resin Substances 0.000 abstract 1
- 229920005989 resin Polymers 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/02—Preparation of lactams
- C07D201/04—Preparation of lactams from or via oximes by Beckmann rearrangement
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/18—Phosphoric acid
- C01B25/234—Purification; Stabilisation; Concentration
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR926314A FR1357789A (fr) | 1963-02-28 | 1963-02-28 | Procédé de fabrication de lactames |
| FR931891A FR84011E (fr) | 1963-04-18 | 1963-04-18 | Procédé de fabrication de lactames |
| FR931892A FR84559E (fr) | 1963-04-18 | 1963-04-18 | Procédé de fabrication de lactames |
| FR937234A FR84561E (fr) | 1963-06-06 | 1963-06-06 | Procédé de fabrication de lactames |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1021197A true GB1021197A (en) | 1966-03-02 |
Family
ID=27445551
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB760064A Expired GB1021197A (en) | 1963-02-28 | 1964-02-24 | Process for the manufacture of lactams |
Country Status (5)
| Country | Link |
|---|---|
| BE (1) | BE644536A (enrdf_load_stackoverflow) |
| FR (1) | FR1357789A (enrdf_load_stackoverflow) |
| GB (1) | GB1021197A (enrdf_load_stackoverflow) |
| LU (1) | LU45533A1 (enrdf_load_stackoverflow) |
| NL (1) | NL6401618A (enrdf_load_stackoverflow) |
-
1963
- 1963-02-28 FR FR926314A patent/FR1357789A/fr not_active Expired
-
1964
- 1964-02-20 NL NL6401618A patent/NL6401618A/xx unknown
- 1964-02-24 GB GB760064A patent/GB1021197A/en not_active Expired
- 1964-02-26 LU LU45533A patent/LU45533A1/xx unknown
- 1964-02-28 BE BE644536A patent/BE644536A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| LU45533A1 (enrdf_load_stackoverflow) | 1964-04-27 |
| NL6401618A (enrdf_load_stackoverflow) | 1964-08-31 |
| FR1357789A (fr) | 1964-04-10 |
| BE644536A (enrdf_load_stackoverflow) | 1964-06-15 |
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