FR3106829B1 - Process for manufacturing ceramic matrix composites comprising a specific interphase - Google Patents
Process for manufacturing ceramic matrix composites comprising a specific interphase Download PDFInfo
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- FR3106829B1 FR3106829B1 FR2001173A FR2001173A FR3106829B1 FR 3106829 B1 FR3106829 B1 FR 3106829B1 FR 2001173 A FR2001173 A FR 2001173A FR 2001173 A FR2001173 A FR 2001173A FR 3106829 B1 FR3106829 B1 FR 3106829B1
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- interphase
- fibers
- ceramic matrix
- matrix composites
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- 230000016507 interphase Effects 0.000 title abstract 9
- 238000004519 manufacturing process Methods 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 4
- 239000011153 ceramic matrix composite Substances 0.000 title abstract 3
- 239000000835 fiber Substances 0.000 abstract 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 239000000919 ceramic Substances 0.000 abstract 2
- 239000002131 composite material Substances 0.000 abstract 2
- 230000008021 deposition Effects 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- 239000011159 matrix material Substances 0.000 abstract 2
- FAQYAMRNWDIXMY-UHFFFAOYSA-N trichloroborane Chemical compound ClB(Cl)Cl FAQYAMRNWDIXMY-UHFFFAOYSA-N 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 230000008595 infiltration Effects 0.000 abstract 1
- 238000001764 infiltration Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 230000001590 oxidative effect Effects 0.000 abstract 1
- 230000002787 reinforcement Effects 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/71—Ceramic products containing macroscopic reinforcing agents
- C04B35/78—Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
- C04B35/80—Fibres, filaments, whiskers, platelets, or the like
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/56—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
- C04B35/565—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide
- C04B35/571—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide obtained from Si-containing polymer precursors or organosilicon monomers
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/56—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides
- C04B35/565—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide
- C04B35/573—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbides or oxycarbides based on silicon carbide obtained by reaction sintering or recrystallisation
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- C—CHEMISTRY; METALLURGY
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/628—Coating the powders or the macroscopic reinforcing agents
- C04B35/62844—Coating fibres
- C04B35/62857—Coating fibres with non-oxide ceramics
- C04B35/6286—Carbides
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/628—Coating the powders or the macroscopic reinforcing agents
- C04B35/62844—Coating fibres
- C04B35/62857—Coating fibres with non-oxide ceramics
- C04B35/62865—Nitrides
- C04B35/62868—Boron nitride
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/628—Coating the powders or the macroscopic reinforcing agents
- C04B35/62844—Coating fibres
- C04B35/62878—Coating fibres with boron or silicon
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/628—Coating the powders or the macroscopic reinforcing agents
- C04B35/62884—Coating the powders or the macroscopic reinforcing agents by gas phase techniques
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/628—Coating the powders or the macroscopic reinforcing agents
- C04B35/62897—Coatings characterised by their thickness
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/04—Coating on selected surface areas, e.g. using masks
- C23C16/045—Coating cavities or hollow spaces, e.g. interior of tubes; Infiltration of porous substrates
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/455—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
- C23C16/45559—Diffusion of reactive gas to substrate
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/614—Gas infiltration of green bodies or pre-forms
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- C—CHEMISTRY; METALLURGY
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/616—Liquid infiltration of green bodies or pre-forms
Abstract
Procédé de fabrication de composites à matrice céramique comprenant une interphase spécifique Des matériaux composites comportant un renforcement par des fibres et une matrice céramique dans laquelle les fibres revêtues d’une couche mince dénommée interphase sont incluses, sont fabriqués par un procédé caractérisé en ce qu’il comprend : - sur les fibres, la formation d’une interphase par dépôt ou infiltration chimique effectuée en deux étapes enchaînées sans interruption, la principale étape de fabrication étant caractérisée par l’utilisation, pendant au moins 80% du temps de dépôt de toute l’interphase, d’un mélange de gaz composé d’une part au moins d’ammoniac et d’hydrogène et d’autre part de trichlorure de bore et de dichlorure de carbonyle, la concentration de ce dernier étant comprise entre plus de 1% et environ 5% en pourcentage atomique par rapport au trichlorure de bore, interphase dont l’épaisseur totale finale est comprise entre 0,1 et 1 µm ; - le traitement thermique des fibres ainsi revêtues de l’interphase, sans exposition à une atmosphère oxydante après revêtement des fibres par l’interphase, traitement thermique effectué à une température égale ou supérieure à environ 1100°C ; - puis la fabrication du matériau composite par inclusion des fibres revêtues de l’interphase dans la matrice faite de céramique, au moins pour la plus grande partie. Des composites à matrice céramique performants sont fabriqués avec ce procédé moins onéreux.Process for manufacturing ceramic matrix composites comprising a specific interphase Composite materials comprising reinforcement by fibers and a ceramic matrix in which the fibers coated with a thin layer called interphase are included, are manufactured by a process characterized in that it includes: - on the fibers, the formation of an interphase by deposition or chemical infiltration carried out in two stages linked together without interruption, the main manufacturing stage being characterized by the use, for at least 80% of the deposition time of any the interphase, of a mixture of gases composed of at least ammonia and hydrogen on the one hand and boron trichloride and carbonyl dichloride on the other hand, the concentration of the latter being between more than 1 % and approximately 5% in atomic percentage relative to boron trichloride, interphase whose final total thickness is between 0.1 and 1 µm; - the heat treatment of the fibers thus coated with the interphase, without exposure to an oxidizing atmosphere after coating the fibers with the interphase, heat treatment carried out at a temperature equal to or greater than approximately 1100°C; - then the manufacture of the composite material by inclusion of the fibers coated with the interphase in the matrix made of ceramic, at least for the majority. High-performance ceramic matrix composites are manufactured with this less expensive process.
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR2001173A FR3106829B1 (en) | 2020-02-05 | 2020-02-05 | Process for manufacturing ceramic matrix composites comprising a specific interphase |
PCT/FR2020/000284 WO2021156549A1 (en) | 2020-02-05 | 2020-12-22 | Method for manufacturing ceramic matrix composites comprising a specific interphase |
CN202080099288.6A CN115515914B (en) | 2020-02-05 | 2020-12-22 | Method for manufacturing ceramic matrix composite material containing specific interface phase |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR2001173 | 2020-02-05 | ||
FR2001173A FR3106829B1 (en) | 2020-02-05 | 2020-02-05 | Process for manufacturing ceramic matrix composites comprising a specific interphase |
Publications (2)
Publication Number | Publication Date |
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FR3106829A1 FR3106829A1 (en) | 2021-08-06 |
FR3106829B1 true FR3106829B1 (en) | 2023-09-29 |
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FR2001173A Active FR3106829B1 (en) | 2020-02-05 | 2020-02-05 | Process for manufacturing ceramic matrix composites comprising a specific interphase |
Country Status (3)
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CN (1) | CN115515914B (en) |
FR (1) | FR3106829B1 (en) |
WO (1) | WO2021156549A1 (en) |
Families Citing this family (1)
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CN117003566B (en) * | 2023-09-27 | 2023-12-08 | 中国航发北京航空材料研究院 | Preparation device and preparation method of continuous chemical vapor deposition thin belt interface coating |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
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US5015540A (en) | 1987-06-01 | 1991-05-14 | General Electric Company | Fiber-containing composite |
US4889686A (en) | 1989-02-17 | 1989-12-26 | General Electric Company | Composite containing coated fibrous material |
FR2668477B1 (en) | 1990-10-26 | 1993-10-22 | Propulsion Ste Europeenne | REFRACTORY COMPOSITE MATERIAL PROTECTED AGAINST CORROSION, AND METHOD FOR THE PRODUCTION THEREOF. |
WO1996031687A1 (en) | 1995-04-06 | 1996-10-10 | General Electric Company | Method and composite for protection of thermal barrier coating with an impermeable barrier coating |
FR2732338B1 (en) | 1995-03-28 | 1997-06-13 | Europ Propulsion | COMPOSITE MATERIAL PROTECTED AGAINST OXIDATION BY SELF-HEALING MATRIX AND MANUFACTURING METHOD THEREOF |
FR2756277B1 (en) | 1996-11-28 | 1999-04-02 | Europ Propulsion | COMPOSITE MATERIAL WITH CERAMIC MATRIX AND SIC FIBER REINFORCEMENT AND METHOD FOR THE PRODUCTION THEREOF |
US6630029B2 (en) | 2000-12-04 | 2003-10-07 | General Electric Company | Fiber coating method and reactor |
US7364807B2 (en) | 2004-12-06 | 2008-04-29 | General Electric Company | Thermal barrier coating/environmental barrier coating system for a ceramic-matrix composite (CMC) article to improve high temperature capability |
FR2882356B1 (en) * | 2005-02-23 | 2008-08-15 | Snecma Propulsion Solide Sa | METHOD FOR MANUFACTURING PIECE OF COMPOSITE MATERIAL WITH CERAMIC MATRIX AND PART THUS OBTAINED |
WO2007098152A2 (en) | 2006-02-20 | 2007-08-30 | Lee Kang N | Article including enviromental barrier coating system |
FR2933970B1 (en) * | 2008-07-21 | 2012-05-11 | Snecma Propulsion Solide | METHOD FOR MANUFACTURING A PIECE OF THERMOSTRUCTURAL COMPOSITE MATERIAL AND PIECE THUS OBTAINED |
US8986845B2 (en) | 2011-07-22 | 2015-03-24 | United Technologies Corporation | Ceramic composite article having laminar ceramic matrix |
FR2995892B1 (en) * | 2012-09-27 | 2014-10-17 | Herakles | PROCESS FOR MANUFACTURING A CMC PIECE |
US20160229758A1 (en) | 2015-02-11 | 2016-08-11 | United Technologies Corporation | Continuous chemical vapor deposition/infiltration coater |
FR3057864B1 (en) * | 2016-10-25 | 2018-11-23 | Safran Ceram | METHOD OF INFILTRATION OR CHEMICAL VAPOR DEPOSITION USING THE PRECURSOR CI2BNH2 TO FORM BORON NITRIDE |
FR3062336B1 (en) * | 2017-02-02 | 2019-04-12 | Safran Ceramics | PROCESS FOR MANUFACTURING A PIECE OF COMPOSITE MATERIAL |
FR3067026A1 (en) | 2017-05-31 | 2018-12-07 | Lionel Gerard Vandenbulcke | CORROSION RESISTANT CERAMIC MATRIX COMPOSITE AND METHOD FOR MANUFACTURING THE SAME |
US10648348B2 (en) | 2017-06-15 | 2020-05-12 | General Electric Company | Coated ceramic matrix composition component and a method for forming a coated ceramic matrix composition component |
CN109592987B (en) * | 2019-01-15 | 2021-11-19 | 湖南世鑫新材料有限公司 | Preparation method of C/C-SiC composite material containing carbon-rich boron nitride interface phase |
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2020
- 2020-02-05 FR FR2001173A patent/FR3106829B1/en active Active
- 2020-12-22 WO PCT/FR2020/000284 patent/WO2021156549A1/en active Application Filing
- 2020-12-22 CN CN202080099288.6A patent/CN115515914B/en active Active
Also Published As
Publication number | Publication date |
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CN115515914B (en) | 2024-02-09 |
WO2021156549A1 (en) | 2021-08-12 |
CN115515914A (en) | 2022-12-23 |
FR3106829A1 (en) | 2021-08-06 |
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