FR3095440B1 - Procédé de préparation du bis(fluorosulfonyle) imide - Google Patents
Procédé de préparation du bis(fluorosulfonyle) imide Download PDFInfo
- Publication number
- FR3095440B1 FR3095440B1 FR1904384A FR1904384A FR3095440B1 FR 3095440 B1 FR3095440 B1 FR 3095440B1 FR 1904384 A FR1904384 A FR 1904384A FR 1904384 A FR1904384 A FR 1904384A FR 3095440 B1 FR3095440 B1 FR 3095440B1
- Authority
- FR
- France
- Prior art keywords
- imide
- bis
- fluorosulfonyl
- liquid phase
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/086—Compounds containing nitrogen and non-metals and optionally metals containing one or more sulfur atoms
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/087—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
- C01B21/093—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms containing also one or more sulfur atoms
- C01B21/0935—Imidodisulfonic acid; Nitrilotrisulfonic acid; Salts thereof
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
- B01J2204/002—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
- H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
- H01M10/0566—Liquid materials
- H01M10/0568—Liquid materials characterised by the solutes
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
La présente invention concerne un procédé de préparation du bis(fluorosulfonyle) imide comprenant les étapes de : i) la fourniture d’un courant A1 comprenant de l’acide fluorhydrique ; la fourniture d’un réacteur contenant une phase liquide A2 comprenant du bis(halosulfonyle) imide ; la fourniture d’au moins un dispositif de mélange connecté à l’entrée dudit réacteur ; ii) l’alimentation dudit au moins un dispositif de mélange par la phase liquide A2 et par ledit courant A1; iii) mise en contact, dans ledit dispositif de mélange, de ladite phase liquide A2 avec ledit courant A1, pour former un mélange réactionnel B, sous forme liquide, comprenant bis(fluorosulfonyle) imide ; iv) l’introduction du mélange réactionnel B produit à l’étape iii) dans la phase liquide A2 dudit réacteur.
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1904384A FR3095440B1 (fr) | 2019-04-25 | 2019-04-25 | Procédé de préparation du bis(fluorosulfonyle) imide |
| HUE20719206A HUE070072T2 (hu) | 2019-04-25 | 2020-04-21 | Eljárás bisz(fluor-szulfonil)-imid elõállítására |
| US17/604,929 US20220204345A1 (en) | 2019-04-25 | 2020-04-21 | Process for preparing bis(fluorosulfonyl) imide |
| EP20719206.3A EP3959172B1 (fr) | 2019-04-25 | 2020-04-21 | Procede de preparation du bis(fluorosulfonyle) imide |
| PL20719206.3T PL3959172T3 (pl) | 2019-04-25 | 2020-04-21 | Sposób wytwarzania bis(fluorosulfonylo)imidu |
| PCT/EP2020/061064 WO2020216736A1 (fr) | 2019-04-25 | 2020-04-21 | Procede de preparation du bis(fluorosulfonyle) imide |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1904384 | 2019-04-25 | ||
| FR1904384A FR3095440B1 (fr) | 2019-04-25 | 2019-04-25 | Procédé de préparation du bis(fluorosulfonyle) imide |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR3095440A1 FR3095440A1 (fr) | 2020-10-30 |
| FR3095440B1 true FR3095440B1 (fr) | 2022-03-25 |
Family
ID=67956977
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR1904384A Active FR3095440B1 (fr) | 2019-04-25 | 2019-04-25 | Procédé de préparation du bis(fluorosulfonyle) imide |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US20220204345A1 (fr) |
| EP (1) | EP3959172B1 (fr) |
| FR (1) | FR3095440B1 (fr) |
| HU (1) | HUE070072T2 (fr) |
| PL (1) | PL3959172T3 (fr) |
| WO (1) | WO2020216736A1 (fr) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US12421114B2 (en) * | 2021-01-29 | 2025-09-23 | Honeywell International Inc. | Sulfamyl fluoride compositions and processes for making sulfamyl fluoride compositions |
| CN113716534B (zh) * | 2021-08-27 | 2022-04-01 | 中船(邯郸)派瑞特种气体股份有限公司 | 一种双氟磺酰亚胺锂的制备装置及方法 |
| CN114408883A (zh) * | 2022-01-29 | 2022-04-29 | 宁德时代新能源科技股份有限公司 | 回收双氟磺酰亚胺锂的方法 |
| WO2023142046A1 (fr) | 2022-01-29 | 2023-08-03 | 宁德时代新能源科技股份有限公司 | Méthode de récupération de bis(fluorosulfonyl)imide de lithium |
| MA71316A (fr) * | 2022-07-01 | 2025-04-30 | Centre National De La Recherche Scientifique | Procédé de fluoration de bis(chlorosulfonyl)imide d'hydrogène en phase gazeuse |
| CN116040593A (zh) * | 2022-12-30 | 2023-05-02 | 浙江研一新能源科技有限公司 | 一种双氟磺酰亚胺的制备方法、一种双氟磺酰亚胺锂及其制备方法和应用 |
| WO2025132313A1 (fr) * | 2023-12-20 | 2025-06-26 | Specialty Operations France | Procédé de fluoration d'hydrogène bis(chlorosulfonyl)imide en phase gazeuse |
| WO2025132314A1 (fr) * | 2023-12-20 | 2025-06-26 | Specialty Operations France | Procédé de fluoration d'hydrogène bis(chlorosulfonyl)imide en phase gazeuse |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009123328A1 (fr) | 2008-03-31 | 2009-10-08 | Nippon Shokubai Co., Ltd. | Sel sulfonylimide et procédé de production de celui-ci |
| US8722005B1 (en) | 2013-07-26 | 2014-05-13 | Boulder Ionics Corporation | Synthesis of hydrogen bis(fluorosulfonyl)imide |
| KR20180083896A (ko) * | 2015-11-13 | 2018-07-23 | 론자 리미티드 | 비스(플루오로설포닐)-이미드 및 그 염의 제조 방법 |
| CN108290833B (zh) * | 2015-12-04 | 2021-08-31 | 麻省固能控股有限公司 | 生产双(氟磺酰基)酰亚胺的方法 |
-
2019
- 2019-04-25 FR FR1904384A patent/FR3095440B1/fr active Active
-
2020
- 2020-04-21 HU HUE20719206A patent/HUE070072T2/hu unknown
- 2020-04-21 EP EP20719206.3A patent/EP3959172B1/fr active Active
- 2020-04-21 PL PL20719206.3T patent/PL3959172T3/pl unknown
- 2020-04-21 WO PCT/EP2020/061064 patent/WO2020216736A1/fr not_active Ceased
- 2020-04-21 US US17/604,929 patent/US20220204345A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| US20220204345A1 (en) | 2022-06-30 |
| EP3959172B1 (fr) | 2025-01-08 |
| EP3959172A1 (fr) | 2022-03-02 |
| WO2020216736A1 (fr) | 2020-10-29 |
| FR3095440A1 (fr) | 2020-10-30 |
| PL3959172T3 (pl) | 2025-03-10 |
| HUE070072T2 (hu) | 2025-05-28 |
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Legal Events
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| PLFP | Fee payment |
Year of fee payment: 2 |
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| PLSC | Publication of the preliminary search report |
Effective date: 20201030 |
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| CA | Change of address |
Effective date: 20250718 |