FR3084885B1 - MANUFACTURING PROCESS OF A PART IN COMPOSITE MATERIAL - Google Patents

MANUFACTURING PROCESS OF A PART IN COMPOSITE MATERIAL Download PDF

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Publication number
FR3084885B1
FR3084885B1 FR1857400A FR1857400A FR3084885B1 FR 3084885 B1 FR3084885 B1 FR 3084885B1 FR 1857400 A FR1857400 A FR 1857400A FR 1857400 A FR1857400 A FR 1857400A FR 3084885 B1 FR3084885 B1 FR 3084885B1
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FR
France
Prior art keywords
composite material
fiber preform
manufacturing process
suspension
liquid medium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1857400A
Other languages
French (fr)
Other versions
FR3084885A1 (en
Inventor
Pascal Diss
Eric Lavasserie
Eric Bouillon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Safran Ceramics SA
Original Assignee
Safran Ceramics SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Safran Ceramics SA filed Critical Safran Ceramics SA
Priority to FR1857400A priority Critical patent/FR3084885B1/en
Publication of FR3084885A1 publication Critical patent/FR3084885A1/en
Application granted granted Critical
Publication of FR3084885B1 publication Critical patent/FR3084885B1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/447Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on phosphates, e.g. hydroxyapatite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/71Ceramic products containing macroscopic reinforcing agents
    • C04B35/78Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
    • C04B35/80Fibres, filaments, whiskers, platelets, or the like
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B37/00Joining burned ceramic articles with other burned ceramic articles or other articles by heating
    • C04B37/003Joining burned ceramic articles with other burned ceramic articles or other articles by heating by means of an interlayer consisting of a combination of materials selected from glass, or ceramic material with metals, metal oxides or metal salts
    • C04B37/005Joining burned ceramic articles with other burned ceramic articles or other articles by heating by means of an interlayer consisting of a combination of materials selected from glass, or ceramic material with metals, metal oxides or metal salts consisting of glass or ceramic material
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/616Liquid infiltration of green bodies or pre-forms
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/66Specific sintering techniques, e.g. centrifugal sintering
    • C04B2235/668Pressureless sintering
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/02Aspects relating to interlayers, e.g. used to join ceramic articles with other articles by heating
    • C04B2237/04Ceramic interlayers
    • C04B2237/06Oxidic interlayers
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/30Composition of layers of ceramic laminates or of ceramic or metallic articles to be joined by heating, e.g. Si substrates
    • C04B2237/32Ceramic
    • C04B2237/38Fiber or whisker reinforced

Abstract

L'invention concerne notamment un procédé de fabrication d'une pièce en matériau composite, comprenant au moins : - la formation d'une préforme fibreuse imprégnée par une suspension, la suspension comprenant un milieu liquide comprenant un phosphate d'aluminium présentant un rapport atomique Al/P inférieur à 1, et des particules céramiques présentes dans le milieu liquide, et - le traitement thermique de la préforme fibreuse imprégnée à une température comprise entre 350°C et 1050°C afin de former, dans la porosité de la préforme fibreuse, une matrice liant les fibres de la préforme et comprenant du métaphosphate d'aluminium Al(PO3)3 cristallin.The invention relates in particular to a method of manufacturing a part made of composite material, comprising at least: the formation of a fiber preform impregnated with a suspension, the suspension comprising a liquid medium comprising an aluminum phosphate having an atomic ratio Al / P less than 1, and ceramic particles present in the liquid medium, and - the heat treatment of the impregnated fiber preform at a temperature between 350 ° C and 1050 ° C in order to form, in the porosity of the fiber preform , a matrix binding the fibers of the preform and comprising crystalline aluminum metaphosphate Al (PO3) 3.

FR1857400A 2018-08-09 2018-08-09 MANUFACTURING PROCESS OF A PART IN COMPOSITE MATERIAL Active FR3084885B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
FR1857400A FR3084885B1 (en) 2018-08-09 2018-08-09 MANUFACTURING PROCESS OF A PART IN COMPOSITE MATERIAL

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1857400A FR3084885B1 (en) 2018-08-09 2018-08-09 MANUFACTURING PROCESS OF A PART IN COMPOSITE MATERIAL

Publications (2)

Publication Number Publication Date
FR3084885A1 FR3084885A1 (en) 2020-02-14
FR3084885B1 true FR3084885B1 (en) 2021-01-15

Family

ID=65201052

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1857400A Active FR3084885B1 (en) 2018-08-09 2018-08-09 MANUFACTURING PROCESS OF A PART IN COMPOSITE MATERIAL

Country Status (1)

Country Link
FR (1) FR3084885B1 (en)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5260125A (en) * 1991-04-12 1993-11-09 Minnesota Mining And Manufacturing Company Ceramic composite of aluminoborosilicate fibers coated with several layers
FR2858318B1 (en) * 2003-07-31 2007-03-02 Snecma Propulsion Solide PROTECTION AGAINST OXIDATION OF COMPOSITE MATERIALS CONTAINING CARBON AND PARTS THUS PROTECTED
FR3019818B1 (en) * 2014-04-10 2016-05-06 Messier Bugatti Dowty PROTECTION AGAINST THE OXIDATION OF CARBON COMPOSITE MATERIALS

Also Published As

Publication number Publication date
FR3084885A1 (en) 2020-02-14

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