FR3078269B1 - Adsorbeur pour l'epuration ou la separation d'un flux gazeux comprenant un systeme de remplissage amovible - Google Patents

Adsorbeur pour l'epuration ou la separation d'un flux gazeux comprenant un systeme de remplissage amovible Download PDF

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Publication number
FR3078269B1
FR3078269B1 FR1851601A FR1851601A FR3078269B1 FR 3078269 B1 FR3078269 B1 FR 3078269B1 FR 1851601 A FR1851601 A FR 1851601A FR 1851601 A FR1851601 A FR 1851601A FR 3078269 B1 FR3078269 B1 FR 3078269B1
Authority
FR
France
Prior art keywords
granular material
particle size
adsorber
filling system
dna
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1851601A
Other languages
English (en)
Other versions
FR3078269A1 (fr
Inventor
Guillaume Rodrigues
Bernard Fraioli
Patrick Pereira
Patrick Le Bot
Benjamin Morineau
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Priority to FR1851601A priority Critical patent/FR3078269B1/fr
Priority to US16/975,046 priority patent/US11679355B2/en
Priority to RU2020129172A priority patent/RU2778060C2/ru
Priority to PCT/FR2019/050293 priority patent/WO2019162591A1/fr
Priority to CN201980013707.7A priority patent/CN111727081B/zh
Priority to EP19710735.2A priority patent/EP3755452A1/fr
Publication of FR3078269A1 publication Critical patent/FR3078269A1/fr
Application granted granted Critical
Publication of FR3078269B1 publication Critical patent/FR3078269B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0242—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical
    • B01J8/025—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly vertical in a cylindrical shaped bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0407—Constructional details of adsorbing systems
    • B01D53/0423—Beds in columns
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B01J8/003—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor in a downward flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0453—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/02—Preparation of oxygen
    • C01B13/0229—Purification or separation processes
    • C01B13/0248—Physical processing only
    • C01B13/0259—Physical processing only by adsorption on solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/30—Physical properties of adsorbents
    • B01D2253/302—Dimensions
    • B01D2253/304—Linear dimensions, e.g. particle shape, diameter
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/12—Oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/414—Further details for adsorption processes and devices using different types of adsorbents
    • B01D2259/4141—Further details for adsorption processes and devices using different types of adsorbents within a single bed
    • B01D2259/4145—Further details for adsorption processes and devices using different types of adsorbents within a single bed arranged in series
    • B01D2259/4146—Contiguous multilayered adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B01D53/0476—Vacuum pressure swing adsorption
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00752—Feeding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00884—Means for supporting the bed of particles, e.g. grids, bars, perforated plates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)

Abstract

Adsorbeur pour l'épuration ou la séparation d'un flux gazeux comprenant une virole cylindrique (R), un fond bombé inférieur (F1), un fond bombé supérieur (F2) comprenant un orifice principal de remplissage d'un matériau granulaire, avec ledit orifice présentant un diamètre intérieur Din, un matériau granulaire de granulométrie ADN, un matériau granulaire de granulométrie M et un système de remplissage (A) amovible de la virole en matériau granulaire positionné dans l'orifice principal de remplissage, caractérisé en ce que : - le système de remplissage (A) est composé d'un cylindre perforé sur toute ou partie de sa hauteur, de son fond supérieur de diamètre Dext et de son fond inférieur, - la distance Din-Dext est strictement supérieure à deux fois la taille des particules du matériau de granulométrie M, - le matériau granulaire de granulométrie ADN et le matériau granulaire de granulométrie M se succèdent dans le sens de circulation du flux gazeux et sont tels que M > ADN - le matériau de granulométrie M est en contact à fois avec au moins une partie de la surface extérieure du système (A) et au moins une partie de la surface intérieure du fond bombé supérieur (F2).
FR1851601A 2018-02-23 2018-02-23 Adsorbeur pour l'epuration ou la separation d'un flux gazeux comprenant un systeme de remplissage amovible Active FR3078269B1 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
FR1851601A FR3078269B1 (fr) 2018-02-23 2018-02-23 Adsorbeur pour l'epuration ou la separation d'un flux gazeux comprenant un systeme de remplissage amovible
US16/975,046 US11679355B2 (en) 2018-02-23 2019-02-11 Adsorber for purifying or separating a gas stream comprising a removable filling system
RU2020129172A RU2778060C2 (ru) 2018-02-23 2019-02-11 Адсорбер для очистки или разделения потока газа, содержащий съемную систему заполнения
PCT/FR2019/050293 WO2019162591A1 (fr) 2018-02-23 2019-02-11 Adsorbeur pour l'épuration ou la séparation d'un flux gazeux comprenant un système de remplissage amovible
CN201980013707.7A CN111727081B (zh) 2018-02-23 2019-02-11 包括可移除的填充系统的用于净化或分离气流的吸附器
EP19710735.2A EP3755452A1 (fr) 2018-02-23 2019-02-11 Adsorbeur pour l'épuration ou la séparation d'un flux gazeux comprenant un système de remplissage amovible

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1851601A FR3078269B1 (fr) 2018-02-23 2018-02-23 Adsorbeur pour l'epuration ou la separation d'un flux gazeux comprenant un systeme de remplissage amovible
FR1851601 2018-02-23

Publications (2)

Publication Number Publication Date
FR3078269A1 FR3078269A1 (fr) 2019-08-30
FR3078269B1 true FR3078269B1 (fr) 2020-02-14

Family

ID=62222919

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1851601A Active FR3078269B1 (fr) 2018-02-23 2018-02-23 Adsorbeur pour l'epuration ou la separation d'un flux gazeux comprenant un systeme de remplissage amovible

Country Status (5)

Country Link
US (1) US11679355B2 (fr)
EP (1) EP3755452A1 (fr)
CN (1) CN111727081B (fr)
FR (1) FR3078269B1 (fr)
WO (1) WO2019162591A1 (fr)

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2884372A (en) * 1956-05-29 1959-04-28 Socony Mobil Oil Co Inc Spherical reactor for the conversion of hydrocarbons
DE1100660B (de) * 1957-09-05 1961-03-02 Linde S Eismaschinen Ag Zweign Vorrichtung zur Vorreinigung eines fuer die Zerlegung durch Kompression und Tiefkuehlung bestimmten Gasgemisches
US3479146A (en) * 1966-10-28 1969-11-18 Exxon Research Engineering Co Fluid flow distributor
DE2516223C3 (de) 1975-04-14 1978-12-14 Linde Ag, 6200 Wiesbaden Verfahren und Vorrichtung zum Regenerieren von Adsorbent
US4372857A (en) * 1981-03-05 1983-02-08 Union Carbide Corporation Liquid adsorption process and apparatus
US4938422A (en) * 1987-12-23 1990-07-03 Uop Inlet distributor for downflow reactor
FI903220A (fi) * 1990-06-26 1991-12-27 Uop Inc Tvaoriktad foerdelningsapparat foer inkommande vaetska, avsedd nedstroemskaerl innehaollande en baedd av fasta partiklar.
US5538544A (en) * 1994-12-27 1996-07-23 Praxair Technology, Inc. Adsorption flow distribution
FR2750617B1 (fr) * 1996-07-02 1998-09-25 Air Liquide Distributeur de gaz destine a etre fixe dans une bouteille de traitement de gaz et bouteille de gaz le comportant
US5769928A (en) * 1996-12-12 1998-06-23 Praxair Technology, Inc. PSA gas purifier and purification process
US5836362A (en) * 1997-07-15 1998-11-17 Praxair Technology, Inc. Multiple adsorbent loading method and apparatus for a radial flow vessel
US6089950A (en) 1998-06-01 2000-07-18 C. J. Associates, Ltd. Toy figure with articulating joints
EP1080722A1 (fr) * 1999-08-31 2001-03-07 Novartis AG Compositions antimycotiques
US6334889B1 (en) * 1999-09-01 2002-01-01 Praxair Technology, Inc. Bed restraint for an adsorber
US6605135B2 (en) 2001-09-26 2003-08-12 Air Products And Chemicals, Inc. Granular bed restraint system
US7166151B2 (en) * 2004-01-15 2007-01-23 Praxair Technology, Inc. Flow distributor for PSA vessel
US9861947B2 (en) * 2012-02-28 2018-01-09 Phillips 66 Company Reactor inlet vapor velocity equalizer and distributor
US9034084B2 (en) * 2013-03-27 2015-05-19 Lummus Technology Inc. Apparatus for distributing flow
US20160158770A1 (en) * 2014-12-04 2016-06-09 Chevron U.S.A. Inc. Gas distributor and method of use thereof

Also Published As

Publication number Publication date
RU2020129172A (ru) 2022-03-03
RU2020129172A3 (fr) 2022-03-29
CN111727081A (zh) 2020-09-29
CN111727081B (zh) 2022-08-23
WO2019162591A1 (fr) 2019-08-29
US11679355B2 (en) 2023-06-20
EP3755452A1 (fr) 2020-12-30
FR3078269A1 (fr) 2019-08-30
US20200398211A1 (en) 2020-12-24

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