FR3063914B1 - Procede de fabrication d'une dispersion de gouttes d'une premiere phase dans une deuxieme phase immiscible par fragmentation d'un jet et coacervation - Google Patents

Procede de fabrication d'une dispersion de gouttes d'une premiere phase dans une deuxieme phase immiscible par fragmentation d'un jet et coacervation Download PDF

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FR3063914B1
FR3063914B1 FR1752215A FR1752215A FR3063914B1 FR 3063914 B1 FR3063914 B1 FR 3063914B1 FR 1752215 A FR1752215 A FR 1752215A FR 1752215 A FR1752215 A FR 1752215A FR 3063914 B1 FR3063914 B1 FR 3063914B1
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France
Prior art keywords
phase
liquid
drops
dispersion
duct
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FR1752215A
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FR3063914A1 (fr
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Javier Angel Tesan
Elodie Galandrin
Mathieu Goutayer
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Capsum SAS
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Capsum SAS
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/06—Making microcapsules or microballoons by phase separation
    • B01J13/10—Complex coacervation, i.e. interaction of oppositely charged particles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/06—Emulsions
    • A61K8/066—Multiple emulsions, e.g. water-in-oil-in-water
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/11—Encapsulated compositions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25—Silicon; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89—Polysiloxanes
    • A61K8/896—Polysiloxanes containing atoms other than silicon, carbon, oxygen and hydrogen, e.g. dimethicone copolyol phosphate
    • A61K8/898—Polysiloxanes containing atoms other than silicon, carbon, oxygen and hydrogen, e.g. dimethicone copolyol phosphate containing nitrogen, e.g. amodimethicone, trimethyl silyl amodimethicone or dimethicone propyl PG-betaine
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10—General cosmetic use
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Dermatology (AREA)
  • Inorganic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Cosmetics (AREA)
  • Colloid Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

Procédé de fabrication d'une dispersion (5) comprenant des gouttes (17) d'une première phase (10), la dispersion comprenant en outre une deuxième phase (15) sensiblement immiscible avec la première phase et dans laquelle les gouttes sont dispersées, comprenant au moins les étapes suivantes : - écoulement d'un premier liquide (27) comprenant la première phase dans un premier conduit (43) ; - écoulement d'un deuxième liquide (31) comprenant la deuxième phase dans un deuxième conduit (45) entourant de manière concentrique le premier conduit ; le premier liquide comprenant en outre au moins un premier polymère et le deuxième liquide comprenant en outre au moins un deuxième polymère apte à réagir avec le premier polymère pour former une couche de coacervat, et/ou le premier liquide comprenant en outre au moins un agent gélifiant ; - obtention d'un jet liquide (23) en sortie du deuxième conduit dans une atmosphère gazeuse (64) ; - fragmentation du jet liquide dans l'atmosphère gazeuse et obtention de gouttes composites (24) comprenant une couche externe formée par le deuxième liquide ; - formation d'une écorce (19) par coacervation, et/ou gélification de la première phase par l'agent gélifiant; et - récupération des gouttes composites et obtention de la dispersion, la couche externe venant s'ajouter à la deuxième phase par coalescence.
FR1752215A 2017-03-17 2017-03-17 Procede de fabrication d'une dispersion de gouttes d'une premiere phase dans une deuxieme phase immiscible par fragmentation d'un jet et coacervation Active FR3063914B1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
FR1752215A FR3063914B1 (fr) 2017-03-17 2017-03-17 Procede de fabrication d'une dispersion de gouttes d'une premiere phase dans une deuxieme phase immiscible par fragmentation d'un jet et coacervation

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1752215A FR3063914B1 (fr) 2017-03-17 2017-03-17 Procede de fabrication d'une dispersion de gouttes d'une premiere phase dans une deuxieme phase immiscible par fragmentation d'un jet et coacervation
FR1752215 2017-03-17

Publications (2)

Publication Number Publication Date
FR3063914A1 FR3063914A1 (fr) 2018-09-21
FR3063914B1 true FR3063914B1 (fr) 2021-10-01

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3121042B1 (fr) * 2021-03-29 2023-11-10 Laboratoires Lea Nouvelle composition comprenant une phase grasse dispersée sous forme de gouttelettes dans une phase aqueuse continue liquide
CN115445461A (zh) * 2022-08-17 2022-12-09 广东省科学院生物与医学工程研究所 双层微液滴生成装置以及双层微液滴生成方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2964017B1 (fr) * 2010-09-01 2013-05-31 Capsum Procede de fabrication d'une serie de capsules de taille submillimetrique
US10300006B2 (en) * 2011-03-08 2019-05-28 Capsum Method for forming drops of a first phase, dispersed in a second phase substantially immiscible with the first phase
FR3012050B1 (fr) * 2013-10-17 2016-01-01 Capsum Procede de formation d'une dispersion comprenant des gouttes, et appareil associe

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FR3063914A1 (fr) 2018-09-21

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