FR3049604B1 - Procede de preparation de particules de platine conductrices de protons a forte surface active greffees a leur surface par des polymeres conducteurs de protons specifiques - Google Patents

Procede de preparation de particules de platine conductrices de protons a forte surface active greffees a leur surface par des polymeres conducteurs de protons specifiques Download PDF

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Publication number
FR3049604B1
FR3049604B1 FR1652936A FR1652936A FR3049604B1 FR 3049604 B1 FR3049604 B1 FR 3049604B1 FR 1652936 A FR1652936 A FR 1652936A FR 1652936 A FR1652936 A FR 1652936A FR 3049604 B1 FR3049604 B1 FR 3049604B1
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France
Prior art keywords
proton
conducting polymers
platinum particles
preparing high
particles grafted
Prior art date
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Expired - Fee Related
Application number
FR1652936A
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English (en)
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FR3049604A1 (fr
Inventor
Pierrick Buvat
Janick Bigarre
Christophe Coutanceau
Steve Baranton
Delphine Dru
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Commissariat a lEnergie Atomique et aux Energies Alternatives CEA
Original Assignee
Centre National de la Recherche Scientifique CNRS
Commissariat a lEnergie Atomique CEA
Universite de Poitiers
Commissariat a lEnergie Atomique et aux Energies Alternatives CEA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Centre National de la Recherche Scientifique CNRS, Commissariat a lEnergie Atomique CEA, Universite de Poitiers, Commissariat a lEnergie Atomique et aux Energies Alternatives CEA filed Critical Centre National de la Recherche Scientifique CNRS
Priority to FR1652936A priority Critical patent/FR3049604B1/fr
Priority to ES17715680T priority patent/ES2816067T3/es
Priority to CA3019644A priority patent/CA3019644A1/fr
Priority to PCT/EP2017/057879 priority patent/WO2017174524A1/fr
Priority to EP17715680.9A priority patent/EP3440727B1/fr
Priority to US16/089,240 priority patent/US10673076B2/en
Publication of FR3049604A1 publication Critical patent/FR3049604A1/fr
Application granted granted Critical
Publication of FR3049604B1 publication Critical patent/FR3049604B1/fr
Expired - Fee Related legal-status Critical Current
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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/90—Selection of catalytic material
    • H01M4/9008—Organic or organo-metallic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/42—Platinum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/009—Preparation by separation, e.g. by filtration, decantation, screening
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0213—Preparation of the impregnating solution
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06—Washing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16—Reducing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/34—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation
    • B01J37/341—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation
    • B01J37/343—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation of ultrasonic wave energy
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/34—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation
    • B01J37/341—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation
    • B01J37/344—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation of electromagnetic wave energy
    • B01J37/346—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation of electromagnetic wave energy of microwave energy
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/50—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton
    • C07C323/51—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C323/52—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and carboxyl groups bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F112/00—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
    • C08F112/02—Monomers containing only one unsaturated aliphatic radical
    • C08F112/04—Monomers containing only one unsaturated aliphatic radical containing one ring
    • C08F112/14—Monomers containing only one unsaturated aliphatic radical containing one ring substituted by hetero atoms or groups containing heteroatoms
    • C08F112/30—Sulfur
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F12/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
    • C08F12/02—Monomers containing only one unsaturated aliphatic radical
    • C08F12/04—Monomers containing only one unsaturated aliphatic radical containing one ring
    • C08F12/14—Monomers containing only one unsaturated aliphatic radical containing one ring substituted by hetero atoms or groups containing heteroatoms
    • C08F12/30—Sulfur
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F292/00—Macromolecular compounds obtained by polymerising monomers on to inorganic materials
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/90—Selection of catalytic material
    • H01M4/92—Metals of platinum group
    • H01M4/923—Compounds thereof with non-metallic elements
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/90—Selection of catalytic material
    • H01M4/92—Metals of platinum group
    • H01M4/925—Metals of platinum group supported on carriers, e.g. powder carriers
    • H01M4/926—Metals of platinum group supported on carriers, e.g. powder carriers on carbon or graphite
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2438/00—Living radical polymerisation
    • C08F2438/01—Atom Transfer Radical Polymerization [ATRP] or reverse ATRP
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/50—Fuel cells

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Optics & Photonics (AREA)
  • Plasma & Fusion (AREA)
  • Toxicology (AREA)
  • Electromagnetism (AREA)
  • Inorganic Chemistry (AREA)
  • Inert Electrodes (AREA)
  • Catalysts (AREA)

Abstract

L'invention a trait à un procédé spécifique de préparation de particules de platine greffées par des polymères conducteurs de protons. Utilisation de ces particules comme catalyseurs pour la réduction de l'oxygène.
FR1652936A 2016-04-04 2016-04-04 Procede de preparation de particules de platine conductrices de protons a forte surface active greffees a leur surface par des polymeres conducteurs de protons specifiques Expired - Fee Related FR3049604B1 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
FR1652936A FR3049604B1 (fr) 2016-04-04 2016-04-04 Procede de preparation de particules de platine conductrices de protons a forte surface active greffees a leur surface par des polymeres conducteurs de protons specifiques
ES17715680T ES2816067T3 (es) 2016-04-04 2017-04-03 Procedimiento de preparación de partículas de platino conductoras de protones con una gran superficie activa injertadas en su superficie con polímeros conductores de protones específicos
CA3019644A CA3019644A1 (fr) 2016-04-04 2017-04-03 Procede de preparation de particules de platine conductrices de protons a forte surface active greffees a leur surface par des polymeres conducteurs de protons specifiques
PCT/EP2017/057879 WO2017174524A1 (fr) 2016-04-04 2017-04-03 Procede de preparation de particules de platine conductrices de protons a forte surface active greffees a leur surface par des polymeres conducteurs de protons specifiques
EP17715680.9A EP3440727B1 (fr) 2016-04-04 2017-04-03 Procede de preparation de particules de platine conductrices de protons a forte surface active greffees a leur surface par des polymeres conducteurs de protons specifiques
US16/089,240 US10673076B2 (en) 2016-04-04 2017-04-03 Method for producing proton-conducting platinum particles with a large active surface area and surface-grafted with specific, proton-conducting polymers

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1652936A FR3049604B1 (fr) 2016-04-04 2016-04-04 Procede de preparation de particules de platine conductrices de protons a forte surface active greffees a leur surface par des polymeres conducteurs de protons specifiques
FR1652936 2016-04-04

Publications (2)

Publication Number Publication Date
FR3049604A1 FR3049604A1 (fr) 2017-10-06
FR3049604B1 true FR3049604B1 (fr) 2018-04-13

Family

ID=56008799

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FR1652936A Expired - Fee Related FR3049604B1 (fr) 2016-04-04 2016-04-04 Procede de preparation de particules de platine conductrices de protons a forte surface active greffees a leur surface par des polymeres conducteurs de protons specifiques

Country Status (6)

Country Link
US (1) US10673076B2 (fr)
EP (1) EP3440727B1 (fr)
CA (1) CA3019644A1 (fr)
ES (1) ES2816067T3 (fr)
FR (1) FR3049604B1 (fr)
WO (1) WO2017174524A1 (fr)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3055105B1 (fr) * 2016-08-19 2018-09-21 Commissariat A L'energie Atomique Et Aux Energies Alternatives Procede de preparation de particules aptes a catalyser la reduction de l'oxygene ou l'oxydation de l'hydrogene conductrices de protons par greffage a leur surface de polymeres fluores conducteurs de protons specifiques
FR3062075B1 (fr) 2017-01-25 2021-09-10 Commissariat Energie Atomique Particules inorganiques conductrices de protons, procede de preparation de celles-ci et utilisation de celles-ci pour constituer une membrane de pile a combustible
FR3062122B1 (fr) 2017-01-25 2019-04-19 Commissariat A L'energie Atomique Et Aux Energies Alternatives Particules inorganiques conductrices de protons fluorees et utilisation de ces particules dans des membranes conductrices de protons

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2982264B1 (fr) * 2011-11-07 2014-12-26 Commissariat Energie Atomique Procede de preparation de particules aptes a catalyser la reduction de l'oxygene ou l'oxydation de l'hydrogene conductrices de protons par greffage a leur surface de polymeres conducteurs de protons
FR2982173B1 (fr) * 2011-11-07 2014-12-26 Commissariat Energie Atomique Procede de preparation de particules aptes a catalyser la reduction de l'oxygene ou l'oxydation de l'hydrogene conductrices de protons

Also Published As

Publication number Publication date
FR3049604A1 (fr) 2017-10-06
EP3440727A1 (fr) 2019-02-13
US10673076B2 (en) 2020-06-02
EP3440727B1 (fr) 2020-06-24
CA3019644A1 (fr) 2017-10-12
WO2017174524A1 (fr) 2017-10-12
ES2816067T3 (es) 2021-03-31
US20190109329A1 (en) 2019-04-11

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