FR3032722B1 - PROCESS FOR EXTRACTING ZIRCONIUM AND HAFNIUM FROM A MIXTURE - Google Patents

PROCESS FOR EXTRACTING ZIRCONIUM AND HAFNIUM FROM A MIXTURE Download PDF

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Publication number
FR3032722B1
FR3032722B1 FR1551151A FR1551151A FR3032722B1 FR 3032722 B1 FR3032722 B1 FR 3032722B1 FR 1551151 A FR1551151 A FR 1551151A FR 1551151 A FR1551151 A FR 1551151A FR 3032722 B1 FR3032722 B1 FR 3032722B1
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FR
France
Prior art keywords
hafnium
zirconium
mixture
yttrium
dissolved
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1551151A
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French (fr)
Other versions
FR3032722A1 (en
Inventor
Auriane GENGO
Laurent Cassayre
Philippe DESTRAC
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Safran Aircraft Engines SAS
Centre National de la Recherche Scientifique CNRS
Institut National Polytechnique de Toulouse INPT
Original Assignee
Safran Aircraft Engines SAS
Centre National de la Recherche Scientifique CNRS
Institut National Polytechnique de Toulouse INPT
SNECMA SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Safran Aircraft Engines SAS, Centre National de la Recherche Scientifique CNRS, Institut National Polytechnique de Toulouse INPT, SNECMA SAS filed Critical Safran Aircraft Engines SAS
Priority to FR1551151A priority Critical patent/FR3032722B1/en
Publication of FR3032722A1 publication Critical patent/FR3032722A1/en
Application granted granted Critical
Publication of FR3032722B1 publication Critical patent/FR3032722B1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/006Wet processes
    • C22B7/007Wet processes by acid leaching
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/14Obtaining zirconium or hafnium
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Organic Chemistry (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

La présente invention concerne un procédé d'extraction du zirconium et du hafnium d'un mélange comportant au moins les étapes suivantes : a) dissoudre tout ou partie d'un matériau céramique à traiter comprenant au moins du zirconium, du hafnium et de l'yttrium par un solvant aqueux présentant un pH inférieur ou égal à 2 afin d'obtenir une composition liquide dans laquelle le zirconium, le hafnium et l'yttrium dudit matériau sont dissous, et b) extraire sélectivement le zirconium et le hafnium dissous dans la composition en les séparant de l'yttrium dissous dans la composition afin d'obtenir un premier produit d'extraction comprenant le zirconium et le hafnium ainsi sélectivement extraits.The present invention relates to a method for extracting zirconium and hafnium from a mixture comprising at least the following steps: a) dissolving all or part of a ceramic material to be treated comprising at least zirconium, hafnium and yttrium with an aqueous solvent having a pH of less than or equal to 2 in order to obtain a liquid composition in which the zirconium, hafnium and yttrium of said material are dissolved, and b) selectively extract zirconium and hafnium dissolved in the composition separating them from yttrium dissolved in the composition in order to obtain a first extraction product comprising zirconium and hafnium thus selectively extracted.

FR1551151A 2015-02-12 2015-02-12 PROCESS FOR EXTRACTING ZIRCONIUM AND HAFNIUM FROM A MIXTURE Active FR3032722B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
FR1551151A FR3032722B1 (en) 2015-02-12 2015-02-12 PROCESS FOR EXTRACTING ZIRCONIUM AND HAFNIUM FROM A MIXTURE

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1551151 2015-02-12
FR1551151A FR3032722B1 (en) 2015-02-12 2015-02-12 PROCESS FOR EXTRACTING ZIRCONIUM AND HAFNIUM FROM A MIXTURE

Publications (2)

Publication Number Publication Date
FR3032722A1 FR3032722A1 (en) 2016-08-19
FR3032722B1 true FR3032722B1 (en) 2019-05-31

Family

ID=53674021

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1551151A Active FR3032722B1 (en) 2015-02-12 2015-02-12 PROCESS FOR EXTRACTING ZIRCONIUM AND HAFNIUM FROM A MIXTURE

Country Status (1)

Country Link
FR (1) FR3032722B1 (en)

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU3898785A (en) * 1984-02-22 1985-08-29 Iron Ore Co. Of Canada Recovery of zirconium (and the like) by solvent extraction

Also Published As

Publication number Publication date
FR3032722A1 (en) 2016-08-19

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