FR2419301A1 - Procede de preparation de polyethers glycidyliques monomeres de polyphenols, de faible viscosite - Google Patents

Procede de preparation de polyethers glycidyliques monomeres de polyphenols, de faible viscosite

Info

Publication number
FR2419301A1
FR2419301A1 FR7807530A FR7807530A FR2419301A1 FR 2419301 A1 FR2419301 A1 FR 2419301A1 FR 7807530 A FR7807530 A FR 7807530A FR 7807530 A FR7807530 A FR 7807530A FR 2419301 A1 FR2419301 A1 FR 2419301A1
Authority
FR
France
Prior art keywords
polyphenol
prod
low
equiv
chlorine content
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7807530A
Other languages
English (en)
Other versions
FR2419301B1 (fr
Inventor
Jean Louis Locatelli
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhone Poulenc Industries SA
Original Assignee
Rhone Poulenc Industries SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhone Poulenc Industries SA filed Critical Rhone Poulenc Industries SA
Priority to FR7807530A priority Critical patent/FR2419301A1/fr
Publication of FR2419301A1 publication Critical patent/FR2419301A1/fr
Application granted granted Critical
Publication of FR2419301B1 publication Critical patent/FR2419301B1/fr
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/02Polycondensates containing more than one epoxy group per molecule
    • C08G59/04Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof
    • C08G59/06Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols
    • C08G59/063Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols with epihalohydrins
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Epoxy Resins (AREA)

Abstract

La présente invention se rapporte à un procédé perfectionné de préparation d'éthers glycidyliques monomères de polyphénols, de faible viscosité, par réaction de l'épichlorhydrine en excès sur un polyphénol, et déshydrochloration du produit obtenu. Le procédé consiste notamment à introduire, rapidement et uniformément, une solution aqueuse d'agent alcalin à raison de 0,85 à 0,98 mole d'agent alcalin par équivalent hydroxy du polyphénol engagé, à éliminer simultanément l'eau du milieu réactionnel, puis à distiller l'épichlorhydrine restante et à éliminer le sel formé, avant de soumettre la résine à la déshydrochloration. Le procédé convient notamment à la fabrication du diéther glycidylique du bisphénol-A.
FR7807530A 1978-03-07 1978-03-07 Procede de preparation de polyethers glycidyliques monomeres de polyphenols, de faible viscosite Granted FR2419301A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
FR7807530A FR2419301A1 (fr) 1978-03-07 1978-03-07 Procede de preparation de polyethers glycidyliques monomeres de polyphenols, de faible viscosite

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7807530A FR2419301A1 (fr) 1978-03-07 1978-03-07 Procede de preparation de polyethers glycidyliques monomeres de polyphenols, de faible viscosite

Publications (2)

Publication Number Publication Date
FR2419301A1 true FR2419301A1 (fr) 1979-10-05
FR2419301B1 FR2419301B1 (fr) 1981-10-30

Family

ID=9205839

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7807530A Granted FR2419301A1 (fr) 1978-03-07 1978-03-07 Procede de preparation de polyethers glycidyliques monomeres de polyphenols, de faible viscosite

Country Status (1)

Country Link
FR (1) FR2419301A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016035668A1 (fr) * 2014-09-03 2016-03-10 Dic株式会社 Résine époxy, procédé de production de résine époxy, composition de résine durcissable, produit durci, matériau composite renforcé par des fibres, et article moulé

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1116397B (de) * 1955-01-31 1961-11-02 Bataafsche Petroleum Verfahren zur Herstellung von niedrigmolekularen Glycidylaethern mehrwertiger Phenole

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1116397B (de) * 1955-01-31 1961-11-02 Bataafsche Petroleum Verfahren zur Herstellung von niedrigmolekularen Glycidylaethern mehrwertiger Phenole

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2016035668A1 (fr) * 2014-09-03 2016-03-10 Dic株式会社 Résine époxy, procédé de production de résine époxy, composition de résine durcissable, produit durci, matériau composite renforcé par des fibres, et article moulé
JP6008064B2 (ja) * 2014-09-03 2016-10-19 Dic株式会社 エポキシ樹脂、エポキシ樹脂の製造方法、硬化性樹脂組成物、その硬化物、繊維強化複合材料、及び成形品
EP3190135A4 (fr) * 2014-09-03 2018-02-28 DIC Corporation Résine époxy, procédé de production de résine époxy, composition de résine durcissable, produit durci, matériau composite renforcé par des fibres, et article moulé
US10047190B2 (en) 2014-09-03 2018-08-14 Dic Corporation Epoxy resin, method for producing epoxy resin, curable resin composition, cured product, fiber reinforced composite material, and molded article

Also Published As

Publication number Publication date
FR2419301B1 (fr) 1981-10-30

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Legal Events

Date Code Title Description
TP Transmission of property
ST Notification of lapse