FR2375244A1 - Procede de preparation de l'acide 2-carboxyethyl (phenyl) phosphinique - Google Patents

Procede de preparation de l'acide 2-carboxyethyl (phenyl) phosphinique

Info

Publication number
FR2375244A1
FR2375244A1 FR7739118A FR7739118A FR2375244A1 FR 2375244 A1 FR2375244 A1 FR 2375244A1 FR 7739118 A FR7739118 A FR 7739118A FR 7739118 A FR7739118 A FR 7739118A FR 2375244 A1 FR2375244 A1 FR 2375244A1
Authority
FR
France
Prior art keywords
phenyl
carboxyethyl
phosphinic acid
preparation
degrees
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7739118A
Other languages
English (en)
Other versions
FR2375244B1 (fr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Monsanto Co
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Co filed Critical Monsanto Co
Publication of FR2375244A1 publication Critical patent/FR2375244A1/fr
Application granted granted Critical
Publication of FR2375244B1 publication Critical patent/FR2375244B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/49—Phosphorus-containing compounds
    • C08K5/51—Phosphorus bound to oxygen
    • C08K5/53—Phosphorus bound to oxygen bound to oxygen and to carbon only
    • C08K5/5313—Phosphinic compounds, e.g. R2=P(:O)OR'
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/301—Acyclic saturated acids which can have further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/49—Phosphorus-containing compounds
    • C08K5/51—Phosphorus bound to oxygen
    • C08K5/53—Phosphorus bound to oxygen bound to oxygen and to carbon only

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

L'invention concerne un procédé de préparation de l'acide 2-carboxyéthyl (phényl) phosphinique. On mélange de la dichloro (phényl) phosphine entre 80 degrés C et 150 degrés C, avec de l'acide acrylique dans la proportion de 25 et 45 % d'excès molaire d'acide acrylique et on hydrolyse ensuite le mélange résultant à l'aide d'eau. Application du procédé à la fabrication de l'acide phosphinique avec un rendement élevé.
FR7739118A 1976-12-27 1977-12-23 Procede de preparation de l'acide 2-carboxyethyl (phenyl) phosphinique Granted FR2375244A1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/755,363 US4081463A (en) 1976-12-27 1976-12-27 Production of 2-carboxyethyl(phenyl)phosphinic acid

Publications (2)

Publication Number Publication Date
FR2375244A1 true FR2375244A1 (fr) 1978-07-21
FR2375244B1 FR2375244B1 (fr) 1980-10-17

Family

ID=25038834

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7739118A Granted FR2375244A1 (fr) 1976-12-27 1977-12-23 Procede de preparation de l'acide 2-carboxyethyl (phenyl) phosphinique

Country Status (7)

Country Link
US (1) US4081463A (fr)
JP (1) JPS6021600B2 (fr)
DE (1) DE2757770A1 (fr)
FR (1) FR2375244A1 (fr)
GB (1) GB1543688A (fr)
IT (1) IT1089254B (fr)
NL (1) NL7714249A (fr)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4769182A (en) * 1985-06-05 1988-09-06 Hoechst Celanese Corporation Process for production of 3-(hydroxyphenylphosphinyl)-propanoic acid
JP2990953B2 (ja) * 1991-08-09 1999-12-13 堺化学工業株式会社 ホスフィニルカルボン酸誘導体の製造方法
CN1070195C (zh) * 1994-01-27 2001-08-29 三洋化成工业株式会社 制备有机磷酯化合物的方法
US5399428A (en) * 1994-03-11 1995-03-21 Monsanto Company Flame retardant polyester copolymers
US5399429A (en) * 1994-03-11 1995-03-21 Monsanto Company Flame retardant recycled polyester copolymers
US5750603A (en) * 1997-05-23 1998-05-12 Solutia Inc. Polymer-bound non-halogen fire resistant compositions
US5952406A (en) * 1997-05-27 1999-09-14 Solutia Inc. Fire retarded polyamide
DE19739852B4 (de) * 1997-09-11 2006-03-16 Zimmer Ag Verfahren zur Herstellung von flammfesten Polyestern
KR19990070137A (ko) * 1998-02-17 1999-09-15 한형수 난연성 폴리에스터의 제조방법
US6838497B2 (en) * 1998-09-02 2005-01-04 Cheil Industries Inc. Flame retardant thermoplastic resin composition containing styrene polymer as compatabilizer and oxaphospholane compound as flame retardant
WO2000049025A1 (fr) * 1999-02-19 2000-08-24 Solutia Inc. Production d'acide 2-carboxyakyl (phenyl) phosphinique
KR100632988B1 (ko) * 1999-09-07 2006-10-11 주식회사 새 한 3-(히드록시페닐포스피닐)-프로파노익 에시드의 제조방법
EP1092722B1 (fr) * 1999-10-11 2002-09-11 Saehan Industries, Inc. Méthode de préparation d' acide 3-(hydroxyphényl phosphinyl)-propanoique
EP1099705B1 (fr) * 1999-11-12 2004-02-11 Saehan Industries, Inc. Procédé pour la préparation de l'acide 3-(hydroxyphenylphosphinyl)-propanoique
DE10002163A1 (de) * 2000-01-20 2001-07-26 Mitsubishi Polyester Film Gmbh Weiße, schwerentflammbare, UV-stabile Folie aus einem kristallisierbaren Thermoplasten, Verfahren zu ihrer Herstellung und ihre Verwendung
US6399814B1 (en) * 2000-03-20 2002-06-04 Solutia Inc. Process for the preparation of 2-carboxyalkyl(aryl)phosphinic acid and corresponding anhydride(s)
CN103333201A (zh) * 2013-06-27 2013-10-02 南通泰通化学科技有限公司 2-羧乙基苯基次膦酸阻燃剂的制备方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2268158A (en) * 1939-05-05 1941-12-30 Carl S Marvel Esters of gamma oxophosphonic acids

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2268158A (en) * 1939-05-05 1941-12-30 Carl S Marvel Esters of gamma oxophosphonic acids

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
CA1967 *
CA1968 *

Also Published As

Publication number Publication date
NL7714249A (nl) 1978-06-29
FR2375244B1 (fr) 1980-10-17
IT1089254B (it) 1985-06-18
JPS5382757A (en) 1978-07-21
US4081463A (en) 1978-03-28
JPS6021600B2 (ja) 1985-05-28
DE2757770A1 (de) 1978-06-29
GB1543688A (en) 1979-04-04

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Legal Events

Date Code Title Description
ST Notification of lapse