FR2178748A1 - Carbon fibres - for reinforcing materials esp synthetic resins - Google Patents

Carbon fibres - for reinforcing materials esp synthetic resins

Info

Publication number
FR2178748A1
FR2178748A1 FR7211897A FR7211897A FR2178748A1 FR 2178748 A1 FR2178748 A1 FR 2178748A1 FR 7211897 A FR7211897 A FR 7211897A FR 7211897 A FR7211897 A FR 7211897A FR 2178748 A1 FR2178748 A1 FR 2178748A1
Authority
FR
France
Prior art keywords
fibres
layer
carbon fibres
degrees
salt
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7211897A
Other languages
French (fr)
Other versions
FR2178748B1 (en
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bpifrance Financement SA
Original Assignee
Agence National de Valorisation de la Recherche ANVAR
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Agence National de Valorisation de la Recherche ANVAR filed Critical Agence National de Valorisation de la Recherche ANVAR
Priority to FR7211897A priority Critical patent/FR2178748A1/en
Publication of FR2178748A1 publication Critical patent/FR2178748A1/en
Application granted granted Critical
Publication of FR2178748B1 publication Critical patent/FR2178748B1/fr
Granted legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F11/00—Chemical after-treatment of artificial filaments or the like during manufacture
    • D01F11/10—Chemical after-treatment of artificial filaments or the like during manufacture of carbon
    • D01F11/12—Chemical after-treatment of artificial filaments or the like during manufacture of carbon with inorganic substances ; Intercalation
    • D01F11/122—Oxygen, oxygen-generating compounds
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F11/00—Chemical after-treatment of artificial filaments or the like during manufacture
    • D01F11/10—Chemical after-treatment of artificial filaments or the like during manufacture of carbon
    • D01F11/16—Chemical after-treatment of artificial filaments or the like during manufacture of carbon by physicochemical methods

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Inorganic Fibers (AREA)

Abstract

Title carbon fibres have a surface layer of graphite oxide with a thickness of 0.1-0.4 mu. The layer of graphitic oxide contains 3-15 wt.% oxygenated functions, based on total wt. of fibres. The oxide layer is formed on carbon fibres which have been subjected to thermal treatment at >1000 degrees C and possess a modulus of elasticity of >=15,000 hectobars. The fibres are produced by (a) immersing carbon fibres in a reagent bath capable of forming a layer of a graphite salt on the fibres; (b) simultaneously or subsequently converting the salt layer into an oxide layer (c) washing the fibres with water, and (d) drying. The fibres are treated in (1) a bath contg. KClO3 for 4-24 hrs. at 25 degrees C, (2) a bath contg. KMnO4 for 5-15 mins at 35-40 degrees C, or (3) a nitric acid bath contg. an oxidising salt.
FR7211897A 1972-04-05 1972-04-05 Carbon fibres - for reinforcing materials esp synthetic resins Granted FR2178748A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
FR7211897A FR2178748A1 (en) 1972-04-05 1972-04-05 Carbon fibres - for reinforcing materials esp synthetic resins

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7211897A FR2178748A1 (en) 1972-04-05 1972-04-05 Carbon fibres - for reinforcing materials esp synthetic resins

Publications (2)

Publication Number Publication Date
FR2178748A1 true FR2178748A1 (en) 1973-11-16
FR2178748B1 FR2178748B1 (en) 1974-08-02

Family

ID=9096350

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7211897A Granted FR2178748A1 (en) 1972-04-05 1972-04-05 Carbon fibres - for reinforcing materials esp synthetic resins

Country Status (1)

Country Link
FR (1) FR2178748A1 (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0057492A2 (en) * 1981-01-05 1982-08-11 BASF Aktiengesellschaft Process for the surface modification of carbon fibres
EP0168669A2 (en) * 1984-06-22 1986-01-22 Toray Industries, Inc. Ultrahigh strength carbon fibers
US5965470A (en) * 1989-05-15 1999-10-12 Hyperion Catalysis International, Inc. Composites containing surface treated carbon microfibers
US7410628B2 (en) 1992-01-15 2008-08-12 Hyperion Catalysis International, Inc. Surface treatment of carbon microfibers
US10106421B2 (en) 2015-12-16 2018-10-23 Korea Institute Of Science And Technology Composition and method for depolymerization of cured epoxy resin materials using transition metal salts
JP2018177970A (en) * 2017-04-13 2018-11-15 コリア・インスティテュート・オブ・サイエンス・アンド・テクノロジー Method and composition for depolymerization of epoxy resin cured article using transition metal salt or transition metal oxide

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1238308A (en) * 1967-08-14 1971-07-07

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1238308A (en) * 1967-08-14 1971-07-07

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0057492A2 (en) * 1981-01-05 1982-08-11 BASF Aktiengesellschaft Process for the surface modification of carbon fibres
EP0057492A3 (en) * 1981-01-05 1983-11-16 Celanese Corporation Process for the surface modification of carbon fibres
EP0168669A2 (en) * 1984-06-22 1986-01-22 Toray Industries, Inc. Ultrahigh strength carbon fibers
EP0168669A3 (en) * 1984-06-22 1989-05-03 Toray Industries, Inc. Ultrahigh strength carbon fibers
US5965470A (en) * 1989-05-15 1999-10-12 Hyperion Catalysis International, Inc. Composites containing surface treated carbon microfibers
US7410628B2 (en) 1992-01-15 2008-08-12 Hyperion Catalysis International, Inc. Surface treatment of carbon microfibers
US7862794B2 (en) 1992-01-15 2011-01-04 Hyperion Cataylsis International, Inc. Surface treatment of carbon microfibers
US10106421B2 (en) 2015-12-16 2018-10-23 Korea Institute Of Science And Technology Composition and method for depolymerization of cured epoxy resin materials using transition metal salts
JP2018177970A (en) * 2017-04-13 2018-11-15 コリア・インスティテュート・オブ・サイエンス・アンド・テクノロジー Method and composition for depolymerization of epoxy resin cured article using transition metal salt or transition metal oxide

Also Published As

Publication number Publication date
FR2178748B1 (en) 1974-08-02

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Legal Events

Date Code Title Description
ST Notification of lapse