ES424112A1 - Apparatus for the recovery of sublimation products from reaction gases - Google Patents

Apparatus for the recovery of sublimation products from reaction gases

Info

Publication number
ES424112A1
ES424112A1 ES424112A ES424112A ES424112A1 ES 424112 A1 ES424112 A1 ES 424112A1 ES 424112 A ES424112 A ES 424112A ES 424112 A ES424112 A ES 424112A ES 424112 A1 ES424112 A1 ES 424112A1
Authority
ES
Spain
Prior art keywords
tubes
fin
rows
superimposed
tube
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES424112A
Other languages
Spanish (es)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of ES424112A1 publication Critical patent/ES424112A1/en
Expired legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F9/00Casings; Header boxes; Auxiliary supports for elements; Auxiliary members within casings
    • F28F9/007Auxiliary supports for elements
    • F28F9/013Auxiliary supports for elements for tubes or tube-assemblies
    • F28F9/0138Auxiliary supports for elements for tubes or tube-assemblies formed by sleeves for finned tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D7/00Sublimation
    • B01D7/02Crystallisation directly from the vapour phase
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/54Preparation of carboxylic acid anhydrides
    • C07C51/573Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Heat-Exchange Devices With Radiators And Conduit Assemblies (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Furan Compounds (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

Abstract

Improvements in sublimators to obtain sublimation products, especially phthalic acid anhydride, from reaction gases, which consist of a closed casing for the reception or conduction through the reaction gas and several rows of tubes provided with fins mounted there superimposed in an approximately horizontal position inside which a heating medium or a cooling medium circulates alternately and in which the reaction gas is conducted inside the casing in a crossed direction with respect to the flow of heating medium or cooling pipes inside the tubes, the fin tubes of each row having been joined, arranged in each case superimposed, alternately with one of their ends in the form of a hairpin by an elbow bend and endowing themselves at the opposite ends with the means of connection for feeding or evacuating the heating or cooling medium and in which the tubes or rows of superimposed tubes, are supported in a limitedly movable way and spaced from each other to allow different thermal expansions, characterized in that at least in both end zones of each fin tube -with arrangement or distribution equal to each other with respect to the totality of the tubes - slip shoes are attached that surround the fin tube in a box-shaped shape, but are perforated in the form of a cage, whereby the fin tubes, adjacent in height to each other, rest loose on each other, resting the Skate shoes, stacked directly one on top of the other, of the different fin tubes of all the tube rows or of groups of tube rows also loosely on support beams, in each case common, anchored in the casing. (Machine-translation by Google Translate, not legally binding)
ES424112A 1973-03-10 1974-03-09 Apparatus for the recovery of sublimation products from reaction gases Expired ES424112A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2312088A DE2312088C3 (en) 1973-03-10 1973-03-10 Desublimator for the extraction of sublimation products from reaction gases

Publications (1)

Publication Number Publication Date
ES424112A1 true ES424112A1 (en) 1976-05-16

Family

ID=5874464

Family Applications (1)

Application Number Title Priority Date Filing Date
ES424112A Expired ES424112A1 (en) 1973-03-10 1974-03-09 Apparatus for the recovery of sublimation products from reaction gases

Country Status (13)

Country Link
JP (1) JPS596683B2 (en)
AT (1) AT346283B (en)
AU (1) AU475213B2 (en)
BE (1) BE812077A (en)
BR (1) BR7401710D0 (en)
CA (1) CA1015533A (en)
DE (1) DE2312088C3 (en)
ES (1) ES424112A1 (en)
FR (1) FR2220291B1 (en)
GB (1) GB1461461A (en)
IN (1) IN138675B (en)
IT (1) IT1003661B (en)
ZA (1) ZA741524B (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4570704A (en) * 1984-03-26 1986-02-18 L & M Radiator, Inc. Support for heat exchanger tubes
DE19512845C1 (en) * 1995-04-06 1996-07-11 Balcke Duerr Gmbh Crystalliser for sublimed material with supported spirally-finned tube bundle

Also Published As

Publication number Publication date
IT1003661B (en) 1976-06-10
DE2312088C3 (en) 1981-10-15
DE2312088A1 (en) 1974-09-12
AU475213B2 (en) 1976-08-12
CA1015533A (en) 1977-08-16
FR2220291B1 (en) 1980-03-14
BE812077A (en) 1974-09-09
JPS507782A (en) 1975-01-27
JPS596683B2 (en) 1984-02-14
FR2220291A1 (en) 1974-10-04
BR7401710D0 (en) 1974-11-19
GB1461461A (en) 1977-01-13
IN138675B (en) 1976-03-13
ZA741524B (en) 1975-03-26
DE2312088B2 (en) 1980-07-31
AT346283B (en) 1978-11-10
ATA194874A (en) 1978-03-15
AU6626674A (en) 1975-09-11

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