ES403962A1 - Method for preparing the equimolecular salt of piperazine and 1,2-diphenyl-4-butyl-3,5-dioxo-pyrazolidine - Google Patents
Method for preparing the equimolecular salt of piperazine and 1,2-diphenyl-4-butyl-3,5-dioxo-pyrazolidineInfo
- Publication number
- ES403962A1 ES403962A1 ES403962A ES403962A ES403962A1 ES 403962 A1 ES403962 A1 ES 403962A1 ES 403962 A ES403962 A ES 403962A ES 403962 A ES403962 A ES 403962A ES 403962 A1 ES403962 A1 ES 403962A1
- Authority
- ES
- Spain
- Prior art keywords
- pyrazolidine
- dioxo
- diphenyl
- butyl
- piperazine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/28—Two oxygen or sulfur atoms
- C07D231/30—Two oxygen or sulfur atoms attached in positions 3 and 5
- C07D231/32—Oxygen atoms
- C07D231/34—Oxygen atoms with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, attached in position 4
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Detergent Compositions (AREA)
Abstract
Process for the preparation of a derivative of a substituted pyrazolidine and, more particularly, for the preparation of the equimolar salt of piperazine and of diphenyl-1,2-butyl-4-dioxo-3,5-pyrazolidine, characterized by by dissolving anhydrous piperazine and diphenyl-1,2-butyl-4-dioxo-3,5-pyrazolidine separately in the same organic solvent chosen from ketones, ethers, esters and aliphatic chlorinated hydrocarbons according to the formula Cx Hy Clz, in which x = 1,2 or 3; y = 0 to 6 included and z = 1 to 6 included, the solutions obtained being mixed together with stirring and a temperature between 20ºC and the boiling temperature of the solvent, adding seed crystals to the reactive mixture that is subjected to stirring until it is obtain a precipitate of the salt to be obtained, said precipitate then being separated by filtration, washing and drying. (Machine-translation by Google Translate, not legally binding)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1988171A GB1394673A (en) | 1971-06-10 | 1971-06-10 | Method for preparing the equimolecular salt of piperazine and 1,2-diphenyl-4-butyl-3,5-dioxo-pyrazolidine |
Publications (1)
Publication Number | Publication Date |
---|---|
ES403962A1 true ES403962A1 (en) | 1975-05-01 |
Family
ID=10136738
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES403962A Expired ES403962A1 (en) | 1971-06-10 | 1972-06-07 | Method for preparing the equimolecular salt of piperazine and 1,2-diphenyl-4-butyl-3,5-dioxo-pyrazolidine |
Country Status (13)
Country | Link |
---|---|
JP (1) | JPS519002B1 (en) |
AR (1) | AR196994A1 (en) |
AT (1) | AT327197B (en) |
BE (1) | BE784521A (en) |
CA (1) | CA985284A (en) |
CH (1) | CH533118A (en) |
DD (1) | DD98929A5 (en) |
DE (1) | DE2227813A1 (en) |
ES (1) | ES403962A1 (en) |
FR (1) | FR2141338A5 (en) |
GB (1) | GB1394673A (en) |
LU (1) | LU65484A1 (en) |
NL (1) | NL7207877A (en) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS53157112U (en) * | 1977-05-16 | 1978-12-09 | ||
JPS5462514U (en) * | 1977-10-12 | 1979-05-01 | ||
JPS63142321U (en) * | 1987-03-11 | 1988-09-20 | ||
JPH0220098U (en) * | 1988-07-27 | 1990-02-09 |
-
1971
- 1971-06-10 GB GB1988171A patent/GB1394673A/en not_active Expired
-
1972
- 1972-06-07 BE BE784521A patent/BE784521A/en unknown
- 1972-06-07 ES ES403962A patent/ES403962A1/en not_active Expired
- 1972-06-08 DE DE19722227813 patent/DE2227813A1/en active Pending
- 1972-06-08 AT AT493272A patent/AT327197B/en not_active IP Right Cessation
- 1972-06-08 CH CH852472A patent/CH533118A/en not_active IP Right Cessation
- 1972-06-08 LU LU65484D patent/LU65484A1/xx unknown
- 1972-06-09 CA CA144,388A patent/CA985284A/en not_active Expired
- 1972-06-09 DD DD16358572A patent/DD98929A5/xx unknown
- 1972-06-09 NL NL7207877A patent/NL7207877A/xx unknown
- 1972-06-09 FR FR7220853A patent/FR2141338A5/fr not_active Expired
- 1972-06-09 AR AR24247772A patent/AR196994A1/en active
- 1972-06-10 JP JP5813272A patent/JPS519002B1/ja active Pending
Also Published As
Publication number | Publication date |
---|---|
ATA493272A (en) | 1975-04-15 |
CH533118A (en) | 1973-01-31 |
AT327197B (en) | 1976-01-26 |
JPS519002B1 (en) | 1976-03-23 |
GB1394673A (en) | 1975-05-21 |
FR2141338A5 (en) | 1973-01-19 |
AR196994A1 (en) | 1974-03-08 |
NL7207877A (en) | 1972-12-12 |
LU65484A1 (en) | 1972-10-05 |
CA985284A (en) | 1976-03-09 |
BE784521A (en) | 1972-10-02 |
DE2227813A1 (en) | 1973-01-04 |
DD98929A5 (en) | 1973-07-12 |
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