ES394493A1 - Procedure for the obtaining of a benzoyl chloride phenyl hydrazone. (Machine-translation by Google Translate, not legally binding) - Google Patents

Procedure for the obtaining of a benzoyl chloride phenyl hydrazone. (Machine-translation by Google Translate, not legally binding)

Info

Publication number
ES394493A1
ES394493A1 ES394493A ES394493A ES394493A1 ES 394493 A1 ES394493 A1 ES 394493A1 ES 394493 A ES394493 A ES 394493A ES 394493 A ES394493 A ES 394493A ES 394493 A1 ES394493 A1 ES 394493A1
Authority
ES
Spain
Prior art keywords
benzoyl chloride
inclusive
translation
obtaining
machine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES394493A
Other languages
Spanish (es)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Pharmacia and Upjohn Co
Original Assignee
Upjohn Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Upjohn Co filed Critical Upjohn Co
Publication of ES394493A1 publication Critical patent/ES394493A1/en
Expired legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/13Amines
    • A61K31/15Oximes (>C=N—O—); Hydrazines (>N—N<); Hydrazones (>N—N=) ; Imines (C—N=C)
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C243/00Compounds containing chains of nitrogen atoms singly-bound to each other, e.g. hydrazines, triazanes
    • C07C243/24Hydrazines having nitrogen atoms of hydrazine groups acylated by carboxylic acids
    • C07C243/38Hydrazines having nitrogen atoms of hydrazine groups acylated by carboxylic acids with acylating carboxyl groups bound to carbon atoms of six-membered aromatic rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/72Hydrazones

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Process for obtaining a phenylhydrazone of benzoyl chloride, characterized in that a phenylhydrazide of benzoic acid of the formula is reacted ** (see formula) ** With phosphorus pentachloride in the presence of a reaction medium at a temperature in the range 10ºC up to the boiling point of the reaction mixture, thus producing the corresponding benzoyl chloride (dichlorophosphinyl) phenylhydrazone, which is decomposed by the addition of three or more equivalent of phenol to give triphenyl phosphate and the desired benzoyl chloride phenylhydrazone of the formula ** (see formula) ** Wherein x is halogen, alkyl of 1 to 6 carbon atoms, inclusive, and nitro; y is halogen, alkyl of 1 to 6 carbon atoms, inclusive and nitro; n is an integer from 0 to 5, inclusive; m is an integer from 0 to 3, inclusive, the sum of n + m being no more than 6, the sum of the carbon atoms in alkyl substituents being no more than 15 and there being no more than one nitro group in the molecule. (Machine-translation by Google Translate, not legally binding)
ES394493A 1970-08-26 1971-08-24 Procedure for the obtaining of a benzoyl chloride phenyl hydrazone. (Machine-translation by Google Translate, not legally binding) Expired ES394493A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US6722070A 1970-08-26 1970-08-26

Publications (1)

Publication Number Publication Date
ES394493A1 true ES394493A1 (en) 1976-01-01

Family

ID=22074525

Family Applications (1)

Application Number Title Priority Date Filing Date
ES394493A Expired ES394493A1 (en) 1970-08-26 1971-08-24 Procedure for the obtaining of a benzoyl chloride phenyl hydrazone. (Machine-translation by Google Translate, not legally binding)

Country Status (3)

Country Link
ES (1) ES394493A1 (en)
FR (1) FR2103533A2 (en)
ZA (1) ZA713026B (en)

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3879543A (en) * 1968-03-04 1975-04-22 Upjohn Co Certain benzoyl chloride phenylhydrazones as insecticides and miticides
DE1770773A1 (en) * 1968-07-02 1971-12-09 Henkel & Cie Gmbh Optical brightening agent

Also Published As

Publication number Publication date
FR2103533B2 (en) 1975-03-14
FR2103533A2 (en) 1972-04-14
ZA713026B (en) 1973-03-28

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