ES2526141T3 - Granulated powder and process for producing granulated powder - Google Patents
Granulated powder and process for producing granulated powder Download PDFInfo
- Publication number
- ES2526141T3 ES2526141T3 ES11155966.2T ES11155966T ES2526141T3 ES 2526141 T3 ES2526141 T3 ES 2526141T3 ES 11155966 T ES11155966 T ES 11155966T ES 2526141 T3 ES2526141 T3 ES 2526141T3
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- ES
- Spain
- Prior art keywords
- pva
- derivative
- glycerin
- dealkylamine
- granulated powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/14—Treatment of metallic powder
- B22F1/148—Agglomerating
Abstract
Un polvo granulado que comprende una pluralidad de partículas metálicas unidas entre sí por un aglutinante orgánico, en el que el aglutinante orgánico contiene poli(alcohol vinílico) o un derivado del mismo, un poliol y una amina orgánica o un derivado de la misma, y una relación de densidad aparente del polvo granulado a densidad real de las partículas metálicas de 20 a 50 %.A granular powder comprising a plurality of metal particles bonded together by an organic binder, wherein the organic binder contains polyvinyl alcohol or a derivative thereof, a polyol, and an organic amine or derivative thereof, and a ratio of the bulk density of the granulated powder to the real density of the metallic particles of 20 to 50%.
Description
Tabla 1 Table 1
- Polvometálico Dusting
- Aglutinante orgánico Relación deaglutinanteorgánico enpolvogranulado Resultados de evaluación Organic binder Powdergranulated organic binder ratio Evaluation Results
- Poli(alcohol vinílico) Poly (vinyl alcohol)
- Poliol Amina orgánica Relaciónde dens. aparentea dens.real Densidaddemoldeo Densidad desinterización Densidadrelativa Precisión dimensional Polyol Organic amine Density Ratio it looks like dens.real Molding density Deinterity Density Relative density Dimensional accuracy
- 100partesen peso 100 parts by weight
- Composición Partesenpeso Composición Partesenpeso Composición Partesenpeso % en peso % g/cm3 g/cm3 % - Composition Parts by weight Composition Parts by weight Composition Parts by weight % in weigh % g / cm3 g / cm3 % -
- Ejemplo 1 Example 1
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,01 Derivado dealquilamina 0,1 0,90 29,4 6,47 7,42 94,8 B 2% Ni-Fe PVA 0.8 Glycerin 0.01 Dealkylamine derivative 0.1 0.90 29.4 6.47 7.42 94.8 B
- Ejemplo 2 Example 2
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,03 Derivado dealquilamina 0,1 0,92 32,2 6,49 7,45 95,2 A 2% Ni-Fe PVA 0.8 Glycerin 0.03 Dealkylamine derivative 0.1 0.92 32.2 6.49 7.45 95.2 TO
- Ejemplo 3 Example 3
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,05 Derivado dealquilamina 0,1 0,94 35,0 6,52 7,48 95,6 A 2% Ni-Fe PVA 0.8 Glycerin 0.05 Dealkylamine derivative 0.1 0.94 35.0 6.52 7.48 95.6 TO
- Ejemplo 4 Example 4
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,07 Derivado dealquilamina 0,1 0,96 29,4 6,47 7,42 94,8 A 2% Ni-Fe PVA 0.8 Glycerin 0.07 Dealkylamine derivative 0.1 0.96 29.4 6.47 7.42 94.8 TO
- Ejemplo 5 Example 5
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,1 Derivado dealquilamina 0,1 0,99 24,7 6,43 7,37 94,2 B 2% Ni-Fe PVA 0.8 Glycerin 0.1 Dealkylamine derivative 0.1 0.99 24.7 6.43 7.37 94.2 B
- Ejemplo 6 Example 6
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,2 Derivado dealquilamina 0,1 1,09 23,1 6,42 7,36 94,0 B 2% Ni-Fe PVA 0.8 Glycerin 0.2 Dealkylamine derivative 0.1 1.09 23.1 6.42 7.36 94.0 B
- Ejemplo 7 Example 7
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,3 Derivado dealquilamina 0,1 1,19 21,9 6,40 7,34 93,8 B 2% Ni-Fe PVA 0.8 Glycerin 0.3 Dealkylamine derivative 0.1 1.19 21.9 6.40 7.34 93.8 B
- Ejemplo 8 Example 8
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,5 Derivado dealquilamina 0,1 1,38 22,8 6,41 7,35 93,9 B 2% Ni-Fe PVA 0.8 Glycerin 0.5 Dealkylamine derivative 0.1 1.38 22.8 6.41 7.35 93.9 B
- Ejemplo 9 Example 9
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,7 Derivado dealquilamina 0,1 1,57 22,8 6,41 7,35 93,9 C 2% Ni-Fe PVA 0.8 Glycerin 0.7 Dealkylamine derivative 0.1 1.57 22.8 6.41 7.35 93.9 C
- Ejemplo 10 Example 10
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,05 Derivado dealquilamina 0,001 0,84 30,4 6,45 7,43 94,9 B 2% Ni-Fe PVA 0.8 Glycerin 0.05 Dealkylamine derivative 0.001 0.84 30.4 6.45 7.43 94.9 B
- Ejemplo 11 Example 11
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,05 Derivado dealquilamina 0,005 0,85 33,2 6,49 7,45 95,2 A 2% Ni-Fe PVA 0.8 Glycerin 0.05 Dealkylamine derivative 0.005 0.85 33.2 6.49 7.45 95.2 TO
- Ejemplo 12 Example 12
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,05 Derivado dealquilamina 0,01 9,85 34,1 6,51 7,48 95,6 A 2% Ni-Fe PVA 0.8 Glycerin 0.05 Dealkylamine derivative 0.01 9.85 34.1 6.51 7.48 95.6 TO
- Ejemplo 13 Example 13
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,05 Derivado dealquilamina 0,5 1,33 35,4 6,54 7,50 95,8 A 2% Ni-Fe PVA 0.8 Glycerin 0.05 Dealkylamine derivative 0.5 1.33 35.4 6.54 7.50 95.8 TO
- Ejemplo 14 Example 14
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,05 Derivado dealquilamina 1 1,82 35,1 6,53 7,49 95,7 A 2% Ni-Fe PVA 0.8 Glycerin 0.05 Dealkylamine derivative one 1.82 35.1 6.53 7.49 95.7 TO
- Ejemplo 15 Example 15
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,05 Derivado dealquilamina 5 5,53 31,6 6,45 7,41 94,7 B 2% Ni-Fe PVA 0.8 Glycerin 0.05 Dealkylamine derivative 5 5.53 31.6 6.45 7.41 94.7 B
15 fifteen
Tabla 2 Table 2
- Polvometálico Dusting
- Aglutinante orgánico Relación deaglutinanteorgánico enpolvogranulado Resultados de evaluación Organic binder Powdergranulated organic binder ratio Evaluation Results
- Poli(alcohol vinílico) Poly (vinyl alcohol)
- Poliol Amina orgánica Relaciónde dens. aparentea dens.real Densidaddemoldeo Densidad desinterización Densidadrelativa Precisióndimensional Polyol Organic amine Density Ratio it looks like dens.real Molding density Deinterity Density Relative density Dimensional accuracy
- 100partesen peso 100 parts by weight
- Composición Partesenpeso Composición Partesenpeso Composición Partesenpeso % en peso % g/cm3 g/cm3 % - Composition Parts by weight Composition Parts by weight Composition Parts by weight % in weigh % g / cm3 g / cm3 % -
- Ejemplo 16 Example 16
- 2 % de Ni-Fe PVA 0,1 Glicerina 0,05 Derivado dealquilamina 0,1 0,25 40,3 39,7 7,34 93,8 B 2% Ni-Fe PVA 0.1 Glycerin 0.05 Dealkylamine derivative 0.1 0.25 40.3 39.7 7.34 93.8 B
- Ejemplo 17 Example 17
- 2 % de Ni-Fe PVA 0,2 Glicerina 0,05 Derivado dealquilamina 0,1 0,35 36,8 6,47 7,42 94,8 A 2% Ni-Fe PVA 0.2 Glycerin 0.05 Dealkylamine derivative 0.1 0.35 36.8 6.47 7.42 94.8 TO
- Ejemplo 18 Example 18
- 2 % de Ni-Fe PVA 0,5 Glicerina 0,05 Derivado dealquilamina 0,1 0,65 35,9 6,50 7,45 95,2 A 2% Ni-Fe PVA 0.5 Glycerin 0.05 Dealkylamine derivative 0.1 0.65 35.9 6.50 7.45 95.2 TO
- Ejemplo 19 Example 19
- 2 % de Ni-Fe PVA 1 Glicerina 0,05 Derivado dealquilamina 0,1 1,14 24,3 6,51 7,47 95,4 A 2% Ni-Fe PVA one Glycerin 0.05 Dealkylamine derivative 0.1 1.14 24.3 6.51 7.47 95.4 TO
- Ejemplo 20 Example 20
- 2 % de Ni-Fe PVA 2 Glicerina 0,05 Derivado dealquilamina 0,1 2,10 21,1 6,43 7,37 94,2 B 2% Ni-Fe PVA 2 Glycerin 0.05 Dealkylamine derivative 0.1 2.10 21.1 6.43 7.37 94.2 B
- Ejemplo 21 Example 21
- 2 % de Ni-Fe PVA 3 Glicerina 0,05 Derivado dealquilamina 0,1 3,05 20,3 6,24 7,31 93,4 B 2% Ni-Fe PVA 3 Glycerin 0.05 Dealkylamine derivative 0.1 3.05 20.3 6.24 7.31 93.4 B
- Ejemplo 22 Example 22
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,05 - - 0,84 29,4 6,44 7,42 94,8 B 2% Ni-Fe PVA 0.8 Glycerin 0.05 - - 0.84 29.4 6.44 7.42 94.8 B
- Ejemplo 23 Example 23
- 2 % de Ni-Fe PVA 0,8 Etilenglicol 0,05 Derivado dealquilamina 0,1 0,94 25,6 6,48 7,38 94,3 B 2% Ni-Fe PVA 0.8 Ethylene glycol 0.05 Dealkylamine derivative 0.1 0.94 25.6 6.48 7.38 94.3 B
- Ejemplo 24 Example 24
- 2 % de Ni-Fe PVA 0,8 Propilenglicol 0,05 Derivado dealquilamina 0,1 0,94 27,5 6,49 7,40 94,5 B 2% Ni-Fe PVA 0.8 Propylene glycol 0.05 Dealkylamine derivative 0.1 0.94 27.5 6.49 7.40 94.5 B
- Ejemplo 25 Example 25
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,05 Derivado de cicloalquilamina 0,1 0,94 23,8 6,46 7,36 94,0 B 2% Ni-Fe PVA 0.8 Glycerin 0.05 Cycloalkylamine derivative 0.1 0.94 23.8 6.46 7.36 94.0 B
- Ejemplo 26 Example 26
- 2 % de Ni-Fe PVA 0,8 Glicerina 0,05 Derivado dealcanolamina 0,1 0,94 22,8 6,45 7,35 93,9 B 2% Ni-Fe PVA 0.8 Glycerin 0.05 Alkanolamine derivative 0.1 0.94 22.8 6.45 7.35 93.9 B
- Ejemplo 27 Example 27
- SUS316L PVA 0,8 Glicerina 0,05 - - 0,84 30,4 - 7,56 94,7 B SUS316L PVA 0.8 Glycerin 0.05 - - 0.84 30.4 - 7.56 94.7 B
- Ejemplo 28 Example 28
- SUS316L PVA 0,8 Glicerina 0,05 Derivado dealquilamina 0,1 0,94 47,2 - 7,61 95,4 A SUS316L PVA 0.8 Glycerin 0.05 Dealkylamine derivative 0.1 0.94 47.2 - 7.61 95.4 TO
16 16
Tabla 2 (continuación)Table 2 (continued)
- Polvometálico Dusting
- Aglutinante orgánico Relación deaglutinanteorgánico enpolvogranulado Resultados de evaluación Organic binder Powdergranulated organic binder ratio Evaluation Results
- Poli(alcohol vinílico) Poly (vinyl alcohol)
- Poliol Amina orgánica Relación de dens. aparentea dens.real Densidaddemoldeo Densidad desinterización Densidadrelativa Precisióndimensional Polyol Organic amine Density Ratio it looks like dens.real Molding density Deinterity Density Relative density Dimensional accuracy
- 100partesen peso 100 parts by weight
- Composición Partesenpeso Composición Partesenpeso Composición Partesenpeso % en peso % g/cm3 g/cm3 % - Composition Parts by weight Composition Parts by weight Composition Parts by weight % in weigh % g / cm3 g / cm3 % -
- Ejemplocomp. 1 Examplecomp. one
- 2 % de Ni-Fe PVA 0,8 - - - - 0,79 17,2 6,45 7,29 93,1 C 2% Ni-Fe PVA 0.8 - - - - 0.79 17.2 6.45 7.29 93.1 C
- Ejemplo comp. 2 Comp example 2
- 2 % de Ni-Fe PVA 0,05 - - - - 0,05 54,1 6,47 6,95 88,8 D 2% Ni-Fe PVA 0.05 - - - - 0.05 54.1 6.47 6.95 88.8 D
- Ejemplo comp. 3 Comp example 3
- 2 % de Ni-Fe PVA 3,5 - - - - 3,38 9,3 6,14 6,54 83,6 D 2% Ni-Fe PVA 3.5 - - - - 3.38 9.3 6.14 6.54 83.6 D
- Ejemplo comp. 4 Comp example 4
- 2 % de Ni-Fe PVA 0,8 - - - - 0,79 16,3 6,27 7,10 90,7 D 2% Ni-Fe PVA 0.8 - - - - 0.79 16.3 6.27 7.10 90.7 D
- Ejemplo comp. 5 Comp example 5
- 2 % de Ni-Fe PVP 0,8 Glicerina 0,05 Derivado dealquilamina 0,1 0,94 15,4 6,25 7,06 90,2 D 2% Ni-Fe PVP 0.8 Glycerin 0.05 Dealkylamine derivative 0.1 0.94 15.4 6.25 7.06 90.2 D
- Ejemplo comp. 6 Comp example 6
- SUS316L PVA 0,8 - - - - 0,79 18,7 - 7,32 91,7 C SUS316L PVA 0.8 - - - - 0.79 18.7 - 7.32 91.7 C
17 17
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2010043027A JP5544928B2 (en) | 2010-02-26 | 2010-02-26 | Granulated powder and method for producing granulated powder |
JP2010043027 | 2010-02-26 |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2526141T3 true ES2526141T3 (en) | 2015-01-07 |
Family
ID=44170583
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES11155966.2T Active ES2526141T3 (en) | 2010-02-26 | 2011-02-25 | Granulated powder and process for producing granulated powder |
Country Status (5)
Country | Link |
---|---|
US (1) | US20110209575A1 (en) |
EP (1) | EP2364798B1 (en) |
JP (1) | JP5544928B2 (en) |
CN (1) | CN102166648B (en) |
ES (1) | ES2526141T3 (en) |
Families Citing this family (19)
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KR101198619B1 (en) * | 2011-11-11 | 2012-11-07 | 주식회사 신승 | Method for Manufacturing of briquettes using coal and finecoal |
US20140374663A1 (en) * | 2012-01-19 | 2014-12-25 | Yissum Research Development Company Of The Hebrew University Of Jerusalem Ltd. | Metals doped with organic material |
TWI522192B (en) * | 2012-07-31 | 2016-02-21 | 台耀科技股份有限公司 | Method of producing pressed-and-sintered workpiece and workpiece thereof |
CN102814500B (en) * | 2012-08-09 | 2014-04-09 | 山东鼎成新材料有限公司 | Method for manufacturing high-density product with stainless steel powder |
DE102012216052A1 (en) | 2012-09-11 | 2014-04-10 | Robert Bosch Gmbh | Sintered pressing part and method for producing such |
US9475945B2 (en) | 2013-10-03 | 2016-10-25 | Kennametal Inc. | Aqueous slurry for making a powder of hard material |
JP6273869B2 (en) * | 2014-01-31 | 2018-02-07 | セイコーエプソン株式会社 | Method for manufacturing molded body and method for manufacturing structure |
JP6311615B2 (en) * | 2015-01-05 | 2018-04-18 | セイコーエプソン株式会社 | Metal powder for powder metallurgy, compound, granulated powder and sintered body |
JPWO2016199576A1 (en) * | 2015-06-08 | 2018-03-22 | 住友電気工業株式会社 | Granulated powder and method for producing granulated powder |
CN105149601A (en) * | 2015-09-29 | 2015-12-16 | 四川有色金源粉冶材料有限公司 | Manufacturing method for high-gravity alloy feed |
DE102017202497A1 (en) | 2017-02-16 | 2018-08-16 | Robert Bosch Gmbh | Method for press-sintering steel components, press-sintered steel component itself and use of a special steel powder as a starting material for the production thereof |
JP6919229B2 (en) * | 2017-02-28 | 2021-08-18 | セイコーエプソン株式会社 | Composition for manufacturing three-dimensional modeled object and manufacturing method of three-dimensional modeled object |
JP7159172B2 (en) * | 2017-04-28 | 2022-10-24 | ヒューレット-パッカード デベロップメント カンパニー エル.ピー. | metallic building material granules |
CN111741824A (en) * | 2018-02-21 | 2020-10-02 | 杰富意钢铁株式会社 | Mixed powder for powder metallurgy |
CN110627490B (en) * | 2019-10-25 | 2022-02-01 | 中冶武汉冶金建筑研究院有限公司 | Preparation method and application of environment-friendly self-flow aluminum-silicon refractory injection molding material |
CN111069589B (en) * | 2019-12-23 | 2022-05-24 | 东睦新材料集团股份有限公司 | Preparation method of granulation powder for aluminum alloy, aluminum alloy and preparation method of aluminum alloy |
CN112044356A (en) * | 2020-09-16 | 2020-12-08 | 无锡斯贝尔磁性材料有限公司 | Spray tower capable of remarkably improving utilization rate of MnZn ferrite powder and application method thereof |
CN112719262B (en) * | 2020-12-29 | 2022-10-25 | 上海富驰高科技股份有限公司 | Tungsten alloy granulating material for high-speed pressing and preparation method thereof |
CN113427001A (en) * | 2021-06-22 | 2021-09-24 | 上海森永工程设备有限公司 | Method for preparing porous sintered body and porous sintered body |
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US4277288A (en) * | 1978-10-06 | 1981-07-07 | Ciba-Geigy Corporation | Fluidized granulation of pigments using organic granulating assistant |
SE427434B (en) * | 1980-03-06 | 1983-04-11 | Hoeganaes Ab | IRON-BASED POWDER MIXED WITH ADDITION TO MIXTURE AND / OR DAMAGE |
DE3048086A1 (en) * | 1980-12-19 | 1982-07-15 | Bayer Ag, 5090 Leverkusen | AGGLOMERED FERROMAGNETIC IRON PARTICLES |
JPH03165827A (en) * | 1989-11-24 | 1991-07-17 | Asuku:Kk | Method for granulating inorganic powder |
JPH04222627A (en) * | 1990-12-21 | 1992-08-12 | Powrex:Kk | Granulation method using stirring type tumbling and fluidizing apparatus |
DE69429326T2 (en) * | 1993-12-27 | 2002-05-16 | Sumitomo Spec Metals | Process for granulating powder |
US5575830A (en) * | 1994-12-21 | 1996-11-19 | Sumitomo Special Metals Co., Ltd. | Fabrication methods and equipment for granulated powders |
JPH08107034A (en) * | 1994-09-14 | 1996-04-23 | Sumitomo Special Metals Co Ltd | Manufacture of r-fe-b sintered permanent magnet |
JP2002294308A (en) * | 2001-03-30 | 2002-10-09 | Daido Steel Co Ltd | Granulated powder, sintered compact, and their manufacturing method |
JP3952006B2 (en) | 2003-11-26 | 2007-08-01 | セイコーエプソン株式会社 | Raw material powder for sintering or granulated powder for sintering and sintered body thereof |
JP2006206944A (en) * | 2005-01-26 | 2006-08-10 | Seiko Epson Corp | Method for producing granulated powder and granulated powder |
JP2007231396A (en) * | 2006-03-03 | 2007-09-13 | Tdk Corp | Method for producing granule and method for producing rare earth sintered magnet |
CN101346780B (en) * | 2006-05-18 | 2012-02-08 | 日立金属株式会社 | R-Fe-B porous magnet and method for producing the same |
JP4880491B2 (en) * | 2007-02-05 | 2012-02-22 | 日立粉末冶金株式会社 | Granulated powder for mold forming, method for producing the same, and method for producing sintered parts using the granulated powder |
JP5320843B2 (en) * | 2008-06-18 | 2013-10-23 | セイコーエプソン株式会社 | Compound for metal powder injection molding and method for producing sintered body |
-
2010
- 2010-02-26 JP JP2010043027A patent/JP5544928B2/en active Active
-
2011
- 2011-02-24 CN CN201110045491.8A patent/CN102166648B/en active Active
- 2011-02-25 EP EP11155966.2A patent/EP2364798B1/en active Active
- 2011-02-25 ES ES11155966.2T patent/ES2526141T3/en active Active
- 2011-02-28 US US13/036,133 patent/US20110209575A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
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JP2011179051A (en) | 2011-09-15 |
EP2364798B1 (en) | 2014-10-08 |
EP2364798A1 (en) | 2011-09-14 |
CN102166648B (en) | 2016-01-13 |
JP5544928B2 (en) | 2014-07-09 |
CN102166648A (en) | 2011-08-31 |
US20110209575A1 (en) | 2011-09-01 |
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