ES250664A1 - Chemical procedure for the obtaining of new steroid compounds of the pregnan series (Machine-translation by Google Translate, not legally binding)
- Google Patents
Chemical procedure for the obtaining of new steroid compounds of the pregnan series (Machine-translation by Google Translate, not legally binding)
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Merck and Co Inc
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Merck and Co Inc
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Publication of ES250664A1publicationCriticalpatent/ES250664A1/en
Chemical procedure for obtaining new steroid compounds of the pregnane series, especially to prepare a Δ 4-11-oxide-6 α -fluoro-19 α -methyl-pregnen-17 α, 21-diol-3.20- dione, which comprises treating a Δ 5 -11-oxide-17-20,20-21-bismethylenedioxy-16 α -methyl-3-ethylenedioxy-pregnene with a peracid, to produce an 11-oxido-17-20.20 -21-bismethylenedioxy-5 α, 6 α -epoxy-16 α -methyl-3-ethylenedioxy-pregnane; reacting the latter substance with hydrogen fluoride, to form an 11-oxide-17,20,20-21-bismethylenedioxy-5 α -hydroxy-6 β -fluoro-16 α -methyl-3-ethylenedioxy-pregnane; treat this material with an acid, to form a " 4-11-oxide-17-20,20-21-bismethylenedioxy-6 β -fluoro-16 α -methyl-prognen-3-one; and placing the latter steroid in succession in contact with aqueous formic acid and a dry mineral acid, to produce 11-oxido-6 α -fluoro-16 α -methyl-pregnen-17 α, 21-diol-3,20-dione; electing the 11-oxidosubstitute of these steroids, of the class comprising ketone and hydroxyl groups. (Machine-translation by Google Translate, not legally binding)
ES0250664A1958-07-071959-07-01Chemical procedure for the obtaining of new steroid compounds of the pregnan series (Machine-translation by Google Translate, not legally binding)
ExpiredES250664A1
(en)