ES2385768T3 - Procedimiento para la obtención de un producto sólido granulado y estable al almacenaje que contiene esencialmente ácido alfa-alanin-N,N-diacético y/o uno o varios derivados de ácido alfa-alanin-N,N-diacético - Google Patents
Procedimiento para la obtención de un producto sólido granulado y estable al almacenaje que contiene esencialmente ácido alfa-alanin-N,N-diacético y/o uno o varios derivados de ácido alfa-alanin-N,N-diacético Download PDFInfo
- Publication number
- ES2385768T3 ES2385768T3 ES08774531T ES08774531T ES2385768T3 ES 2385768 T3 ES2385768 T3 ES 2385768T3 ES 08774531 T ES08774531 T ES 08774531T ES 08774531 T ES08774531 T ES 08774531T ES 2385768 T3 ES2385768 T3 ES 2385768T3
- Authority
- ES
- Spain
- Prior art keywords
- diacetic acid
- alanin
- derivatives
- alanine
- polyethylene glycol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000000034 method Methods 0.000 title claims abstract description 24
- 239000007787 solid Substances 0.000 title claims abstract description 11
- 238000003860 storage Methods 0.000 title claims abstract description 9
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 29
- 239000000843 powder Substances 0.000 claims abstract description 27
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 26
- 206010039509 Scab Diseases 0.000 claims abstract description 16
- 239000002253 acid Substances 0.000 claims abstract description 9
- 238000002844 melting Methods 0.000 claims abstract description 8
- 230000008018 melting Effects 0.000 claims abstract description 8
- 238000007873 sieving Methods 0.000 claims abstract description 7
- 238000004851 dishwashing Methods 0.000 claims description 9
- 238000003825 pressing Methods 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 6
- QNAYBMKLOCPYGJ-REOHCLBHSA-N L-alanine Chemical class C[C@H](N)C(O)=O QNAYBMKLOCPYGJ-REOHCLBHSA-N 0.000 claims description 5
- 239000000654 additive Substances 0.000 claims description 5
- 229920002266 Pluriol® Polymers 0.000 description 13
- 239000003795 chemical substances by application Substances 0.000 description 11
- 239000000047 product Substances 0.000 description 9
- 239000008187 granular material Substances 0.000 description 8
- 238000009434 installation Methods 0.000 description 5
- 238000005056 compaction Methods 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 238000005194 fractionation Methods 0.000 description 3
- 238000011068 loading method Methods 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 150000002978 peroxides Chemical class 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 238000004026 adhesive bonding Methods 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/44—Stabilisation; Use of additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/22—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by pressing in moulds or between rollers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/30—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic using agents to prevent the granules sticking together; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0047—Detergents in the form of bars or tablets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/3245—Aminoacids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP07111575 | 2007-07-03 | ||
| EP07111575 | 2007-07-03 | ||
| PCT/EP2008/058377 WO2009003979A1 (de) | 2007-07-03 | 2008-06-30 | Verfahren zur herstellung eines rieselfähigen und lagerstabilen feststoffes enthaltend im wesentlichen alpha-alanin-n,n-diessigsäure und/oder ein oder mehrere derivate der alpha-alanin-n,n-diessigsäure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2385768T3 true ES2385768T3 (es) | 2012-07-31 |
Family
ID=39711111
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES08774531T Active ES2385768T3 (es) | 2007-07-03 | 2008-06-30 | Procedimiento para la obtención de un producto sólido granulado y estable al almacenaje que contiene esencialmente ácido alfa-alanin-N,N-diacético y/o uno o varios derivados de ácido alfa-alanin-N,N-diacético |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US20100187724A1 (enExample) |
| EP (1) | EP2175975B1 (enExample) |
| JP (1) | JP5328781B2 (enExample) |
| KR (1) | KR101520121B1 (enExample) |
| CN (1) | CN101687156B (enExample) |
| BR (1) | BRPI0813968A2 (enExample) |
| CA (1) | CA2690332C (enExample) |
| ES (1) | ES2385768T3 (enExample) |
| MX (1) | MX2009013320A (enExample) |
| PL (1) | PL2175975T3 (enExample) |
| WO (1) | WO2009003979A1 (enExample) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010133617A1 (de) | 2009-05-20 | 2010-11-25 | Basf Se | Verfahren zur herstellung eines sprühpulvers enthaltend ein oder mehrere glycin-n,n-diessigsäure-derivate und verwendung des sprühpulvers zur herstellung von pressagglomeraten |
| DE102009038951A1 (de) * | 2009-08-26 | 2011-03-03 | Inprotec Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| CA2938467C (en) | 2014-02-13 | 2022-06-28 | Basf Se | Powder and granule, process for making such powder and granule, and use thereof |
| CN106831466B (zh) * | 2016-12-28 | 2018-05-22 | 安徽省虹升生物股份有限公司 | 一种β-丙氨酸的常规储存方法 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1275019A (en) * | 1985-10-09 | 1990-10-09 | The Procter & Gamble Company | Granular detergent compositions having improved solubility |
| US5100592A (en) * | 1986-03-12 | 1992-03-31 | Washington University Technology Associated, Inc. | Method and apparatus for granulation and granulated product |
| DE4444347A1 (de) * | 1994-12-14 | 1996-06-20 | Basf Ag | Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen bei der Förderung und beim Transport von Erdöl und Erdgas |
| EP0783034B1 (en) * | 1995-12-22 | 2010-08-18 | Mitsubishi Rayon Co., Ltd. | Chelating agent and detergent comprising the same |
| DE19649681A1 (de) * | 1996-11-29 | 1998-06-04 | Basf Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| JP2929276B2 (ja) * | 1996-12-18 | 1999-08-03 | 花王株式会社 | ノニオン洗剤粒子の製造方法 |
| DE19709411A1 (de) * | 1997-03-07 | 1998-09-10 | Henkel Kgaa | Waschmittelformkörper |
| DE19937345A1 (de) * | 1999-08-11 | 2001-02-15 | Basf Ag | Mischpulver oder Mischgranulat auf Basis von Glycin-N,N-diessigsäure |
| DE10137925A1 (de) * | 2001-08-07 | 2003-02-20 | Cognis Deutschland Gmbh | Geminitenside und Polyethylenglycol |
| DE10238302A1 (de) * | 2002-08-21 | 2004-02-26 | BSH Bosch und Siemens Hausgeräte GmbH | Verfahren zum Anpassen eines Spülprogramms in einer Geschirrspülmaschine und Geschirrspülmaschine |
| JP2004204055A (ja) * | 2002-12-25 | 2004-07-22 | Adeka Clean Aid Co Ltd | 洗浄剤組成物 |
| DE102004003286A1 (de) * | 2004-01-22 | 2005-09-29 | Henkel Kgaa | System zur Wasserenthärtung durch Fällenthärtung |
| DE102004032320A1 (de) * | 2004-07-02 | 2006-01-19 | Basf Ag | Mischpulver oder Mischgranulat auf Basis von MGDA |
| DE102005041347A1 (de) * | 2005-08-31 | 2007-03-01 | Basf Ag | Reinigungsformulierungen für die maschinelle Geschirrreinigung enthaltend hydrophil modifizierte Polycarboxylate |
| ES2427152T3 (es) * | 2006-04-20 | 2013-10-29 | The Procter & Gamble Company | Procedimiento para producir partículas blanqueadoras |
| US9227915B2 (en) * | 2011-05-03 | 2016-01-05 | Basf Se | Process for the preparation of a crystalline L-MGDA trialkali metal salt |
-
2008
- 2008-06-30 JP JP2010513956A patent/JP5328781B2/ja not_active Expired - Fee Related
- 2008-06-30 BR BRPI0813968-7A patent/BRPI0813968A2/pt active Search and Examination
- 2008-06-30 ES ES08774531T patent/ES2385768T3/es active Active
- 2008-06-30 PL PL08774531T patent/PL2175975T3/pl unknown
- 2008-06-30 WO PCT/EP2008/058377 patent/WO2009003979A1/de not_active Ceased
- 2008-06-30 MX MX2009013320A patent/MX2009013320A/es active IP Right Grant
- 2008-06-30 KR KR1020107002428A patent/KR101520121B1/ko not_active Expired - Fee Related
- 2008-06-30 CA CA2690332A patent/CA2690332C/en not_active Expired - Fee Related
- 2008-06-30 CN CN2008800228858A patent/CN101687156B/zh not_active Expired - Fee Related
- 2008-06-30 EP EP08774531A patent/EP2175975B1/de not_active Not-in-force
- 2008-06-30 US US12/667,051 patent/US20100187724A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| JP5328781B2 (ja) | 2013-10-30 |
| BRPI0813968A2 (pt) | 2015-07-14 |
| CA2690332A1 (en) | 2009-01-08 |
| EP2175975A1 (de) | 2010-04-21 |
| CA2690332C (en) | 2015-04-21 |
| JP2010531847A (ja) | 2010-09-30 |
| WO2009003979A1 (de) | 2009-01-08 |
| CN101687156B (zh) | 2013-08-07 |
| KR20100057783A (ko) | 2010-06-01 |
| US20100187724A1 (en) | 2010-07-29 |
| PL2175975T3 (pl) | 2012-11-30 |
| KR101520121B1 (ko) | 2015-05-18 |
| EP2175975B1 (de) | 2012-06-20 |
| MX2009013320A (es) | 2010-01-20 |
| CN101687156A (zh) | 2010-03-31 |
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