ES2329645T1 - Procedimiento para producir carbonilos de hodge y lignina oligomerica. - Google Patents

Procedimiento para producir carbonilos de hodge y lignina oligomerica. Download PDF

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Publication number
ES2329645T1
ES2329645T1 ES08164013T ES08164013T ES2329645T1 ES 2329645 T1 ES2329645 T1 ES 2329645T1 ES 08164013 T ES08164013 T ES 08164013T ES 08164013 T ES08164013 T ES 08164013T ES 2329645 T1 ES2329645 T1 ES 2329645T1
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Spain
Prior art keywords
oligomeric
lignin
product
hodge
carbonyls
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ES08164013T
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ES2329645T3 (es
Inventor
Jan Piskorz
Piotr Majerski
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B53/00—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form
    • C10B53/02—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form of cellulose-containing material
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00—Other inorganic fertilisers
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00—Fertilisers characterised by their form
    • C05G5/30—Layered or coated, e.g. dust-preventing coatings
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B51/00—Destructive distillation of solid carbonaceous materials by combined direct and indirect heating
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10C—WORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
    • C10C5/00—Production of pyroligneous acid distillation of wood, dry distillation of organic waste
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10J—PRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J3/00—Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K1/00—Purifying combustible gases containing carbon monoxide
    • C10K1/02—Dust removal
    • C10K1/026—Dust removal by centrifugal forces
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10K—PURIFYING OR MODIFYING THE CHEMICAL COMPOSITION OF COMBUSTIBLE GASES CONTAINING CARBON MONOXIDE
    • C10K1/00—Purifying combustible gases containing carbon monoxide
    • C10K1/08—Purifying combustible gases containing carbon monoxide by washing with liquids; Reviving the used wash liquors
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L5/00—Solid fuels
    • C10L5/40—Solid fuels essentially based on materials of non-mineral origin
    • C10L5/44—Solid fuels essentially based on materials of non-mineral origin on vegetable substances
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/141—Feedstock
    • Y02P20/145—Feedstock the feedstock being materials of biological origin
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Combustion & Propulsion (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Pest Control & Pesticides (AREA)
  • Inorganic Chemistry (AREA)
  • Fertilizers (AREA)
  • Processing Of Solid Wastes (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

Un procedimiento de tratamiento de alimentación de biomasa que comprende: pirolizar rápidamente alimentación de biomasa en presencia de vapor supercalentado a una temperatura seleccionada para producir al menos una corriente de producto.

Claims (21)

1. Un procedimiento de tratamiento de alimentación de biomasa que comprende: pirolizar rápidamente alimentación de biomasa en presencia de vapor supercalentado a una temperatura seleccionada para producir al menos una corriente de producto.
2. El procedimiento de la reivindicación 1, en el que la corriente de producto incluye carbonilos de Hodge, lignina oligomérica y partículas de biocarbón.
3. El procedimiento de la reivindicación 1, en el que la primera corriente de producto incluye una suspensión densa acuosa de partículas de carbón vegetal producidas y lignina oligomérica.
4. El procedimiento de la reivindicación 1, en el que los carbonilos de Hodge son carbonilos hidrosolubles originados por carbohidratos.
5. El procedimiento de la reivindicación 1, en el que la temperatura supera los 400ºC.
6. El procedimiento de la reivindicación 4, en el que los carbonilos de Hodge incluyen al menos uno de hidroxiacetaldehído, gliceraldehídos, acetol, piruvaldehído, glioxal, 5-hidroximetilfurfural, furfurales y formaldehído.
7. El procedimiento de la reivindicación 1, en el que la alimentación de biomasa es celulosas de bajo contenido en lignina.
8. El procedimiento de la reivindicación 7, en el que la temperatura está en el intervalo de 490ºC a 590ºC.
9. El procedimiento de la reivindicación 7, en el que las celulosas se seleccionan del grupo constituido por pulpas y cienos de celulosa y polvos de celulosa microcristalina.
10. El procedimiento de la reivindicación 7, en el que la corriente de producto es una mezcla hidrosoluble de los carbonilos de Hodge con hidroxiacetaldehído, glioxal, metilglioxal, formaldehído, acetol, furfurales y 5-hidroximetilfurfurales.
11. El procedimiento de la reivindicación 1, en el que la alimentación de biomasa es lignocelulosas.
12. El procedimiento de la reivindicación 11, en el que la temperatura está en el intervalo comprendido entre 430 y 550ºC.
13. El procedimiento de la reivindicación 11, en el que las lignocelulosas se seleccionan de biomasa forestal y producida por la agricultura incluyendo desechos y residuos.
14. El procedimiento de la reivindicación 11, en el que se produce una corriente de producto de lignina oligomérica.
15. El procedimiento de la reivindicación 11, en el que la segunda corriente de producto es una mezcla soluble de carbonilos de Hodge con hidroxiacetaldehído, glioxal, metilglioxal, formaldehído, acetol, furfurales y 5-HMF e incluye ácidos fórmico y acético y fenoles hidrosolubles.
16. El procedimiento de la reivindicación 1, en el que la lignina oligomérica y el biocarbón se combinan físicamente.
17. El procedimiento de la reivindicación 16, en el que dicho carbón vegetal tiene un alto contenido en grupos funcionales oxigenados y funciona no sólo como absorbente, sino que también se une a nitrógeno directamente mediante reacción con grupos NH2.
18. Un producto de la pirólisis rápida de alimentación de biomasa, que comprende carbón vegetal combinado con lignina oligomérica.
19. Un producto de la pirólisis rápida de la alimentación de biomasa, que comprende lignina oligomérica y lignina oligomérica en combinación con biocarbón para formar un potenciador del suelo.
20. Un producto de la pirólisis rápida de la alimentación de biomasa, que comprende lignina oligomérica en estado fundido que recubre fertilizantes de N, P, K, convirtiéndolos en un tipo de fertilizante de liberación lenta o controlable.
21. El producto de la reivindicación 20, que incluye biocarbón y se describe por las 4 letras N, P, K y C.
ES08164013T 2007-11-20 2008-09-10 Método para mejorar el suelo Active ES2329645T3 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US943422 2007-11-20
US11/943,422 US8436120B2 (en) 2007-11-20 2007-11-20 Method of producing hodge carbonyls and oligomeric lignin

Publications (2)

Publication Number Publication Date
ES2329645T1 true ES2329645T1 (es) 2009-11-30
ES2329645T3 ES2329645T3 (es) 2019-12-12

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US (1) US8436120B2 (es)
EP (1) EP2072600B1 (es)
CN (1) CN101440026B (es)
BR (1) BRPI0804974B1 (es)
CA (1) CA2639022C (es)
DE (1) DE08164013T1 (es)
DK (1) DK2072600T3 (es)
ES (1) ES2329645T3 (es)
PL (1) PL2072600T3 (es)

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CA2639022A1 (en) 2009-05-20
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US8436120B2 (en) 2013-05-07
CN101440026B (zh) 2016-08-03
BRPI0804974A2 (pt) 2010-05-04
CA2639022C (en) 2014-07-15
BRPI0804974B1 (pt) 2017-09-12
EP2072600A3 (en) 2011-03-23
DE08164013T1 (de) 2010-01-21
EP2072600A2 (en) 2009-06-24
US20090126433A1 (en) 2009-05-21
CN101440026A (zh) 2009-05-27
ES2329645T3 (es) 2019-12-12
DK2072600T3 (da) 2019-08-19

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