ES2125818A1 - Procedimiento de obtencion de cristales liquidos colestericos por recristalizacion estereoselectiva. - Google Patents

Procedimiento de obtencion de cristales liquidos colestericos por recristalizacion estereoselectiva.

Info

Publication number
ES2125818A1
ES2125818A1 ES09700100A ES9700100A ES2125818A1 ES 2125818 A1 ES2125818 A1 ES 2125818A1 ES 09700100 A ES09700100 A ES 09700100A ES 9700100 A ES9700100 A ES 9700100A ES 2125818 A1 ES2125818 A1 ES 2125818A1
Authority
ES
Spain
Prior art keywords
stereoselective
recrystallization
cholesteric liquid
toluene
liquid crystals
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
ES09700100A
Other languages
English (en)
Other versions
ES2125818B1 (es
Inventor
Maria Mercedes Perez-Mendez
Rocha Carlos Marco
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Consejo Superior de Investigaciones Cientificas CSIC
Original Assignee
Consejo Superior de Investigaciones Cientificas CSIC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to ES009700100A priority Critical patent/ES2125818B1/es
Application filed by Consejo Superior de Investigaciones Cientificas CSIC filed Critical Consejo Superior de Investigaciones Cientificas CSIC
Priority to EP98900283A priority patent/EP1004650B1/en
Priority to US09/341,907 priority patent/US6165382A/en
Priority to AT98900283T priority patent/ATE267860T1/de
Priority to AU54863/98A priority patent/AU739076B2/en
Priority to JP53379698A priority patent/JP2001513827A/ja
Priority to CA002278568A priority patent/CA2278568A1/en
Priority to PCT/ES1998/000006 priority patent/WO1998031771A1/es
Priority to DE69824182T priority patent/DE69824182D1/de
Publication of ES2125818A1 publication Critical patent/ES2125818A1/es
Application granted granted Critical
Publication of ES2125818B1 publication Critical patent/ES2125818B1/es
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K19/00—Liquid crystal materials
    • C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
    • C09K19/38—Polymers
    • C09K19/3804—Polymers with mesogenic groups in the main chain
    • C09K19/3809—Polyesters; Polyester derivatives, e.g. polyamides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/60—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from the reaction of a mixture of hydroxy carboxylic acids, polycarboxylic acids and polyhydroxy compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Liquid Crystal Substances (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
  • Liquid Crystal (AREA)
  • Steroid Compounds (AREA)

Abstract

Procedimiento de obtención de cristales líquidos colestéricos por recristalización estereoselectiva. Procedimiento mediante el cual se sintetiza los polímeros, el PTOBEE (C{sub,26 H{sub,20 O{sub,8 ){sub,n y el PTOBDME (C{sub,34 H{sub,36 O{sub,8 ){sub,n , con la adición de dicloruro de ácido y DL-treo-1,2-butanodiol en Cl-naftaleno y DL-1,2-dodecandiol con óxido de difenilo, respectivamente, pasándolos por una corriente de nitrógeno a temperatura ambiente, calentando la mezcla, decantando en tolueno la mezcla y filtrando. En el tolueno resultante de decantar el polímero precipita el enantiómero (-)PTOBEE. Los compuestos obtenidos tienen naturaleza de cristal líquido colestérico, obtenidos por recristalización estereoselectiva en tolueno.
ES009700100A 1997-01-20 1997-01-20 Procedimiento de obtencion de cristales liquidos colestericos por recristalizacion estereoselectiva. Expired - Fee Related ES2125818B1 (es)

Priority Applications (9)

Application Number Priority Date Filing Date Title
ES009700100A ES2125818B1 (es) 1997-01-20 1997-01-20 Procedimiento de obtencion de cristales liquidos colestericos por recristalizacion estereoselectiva.
US09/341,907 US6165382A (en) 1997-01-20 1998-01-16 Process for obtaining cholesteric liquid crystals by stereoselective recrystallization
AT98900283T ATE267860T1 (de) 1997-01-20 1998-01-16 Verfahren zur herstellung von cholesterischem flüssigkristall durch stereoselektive rekristallisiering
AU54863/98A AU739076B2 (en) 1997-01-20 1998-01-16 Process for obtaining cholesteric liquid crystals by stereoselective recrystallization
EP98900283A EP1004650B1 (en) 1997-01-20 1998-01-16 Process for obtaining cholesteric liquid crystals by stereoselective recrystallization
JP53379698A JP2001513827A (ja) 1997-01-20 1998-01-16 立体選択的再結晶によるコレステリン性液晶を得る方法
CA002278568A CA2278568A1 (en) 1997-01-20 1998-01-16 Process for obtaining cholesteric liquid crystals by stereoselective recrystallization
PCT/ES1998/000006 WO1998031771A1 (es) 1997-01-20 1998-01-16 Procedimiento de obtencion de cristales liquidos colestericos por recristalizacion estereoselectiva
DE69824182T DE69824182D1 (de) 1997-01-20 1998-01-16 Verfahren zur herstellung von cholesterischem flüssigkristall durch stereoselektive rekristallisiering

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ES009700100A ES2125818B1 (es) 1997-01-20 1997-01-20 Procedimiento de obtencion de cristales liquidos colestericos por recristalizacion estereoselectiva.

Publications (2)

Publication Number Publication Date
ES2125818A1 true ES2125818A1 (es) 1999-03-01
ES2125818B1 ES2125818B1 (es) 2000-02-16

Family

ID=8297923

Family Applications (1)

Application Number Title Priority Date Filing Date
ES009700100A Expired - Fee Related ES2125818B1 (es) 1997-01-20 1997-01-20 Procedimiento de obtencion de cristales liquidos colestericos por recristalizacion estereoselectiva.

Country Status (9)

Country Link
US (1) US6165382A (es)
EP (1) EP1004650B1 (es)
JP (1) JP2001513827A (es)
AT (1) ATE267860T1 (es)
AU (1) AU739076B2 (es)
CA (1) CA2278568A1 (es)
DE (1) DE69824182D1 (es)
ES (1) ES2125818B1 (es)
WO (1) WO1998031771A1 (es)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
USD787945S1 (en) 2014-06-03 2017-05-30 Seventh Generation Ventures, Inc. Bottle
USD742175S1 (en) 2014-06-03 2015-11-03 Seventh Generation Ventures, Inc. Bottle
USD796261S1 (en) 2015-02-13 2017-09-05 Seventh Generation Ventures, Inc. Bottle
USD753791S1 (en) 2015-02-13 2016-04-12 Seventh Generation Ventures, Inc. Bottle top with filter
USD789745S1 (en) 2015-02-13 2017-06-20 Seventh Generation Ventures, Inc. Bottle
USD794392S1 (en) 2015-02-13 2017-08-15 Seventh Generation Ventures, Inc. Bottle
USD823061S1 (en) 2016-08-19 2018-07-17 O2C Raleigh, Llc Bottle with closure
USD812966S1 (en) 2016-08-19 2018-03-20 O2C Raleigh, Llc Cap for a container
USD878572S1 (en) 2017-11-09 2020-03-17 Neomed, Inc. Collection and feeding bottle
USD878571S1 (en) 2017-11-09 2020-03-17 Neomed, Inc. Collection and feeding bottle

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0218369A1 (en) * 1985-09-04 1987-04-15 Nippon Oil Co. Ltd. Cholesteric liquid crystal copolyesters
EP0251688A2 (en) * 1986-06-26 1988-01-07 Nippon Oil Co. Ltd. Cholesteric liquid crystal polyesters

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4412059A (en) * 1980-08-20 1983-10-25 Duke University High modulus cholesteric mesophase polymers
EP0737707B1 (en) * 1995-04-12 2005-09-28 Sumitomo Chemical Company, Limited Liquid crystal polyester resin composition film
DE19718293A1 (de) * 1997-04-30 1999-03-18 Consortium Elektrochem Ind Verfahren zur Herstellung von dreidimensional vernetzten polymeren Materialien mit breiten cholesterischen Reflexionsbanden und nach diesem Verfahren hergestellte Filter, Reflektoren und Polarisatoren

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0218369A1 (en) * 1985-09-04 1987-04-15 Nippon Oil Co. Ltd. Cholesteric liquid crystal copolyesters
EP0251688A2 (en) * 1986-06-26 1988-01-07 Nippon Oil Co. Ltd. Cholesteric liquid crystal polyesters

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
MOL. CRYST. LIQ. CRYST., 1990, Vol. 179, paginas 405-418. E. CHIELLINI et al. "Chiral Lyquid-Crystalline Polymers. The effect of chiral spaces structure in thermotropic polyesters". *

Also Published As

Publication number Publication date
JP2001513827A (ja) 2001-09-04
DE69824182D1 (de) 2004-07-01
AU739076B2 (en) 2001-10-04
ES2125818B1 (es) 2000-02-16
EP1004650A1 (en) 2000-05-31
CA2278568A1 (en) 1998-07-23
EP1004650B1 (en) 2004-05-26
ATE267860T1 (de) 2004-06-15
WO1998031771A1 (es) 1998-07-23
US6165382A (en) 2000-12-26
AU5486398A (en) 1998-08-07

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