ES2083711T3 - Procedimiento y aparato para la produccion mixta de oxigeno de alta y baja pureza. - Google Patents

Procedimiento y aparato para la produccion mixta de oxigeno de alta y baja pureza.

Info

Publication number
ES2083711T3
ES2083711T3 ES92402798T ES92402798T ES2083711T3 ES 2083711 T3 ES2083711 T3 ES 2083711T3 ES 92402798 T ES92402798 T ES 92402798T ES 92402798 T ES92402798 T ES 92402798T ES 2083711 T3 ES2083711 T3 ES 2083711T3
Authority
ES
Spain
Prior art keywords
current
pressure column
oxygen
fraction
rich
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES92402798T
Other languages
English (en)
Other versions
ES2083711T5 (es
Inventor
Bao Ha
Catherine Garnier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Liquid Air Engineering Corp Canada
Original Assignee
Liquid Air Engineering Corp Canada
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=25104476&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES2083711(T3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Liquid Air Engineering Corp Canada filed Critical Liquid Air Engineering Corp Canada
Publication of ES2083711T3 publication Critical patent/ES2083711T3/es
Application granted granted Critical
Publication of ES2083711T5 publication Critical patent/ES2083711T5/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
    • F25J3/0409—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/32—Other features of fractionating columns ; Constructional details of fractionating columns not provided for in groups B01D3/16 - B01D3/30
    • B01D3/322—Reboiler specifications
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04163—Hot end purification of the feed air
    • F25J3/04169—Hot end purification of the feed air by adsorption of the impurities
    • F25J3/04175—Hot end purification of the feed air by adsorption of the impurities at a pressure of substantially more than the highest pressure column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187—Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/04193—Division of the main heat exchange line in consecutive sections having different functions
    • F25J3/04206—Division of the main heat exchange line in consecutive sections having different functions including a so-called "auxiliary vaporiser" for vaporising and producing a gaseous product
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/0429—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of feed air, e.g. used as waste or product air or expanded into an auxiliary column
    • F25J3/04296—Claude expansion, i.e. expanded into the main or high pressure column
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04406—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
    • F25J3/04418—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system with thermally overlapping high and low pressure columns
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/50—Processes or apparatus using separation by rectification using multiple (re-)boiler-condensers at different heights of the column
    • F25J2200/54—Processes or apparatus using separation by rectification using multiple (re-)boiler-condensers at different heights of the column in the low pressure column of a double pressure main column system
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2215/00—Processes characterised by the type or other details of the product stream
    • F25J2215/50—Oxygen or special cases, e.g. isotope-mixtures or low purity O2
    • F25J2215/52—Oxygen production with multiple purity O2
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2250/00—Details related to the use of reboiler-condensers
    • F25J2250/30—External or auxiliary boiler-condenser in general, e.g. without a specified fluid or one fluid is not a primary air component or an intermediate fluid
    • F25J2250/40—One fluid being air
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2250/00—Details related to the use of reboiler-condensers
    • F25J2250/30—External or auxiliary boiler-condenser in general, e.g. without a specified fluid or one fluid is not a primary air component or an intermediate fluid
    • F25J2250/50—One fluid being oxygen
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S62/00—Refrigeration
    • Y10S62/923—Inert gas
    • Y10S62/924—Argon
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S62/00—Refrigeration
    • Y10S62/939—Partial feed stream expansion, air
    • Y10S62/94—High pressure column

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation By Low-Temperature Treatments (AREA)

Abstract

SE PRESENTA UN PROCESO PARA PRODUCIR SIMULTANEAMENTE OXIGENO TANTO DE ALTA COMO DE BAJA PUREZA, QUE COMPRENDE: A) EL PASO DE UNA CORRIENTE DE SUMINISTRO COMPRIMIDA Y REFRIGERADA (101) QUE CONTENGA AL MENOS OXIGENO Y NITROGENO A UN INTERCAMBIADOR PRINCIPAL (11), EN EL QUE LA CORRIENTE DE SUMINISTRO COMPRIMIDA Y REFRIGERADA SE DIVIDE EN DOS FRACCIONES (A) Y (B), B) LA EXPANSION DE LA PRIMERA FRACCION (A) (103) EN UN EXPANSOR (12) Y LA DIVISION DE LA MISMA EN DOS FRACCIONES ADICIONALES (I) Y (II), C) LA REFRIGERACION ADICIONAL DE LA SEGUNDA FRACCION (B) (104) EN EL INTERCAMBIADOR PRINCIPAL Y LA EXPANSION DE AL MENOS UNA FRACCION DE ESTA CORRIENTE MEDIANTE UNA VALVULA DE EXPANSION (130A) EN UNA COLUMNA DE ALTA PRESION (20) COMO CORRIENTE DE SUMINISTRO LIQUIDA, D) LA INTRODUCCION DE LA PRIMERA FRACCION (I) (106) EN EL INTERIOR DE UNA CALDERA DE EBULLICION (24) SITUADA EN EL FONDO DE LA COLUMNA DE BAJA PRESION (21), EN DONDE LA PRIMERA FRACCION DE LA CORRIENTE DE SUMINISTRO SE CONDENSA EN LA CALDERA SUMINISTRANDO UNA PRIMERA EBULLICION PARA LA DESTILACION, E) EL SUMINISTRO DE AL MENOS UNA FRACCION DE LA CORRIENTE DE SUMINISTRO LICUADA (110) A UNA COLUMNA DE ALTA PRESION O A UNA COLUMNA DE BAJA PRESION O A AMBAS COMO CORRIENTE DE SUMINISTRO, F) LA INTRODUCCION DE LA SEGUNDA FRACCION (II) (107) EN EL FONDO DE LA COLUMNA DE ALTA PRESION COMO SUMINISTRO GASEOSO, MEDIANTE LO CUAL SE FORMAN UNA CORRIENTE LIQUIDA RICA EN OXIGENO Y UNA CORRIENTE GASEOSA RICA EN NITROGENO QUE SE SITUA EN LA PARTE SUPERIOR, G) EL PASO DE LA CORRIENTE LIQUIDA RICA EN OXIGENO (108) A LA COLUMNA DE BAJA PRESION COMO CORRIENTE DE SUMINISTRO, H) LA CONDENSACION DE LA CORRIENTE GASEOSA RICA EN NITROGENO EN UN LIQUIDO EN EBULLICION EN LA CALDERA SUPERIOR (23) DE LA COLUMNA DE BAJA PRESION, SITUADA EN UNA ETAPA INTERMEDIA, MEDIANTE LO CUAL SIRVE COMO SEGUNDA CALDERA PARA LA DESTILACION, I) EL RETORNO DE UNA PARTE (115) DE LA CORRIENTE CONDENSADA RICA EN NITROGENO A LA COLUMNA DE ALTA PRESION COMO REFLUJO, Y EL PASODE AL MENOS UNA FRACCION DE LA PARTE RESTANTE (116) DE LA CORRIENTE RICA EN NITROGENO A LA PARTE SUPERIOR DE LA COLUMNA DE ALTA PRESION COMO REFLUJO, MEDIANTE LO CUAL LA COLUMNA DE BAJA PRESION SEPARA SU CORRIENTE DE SUMINISTRO EN UNA CORRIENTE DE OXIGENO Y UNA CORRIENTE SUPERIOR RICA EN NITROGENO, J) LA RECUPERACION DEL PRODUCTO DEL OXIGENO DE LA CORRIENTE DEL FONDO (188) COMO OXIGENO LIQUIDO DE ALTA PUREZA, K) LA EXTRACCION DE LA CORRIENTE DE OXIGENO DE BAJA PUREZA DE UNA CUBETA O DE UNA ETAPA QUE SE ENCUENTRA ENTRE LAS DOS CALDERAS DE LA COLUMNA DE BAJA PRESION, Y L) EL CALENTAMIENTO SUAVE EN EL INTERCAMBIADOR PRINCIPAL (11) DE LA CORRIENTE DE OXIGENO DE BAJA PUREZA Y DE LA CORRIENTE RICA EN NITROGENO.
ES92402798T 1991-10-15 1992-10-14 Procedimiento y aparato para la produccion mixta de oxigeno de alta y baja pureza. Expired - Lifetime ES2083711T5 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/775,453 US5315833A (en) 1991-10-15 1991-10-15 Process for the mixed production of high and low purity oxygen

Publications (2)

Publication Number Publication Date
ES2083711T3 true ES2083711T3 (es) 1996-04-16
ES2083711T5 ES2083711T5 (es) 1999-10-01

Family

ID=25104476

Family Applications (1)

Application Number Title Priority Date Filing Date
ES92402798T Expired - Lifetime ES2083711T5 (es) 1991-10-15 1992-10-14 Procedimiento y aparato para la produccion mixta de oxigeno de alta y baja pureza.

Country Status (4)

Country Link
US (3) US5315833A (es)
EP (1) EP0538117B2 (es)
DE (1) DE69208418T3 (es)
ES (1) ES2083711T5 (es)

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JP6159242B2 (ja) * 2013-12-13 2017-07-05 大陽日酸株式会社 空気分離方法及び装置
US20150323247A1 (en) * 2014-05-07 2015-11-12 Maulik R. Shelat Heat exchanger assembly and system for a cryogenic air separation unit
CN106989567A (zh) * 2017-04-25 2017-07-28 河南开元空分集团有限公司 一种低能耗的同时生产富氧气体和高纯氮气的装置和方法
CN110566302A (zh) * 2019-09-25 2019-12-13 昆山三一环保科技有限公司 一种低温余热回收系统的装置

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US5349824A (en) 1994-09-27
EP0538117B2 (en) 1999-07-21
DE69208418D1 (de) 1996-03-28
DE69208418T3 (de) 1999-09-23
EP0538117A1 (en) 1993-04-21
EP0538117B1 (en) 1996-02-21
US5396773A (en) 1995-03-14
ES2083711T5 (es) 1999-10-01
US5315833A (en) 1994-05-31
DE69208418T2 (de) 1996-07-04

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