EP3912209A4 - POLYCRYSTALLINE METAL OXIDES WITH ENRICHED GRAIN BOUNDARIES - Google Patents

POLYCRYSTALLINE METAL OXIDES WITH ENRICHED GRAIN BOUNDARIES Download PDF

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Publication number
EP3912209A4
EP3912209A4 EP19910735.0A EP19910735A EP3912209A4 EP 3912209 A4 EP3912209 A4 EP 3912209A4 EP 19910735 A EP19910735 A EP 19910735A EP 3912209 A4 EP3912209 A4 EP 3912209A4
Authority
EP
European Patent Office
Prior art keywords
metal oxides
polycrystalline metal
enriched grain
grain joints
joints
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
EP19910735.0A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP3912209A1 (en
Inventor
Adrian Pullen
David Ofer
Suresh Sriramulu
Kenan Sahin
Jane REMPEL
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CAMX Power LLC
Original Assignee
CAMX Power LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US16/250,622 external-priority patent/US10950857B2/en
Priority claimed from US16/250,615 external-priority patent/US10501335B1/en
Application filed by CAMX Power LLC filed Critical CAMX Power LLC
Publication of EP3912209A1 publication Critical patent/EP3912209A1/en
Publication of EP3912209A4 publication Critical patent/EP3912209A4/en
Pending legal-status Critical Current

Links

Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/40—Complex oxides containing nickel and at least one other metal element
    • C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/40—Complex oxides containing nickel and at least one other metal element
    • C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C01G53/44—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
    • C01G53/50—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO2)n-, e.g. Li(NixMn1-x)O2 or Li(MyNixMn1-x-y)O2
    • C01G53/502—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO2)n-, e.g. Li(NixMn1-x)O2 or Li(MyNixMn1-x-y)O2 containing lithium and cobalt
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/40—Complex oxides containing nickel and at least one other metal element
    • C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
    • C01G53/44—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
    • C01G53/50—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO2)n-, e.g. Li(NixMn1-x)O2 or Li(MyNixMn1-x-y)O2
    • C01G53/502—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO2)n-, e.g. Li(NixMn1-x)O2 or Li(MyNixMn1-x-y)O2 containing lithium and cobalt
    • C01G53/504—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO2)n-, e.g. Li(NixMn1-x)O2 or Li(MyNixMn1-x-y)O2 containing lithium and cobalt with the molar ratio of nickel with respect to all the metals other than alkali metals higher than or equal to 0.5, e.g. Li(MzNixCoyMn1-x-y-z)O2 with x ≥ 0.5
    • C01G53/506—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO2)n-, e.g. Li(NixMn1-x)O2 or Li(MyNixMn1-x-y)O2 containing lithium and cobalt with the molar ratio of nickel with respect to all the metals other than alkali metals higher than or equal to 0.5, e.g. Li(MzNixCoyMn1-x-y-z)O2 with x ≥ 0.5 with the molar ratio of nickel with respect to all the metals other than alkali metals higher than or equal to 0.8, e.g. Li(MzNixCoyMn1-x-y-z)O2 with x ≥ 0.8
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/362—Composites
    • H01M4/366—Composites as layered products
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/77—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by unit-cell parameters, atom positions or structure diagrams
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/85—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by XPS, EDX or EDAX data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/50—Agglomerated particles
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/40—Electric properties
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028—Positive electrodes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Composite Materials (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Secondary Cells (AREA)
EP19910735.0A 2019-01-17 2019-10-23 POLYCRYSTALLINE METAL OXIDES WITH ENRICHED GRAIN BOUNDARIES Pending EP3912209A4 (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US201916250762A 2019-01-17 2019-01-17
US16/250,622 US10950857B2 (en) 2019-01-17 2019-01-17 Polycrystalline metal oxides with enriched grain boundaries
US16/250,615 US10501335B1 (en) 2019-01-17 2019-01-17 Polycrystalline metal oxides with enriched grain boundaries
PCT/US2019/057630 WO2020149910A1 (en) 2019-01-17 2019-10-23 Polycrystalline metal oxides with enriched grain boundaries

Publications (2)

Publication Number Publication Date
EP3912209A1 EP3912209A1 (en) 2021-11-24
EP3912209A4 true EP3912209A4 (en) 2022-11-30

Family

ID=71613350

Family Applications (1)

Application Number Title Priority Date Filing Date
EP19910735.0A Pending EP3912209A4 (en) 2019-01-17 2019-10-23 POLYCRYSTALLINE METAL OXIDES WITH ENRICHED GRAIN BOUNDARIES

Country Status (6)

Country Link
EP (1) EP3912209A4 (enExample)
JP (2) JP7629403B2 (enExample)
KR (2) KR20210105440A (enExample)
CN (2) CN122000331A (enExample)
CA (1) CA3126058A1 (enExample)
WO (1) WO2020149910A1 (enExample)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114051487B (zh) * 2019-07-03 2024-03-22 尤米科尔公司 作为用于可再充电锂离子电池的正电极活性材料的锂镍锰钴复合氧化物
JP7652891B2 (ja) * 2020-11-10 2025-03-27 エルジー エナジー ソリューション リミテッド リチウム二次電池用正極活物質、その製造方法及びそれを含むリチウム二次電池
KR20220087953A (ko) * 2020-12-18 2022-06-27 주식회사 포스코 리튬 이차 전지용 양극 활물질, 이의 제조방법 및 이를 포함하는 리튬 이차 전지
KR102867394B1 (ko) 2021-12-21 2025-10-01 포스코홀딩스 주식회사 리튬 이차 전지용 양극 활물질, 이의 제조방법 및 이를 포함하는 리튬 이차 전지
KR20250142148A (ko) * 2024-03-21 2025-09-30 주식회사 엘지에너지솔루션 양극 활물질, 이의 제조 방법, 이를 포함하는 양극 및 리튬 이차 전지

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2744754B1 (en) * 2011-08-16 2016-11-02 Tiax Llc Polycrystalline metal oxide, methods of manufacture thereof, and articles comprising the same
WO2017189887A1 (en) * 2016-04-27 2017-11-02 Camx Power, L.L.C. Polycrystalline layered metal oxides comprising nano-crystals
US20190006669A1 (en) * 2017-06-30 2019-01-03 Samsung Electronics Co., Ltd. Composite cathode active material, cathode and lithium battery including the same, and method of preparing the composite cathode active material

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010211925A (ja) 2009-03-06 2010-09-24 Panasonic Corp 非水電解質二次電池用正極活物質、その製造方法、および非水電解質二次電池
KR101297175B1 (ko) 2011-03-10 2013-08-21 삼성에스디아이 주식회사 리튬 이차전지용 양극 활물질, 이의 제조방법 및 이를 이용한 리튬 이차전지
JP5971109B2 (ja) * 2011-12-20 2016-08-17 住友金属鉱山株式会社 ニッケル複合水酸化物とその製造方法、非水系電解質二次電池用正極活物質とその製造方法、および非水系電解質二次電池
JP2015213038A (ja) * 2014-05-07 2015-11-26 日立マクセル株式会社 非水電解質二次電池用正極材料および非水電解質二次電池
US11081693B2 (en) 2017-08-30 2021-08-03 Samsung Electronics Co., Ltd. Composite cathode active material, method of preparing the same, and cathode and lithium battery including the composite cathode active material

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2744754B1 (en) * 2011-08-16 2016-11-02 Tiax Llc Polycrystalline metal oxide, methods of manufacture thereof, and articles comprising the same
WO2017189887A1 (en) * 2016-04-27 2017-11-02 Camx Power, L.L.C. Polycrystalline layered metal oxides comprising nano-crystals
US20190006669A1 (en) * 2017-06-30 2019-01-03 Samsung Electronics Co., Ltd. Composite cathode active material, cathode and lithium battery including the same, and method of preparing the composite cathode active material

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of WO2020149910A1 *

Also Published As

Publication number Publication date
JP2025026975A (ja) 2025-02-26
JP2022522999A (ja) 2022-04-21
EP3912209A1 (en) 2021-11-24
CA3126058A1 (en) 2020-07-23
JP7629403B2 (ja) 2025-02-13
WO2020149910A1 (en) 2020-07-23
JP7857680B2 (ja) 2026-05-13
CN113678285A (zh) 2021-11-19
CN122000331A (zh) 2026-05-08
KR20210105440A (ko) 2021-08-26
KR20260008192A (ko) 2026-01-15

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