EP3830527A1 - Fluid contaminant detection using noise levels in magnetic flow meter sensor signals - Google Patents

Fluid contaminant detection using noise levels in magnetic flow meter sensor signals

Info

Publication number
EP3830527A1
EP3830527A1 EP19735093.7A EP19735093A EP3830527A1 EP 3830527 A1 EP3830527 A1 EP 3830527A1 EP 19735093 A EP19735093 A EP 19735093A EP 3830527 A1 EP3830527 A1 EP 3830527A1
Authority
EP
European Patent Office
Prior art keywords
noise
sensor signal
contaminant
flow meter
noise level
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP19735093.7A
Other languages
German (de)
French (fr)
Other versions
EP3830527B1 (en
Inventor
Scot Ronald Foss
Andrew Thomas KLINE
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Micro Motion Inc
Original Assignee
Micro Motion Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Micro Motion Inc filed Critical Micro Motion Inc
Publication of EP3830527A1 publication Critical patent/EP3830527A1/en
Application granted granted Critical
Publication of EP3830527B1 publication Critical patent/EP3830527B1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F1/00Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow
    • G01F1/56Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow by using electric or magnetic effects
    • G01F1/58Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow by using electric or magnetic effects by electromagnetic flowmeters
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F1/00Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow
    • G01F1/56Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow by using electric or magnetic effects
    • G01F1/58Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow by using electric or magnetic effects by electromagnetic flowmeters
    • G01F1/588Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow by using electric or magnetic effects by electromagnetic flowmeters combined constructions of electrodes, coils or magnetic circuits, accessories therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F1/00Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow
    • G01F1/56Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow by using electric or magnetic effects
    • G01F1/58Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow by using electric or magnetic effects by electromagnetic flowmeters
    • G01F1/60Circuits therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F1/00Measuring the volume flow or mass flow of fluid or fluent solid material wherein the fluid passes through a meter in a continuous flow
    • G01F1/74Devices for measuring flow of a fluid or flow of a fluent solid material in suspension in another fluid
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01MTESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00Investigating fluid-tightness of structures
    • G01M3/02Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/26Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/72Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables
    • G01N27/74Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables of fluids
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26Oils; Viscous liquids; Paints; Inks
    • G01N33/28Oils, i.e. hydrocarbon liquids
    • G01N33/2835Specific substances contained in the oils or fuels
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26Oils; Viscous liquids; Paints; Inks
    • G01N33/28Oils, i.e. hydrocarbon liquids
    • G01N33/2835Specific substances contained in the oils or fuels
    • G01N33/2841Gas in oils, e.g. hydrogen in insulating oils

Definitions

  • Oil wells bring fossil-fuels from underground to the surface.
  • the output of the well includes a combination of oil, natural gas, water and solid material, such as sand or silt.
  • Separators reside on onshore well pads and offshore platforms and are used to separate the oil and natural gas from each other and from the water and solid debris.
  • Separators include an inflow pipe that brings the output of the well into the separator, a natural gas output pipe, an oil output pipe and a water output pipe. If the oil level or water level drops too low, it is possible for natural gas to flow into the oil output pipe or the water output pipe. In addition, it is possible for oil or sand to enter the water output pipe. To prevent this, some separators place valves on the oil output pipe and the water output pipe that are designed to close when the oil level or the water level is too low. These valves, however, are susceptible to sticking due to sand and other debris present in the inflow to the separator. It would be useful to determine if gas, oil or sand is present in the water flow and to determine if gas is present in the oil flow.
  • a magnetic flow meter includes electrode sensors generating a sensor signal indicative of flow of a liquid through a conduit.
  • a noise identification module identifies a noise level in the sensor signal and a contaminant identification module uses the noise level to determine whether there is a contaminant in the liquid in the conduit.
  • a drive signal is applied to generate a magnetic field in a conduit carrying a liquid.
  • a sensor signal is received from electrodes positioned along the conduit and a noise level in the sensor signal is determined. The noise level is used to determine if the liquid contains a contaminant.
  • a process transmitter includes a magnetic coil and electrode sensors configured to generate a sensor signal.
  • a noise identification module is configured to determine a level of noise in the sensor signal and a contaminant identification module is configured to identify that a liquid contains a contaminant based on the determined level of noise.
  • FIG. 1 is a sectional view of a separator.
  • FIG. 2 is a block diagram of a flow meter in accordance with one embodiment.
  • FIG. 3 is a graph of a drive signal for a magnetic flow meter.
  • FIG. 4 is a graph of a magnetic flow meter sensor signal in response to the drive signal of FIG. 3 for a liquid that does not contain a contaminant.
  • FIG. 5 is a graph of a magnetic flow meter sensor signal in response to the drive signal of FIG. 3 for a liquid containing a contaminant.
  • FIG. 6 is a graph of the noise level in the magnetic flow meter sensor signal as a function of the gas void fraction in the liquid.
  • FIG. 7 is a flow diagram of a method of collecting data in accordance with one embodiment.
  • FIG. 8 is a block diagram of elements used in the method of FIG. 7.
  • FIG. 9 is a flow diagram of a method of identifying noise levels in a magnetic flow meter sensor signal in accordance with one embodiment.
  • FIG. 10 is a block diagram of elements used in the method of FIG. 9.
  • FIG. 11 is a flow diagram of a method of identifying a contaminant using noise levels in accordance with one embodiment.
  • FIG. 12 is a block diagram of elements used in the method of FIG. 11.
  • FIG. 13 provides graphs of Fast Fourier Transforms of magnetic flow meter sensor signals for different percentages of gas void fraction.
  • FIG. 14 is an expanded view of one of the graphs of FIG. 13 showing samples used to determine a noise level in the magnetic flow meter sensor signal.
  • FIG. 15 are graphs of noise levels in magnetic flow meter sensor signals determined for different ranges of frequencies during an increase in gas void fractions.
  • FIG. 16 are graphs of noise levels in magnetic flow meter sensor signals determined for different ranges of frequencies during an increase in oil percentage in a water line.
  • FIG. 17 shows graphs of noise levels in magnetic flow meter sensor signals as a function of gas void fractions for two separate flow rates.
  • FIG. 18 shows a graph of noise levels in magnetic flow meter sensor signals as a function of oil levels in a water line.
  • FIG. 19 shows a graph of noise levels in magnetic flow meter sensor signals as a function of pounds of sand in a water line.
  • FIG. 20 is a flow diagram of a method of collecting noise data in accordance with a further embodiment.
  • FIG. 21 is a block diagram of the elements used in the method of FIG. 20.
  • FIG. 22 is a flow diagram of a method of identifying noise levels in a magnetic flow meter sensor signal in accordance with a further embodiment.
  • FIG. 23 is a block diagram of elements used in the method of FIG. 22.
  • Embodiments described below provide process transmitters that detect when a conductive liquid carried by a conduit contains a contaminant such as a gas, another liquid or particulates, such as sand, for example.
  • the process transmitters make these determinations by monitoring the noise level in a magnetic flow meter’s sensor signal.
  • the present inventors have discovered that as the amount of a contaminant in a liquid increases, the noise level of the magnetic flow meter’s sensor signal increases.
  • FIG. 1 provides an example environment 100 in which flow meter 104 of the various embodiments may be utilized.
  • Environment 100 includes a separator tank 106 that is able to separate an inflow 108 into various constituents including water 110, oil 112, and gas 114.
  • Inflow 108 may be from a well head, in some embodiments.
  • Separator tank 106 includes an inlet baffle 116 and a quieting baffle 118 that are used to reduce the velocity of inflow 108 to allow the constituents of inflow 108 to separate from each other to form a gas layer 122, an oil layer 124 and a water layer 126.
  • a mist pad 120 collects water and oil droplets present in gas layer 122 and causes the collected oil and water to drop into oil layer 124 and water layer 126.
  • Oil layer 124 and water layer 126 flow toward a weir 128 that separates oil layer 124 from water layer 126.
  • oil layer 124 flows over the top of weir 128 into an oil chamber 130.
  • Water layer 126 flows under oil chamber 130 and into a water chamber 132.
  • the level of oil in oil chamber 130 is controlled by a liquid level controller 134 and a valve 136. As liquid level controller 134 drops, valve 136 is closed to prevent fluid from flowing through valve 136.
  • liquid level controller 134 include a mechanical controller, a pneumatic controller, and an electronic controller. When operating properly, liquid level controller 134 should completely close valve 136 when the oil level drops below the intake of a downcomer 138 thereby preventing gas 114 from flowing through an output oil conduit 140. Preventing gas from flowing through conduit 140 is important since such gas is valuable and can be dangerous if not handled properly.
  • liquid level controller 142 The level of water in water chamber 132 is controlled by liquid level controller 142 and valve 144. As the water level in water chamber 132 drops, liquid level controller 142 closes valve 144 to prevent fluids from flowing through output water conduit 146. Liquid level controller 142 may be a mechanical controller, a pneumatic controller, or an electronic controller. By closing valve 144, liquid level controller 142 prevents gas 114 from flowing through conduit 146 when the water 110 in chamber 132 drops below an intake of a downcomer 148. This prevents gas from entering a water storage tank thereby preventing the loss of valuable gas and preventing explosive gases from developing within the water storage tank.
  • flow meter 104 detects when a contaminant such as gas, oil or sand is flowing in water conduit 146. Upon detecting that a contaminant is present in the conduit, flow meter 104 can provide an alert message and/or an indication of the amount of contaminant that is in the conduit.
  • FIG. 2 provides a schematic diagram of a process transmitter in the form of a magnetic flow meter 200, which is an example of flow meter 104, in accordance with the various embodiments.
  • Magnetic flow meter 200 includes a coil driver 202, which drives electrical current through two coils 204 and 206 positioned on opposite sides of a conduit 208. The current in coils 204 and 206 generates a magnetic field 230 that passes through conduit 208. In accordance with most embodiments, the current in coils 204 and 206 is periodically reversed causing the direction of magnetic field 230 to alternate between extending from coil 204 to coil 206 to extending from coil 206 to coil 204.
  • Conduit 208 carries a conductive liquid that moves through conduit 208 in a flow direction 210.
  • Polar molecules or charged molecules and atoms within the liquid experience a force that is orthogonal to magnetic field 230 due to their movement through magnetic field 230 in flow direction 210.
  • positively charged molecules and atoms move in one direction and negatively charged molecules and atoms in an opposite direction.
  • Polar molecules align such that the positive end of the molecules all point in one direction and the negative end of the molecules point in the opposite direction.
  • Electrodes 212 and 214 are connected to an analog-to-digital convertor 216 in a housing 228.
  • Analog-to-digital convertor 216 samples the analog voltage between electrodes 212 and 214 to produce a series of digital samples for a data collection module 218.
  • Data collection module 218 selectively stores some or all of the digital samples for use by a flow calculator 220, which uses the magnitude of the digital samples to estimate a flow rate for the liquid. This flow rate is periodically provided to an input/output circuit 224, which transmits the flow rate to a control room along a communication channel, such as a two- wire process loop 226.
  • FIG. 3 provides a graph 300 of a square wave drive signal that is applied to coils 204 and 206 to generate the magnetic field in accordance with one embodiment.
  • the magnitude of the current is shown along vertical axis 302 and time is shown along horizontal axis 304.
  • the current alternates between a positive and a negative current of the same magnitude.
  • the drive signal is a sine wave or a multi-step pulsed DC wave such as a 75 Hz square wave superimposed on a 5Hz square wave, for example.
  • FIG. 4 provides a graph 400 of a sensor signal generated between electrodes 212 and 214 when a fluid without a contaminant is flowing through conduit 208 and drive signal 300 is applied to coils 204 and 206.
  • the voltage between electrodes 212 and 214 is shown on vertical axis 402 in terms of counts generated by analog-to-digital convertor 216.
  • Time is shown along horizontal axis 404.
  • the voltage alternates between positive and negative values of similar magnitudes and is relatively stable at each positive and negative value.
  • FIG. 5 provides a graph 500 of a sensor signal generated between electrodes 212 and 214 when a contaminant is present in the fluid and drive signal 300 is applied to coils 204 and 206.
  • the voltage between electrodes 212 and 214 is shown on vertical axis 502 in terms of counts generated by analog-to-digital convertor 216 and time is shown along horizontal axis 504.
  • the contaminant causes variations in the sensed voltage during the steady-state portions of drive signal 300. The present inventors refer to these variations in the voltage as noise in the sensor signal.
  • FIG. 6 provides graphs 600 and 602 showing the correlation between gas void fractions in a liquid and noise levels in a sensor signal.
  • graph 600 shows a change in the gas void fraction over time during an experiment, with axis 604 showing the gas void fraction as a percentage of a volume in the conduit.
  • Graph 602 shows the magnitude of the noise in the sensor signal formed during the change in gas void fraction shown in graph 600, with the magnitude of the noise depicted on vertical axis 606.
  • FIG. 6 it can be seen that soon after the gas void fraction begins to increase, the magnitude of the noise in the sensor signal also increases.
  • the digital values output by analog-to-digital converter 216 are provided to a data collection module 240, which selectively samples and filters the digital values to produce a set of digital values for a noise identification module 242.
  • Noise identification module 242 uses the digital values to identify a sequence of noise values, representing the magnitude of the noise in each of a set of time periods or sections of the sensor signal.
  • the sequence of noise values is provided to a contaminant /valve chatter identification module 244, which filters the sequence of noise values to remove spikes in the noise and uses the filtered noise values to determine if the liquid contains a contaminant or if a valve in the process system is experiencing valve chatter.
  • contaminant/valve chatter identification module 244 optionally provides an estimate of the amount of contaminant in the liquid.
  • contaminant/valve chatter identification module 244 sends an alert through I/O circuit 224 and communication channel 226 indicating the contaminant and optionally the estimated amount of the contaminant.
  • FIG. 7 provides a flow diagram of a method implemented by data collection module 240 in accordance with one embodiment.
  • FIG. 8 provides a block diagram of elements used in the method of FIG. 7.
  • analog-to-digital convertor 216 issues an interrupt signal indicating that analog-to-digital convertor 216 has a new digital sample of the sensor signal.
  • the digital sample output by analog-to-digital convertor 216 is stored in a rolling or circular buffer 800 at step 702.
  • a cycle monitor 802 determines if an end of a half-cycle of the drive signal has been reached, where the end of a half cycle is the point where the drive signal changes polarity. For example, time points 306 and 308 of FIG.
  • cycle monitor 802 determines if the end of a half-cycle has been reached by comparing the polarity of the drive signal to the polarity determined at a previous time point to see if the polarity has changed.
  • the end of the half-cycle is determined by comparing the latest output value from analog-to-digital convertor 216 and a previous output of analog-to-digital convertor 216 to an average of the output values from analog-to-digital converter 216.
  • line 506 represents the average of the output values from analog-to-digital convertor 216.
  • Sample 502 is shown to be at the end of a half-cycle 512 and is greater than average 506 while sample 504, the sample immediately after sample 502, is shown to be at the beginning of a next half-cycle 514 and is less than average 506.
  • sample 508 is shown to be at the end of half-cycle 514 and is less than average 506 while sample 510, which is immediately after sample 508, is shown to be at the beginning of the next half-cycle 516 and is greater than average 506.
  • a sample selection module 806 is triggered to select a percentage of the samples generated during the last half-cycle at step 706.
  • the last twenty percent of the samples in the half-cycle are selected. For example, in FIG. 5 the set of samples 520 at the end of half-cycle 512 are selected during a first pass through step 706 and the set of samples 522 at the end of half-cycle 514 are selected during the next pass through step 706.
  • the selection of the samples in step 706 is a selection of a portion of the sensor signal for determining a noise level and separate noise levels are determined for each portion of the sensor signal selected with each execution of step 706.
  • a square wave is used as the drive signal.
  • samples for the last 20% of each half-cycle of the higher-frequency square wave are selected by sample selection module 806. (for example, the 75 Hz square wave when a 75 Hz square wave is superimposed on a 5 Hz square wave to form the pulsed DC wave).
  • the drive signal is a sine wave
  • a high pass filter is used to by sample selection module 806 to select a subset of the samples for measuring noise.
  • the selected samples are then processed in noise identification module 242 using the method of FIG. 9 and the elements in the block diagram of FIG. 10 to identify the level of noise in the selected samples.
  • the samples selected by data collection 240 are ready to be processed.
  • the samples are applied to a DC filter 1000, which subtracts a DC value from the samples.
  • the DC value is an average of the selected samples.
  • the DC filtered samples are applied to a high-pass filter 1002, which removes low frequency signals common to sensor signals generated from pure liquids that do not contain a contaminant.
  • the level of noise in the filtered signal can be determined using one or more of a standard deviation calculator 1004 in step 906, a range calculator 1006 in step 908, an average movement per step calculator 1008 in step 910 and/or a maximum movement per step calculator 1010 in step 912.
  • Standard deviation calculator 1004 determines the standard deviation of the filtered samples and sets the noise level to the standard deviation.
  • Range calculator 1006 determines the difference between the largest filtered sample and the smallest filtered sample in the set of samples selected for the half-cycle and sets the noise level to the difference.
  • Average movement per step calculator 1008 determines the average difference between successive filtered samples in the set of samples selected for the half-cycle and sets the noise level to this average difference.
  • Max movement per step calculator 1010 determines the largest difference between successive filtered samples in the set of samples selected for the half cycle and sets the noise level to this largest difference. In some embodiments, two or more of these noise levels are combined by, for example, averaging the two or more noise levels together.
  • FIG. 11 provides a flow diagram of a method of identifying a contaminant for the noise levels in accordance with one embodiment.
  • FIG. 12 provides a block diagram of elements used in the method of FIG. 11.
  • the noise levels are applied to a median filter 1200 which forms a window of successive noise levels, such as four successive noise levels, and selects the median of those noise levels as the noise level for the window.
  • the noise levels output by median filter 1200 are applied to a low pass filter 1202 to remove high-frequency noise.
  • the filtered noise levels are applied to a comparator 1204, which compares the filtered noise levels to a threshold 1206. If the filtered noise level does not exceed the threshold, the process of FIG. 11 ends at step 1112. If the filtered noise levels exceed threshold 1206 at step 1104, an alert is sent by alert generation 1212 to a host system through I/O circuit 224 and communication channel 226 at step 1106.
  • the filtered noise levels are applied to a contaminant estimator 1210, which estimates the amount of contaminant in the liquid using a noise-to-contaminant function 1208 at step 1108.
  • Noise-to- contaminant function 1208 describes the relationship between the filtered noise levels and the amount of contaminant in the liquid and can be determined from experimental data.
  • contaminant estimator 1210 can estimate an amount of gas in a liquid, an amount of oil in a liquid and/or an amount of solid particles in a liquid
  • contaminant estimator 248 sends the amount of contaminant in the liquid to alert generation 1212, which forwards the amount of contaminant to the host through I/O circuit 224 and communication channel 226.
  • a single alert is sent by alert generation 1212 to convey that the liquid contains a contaminant and the amount of the contaminant in the liquid.
  • data collection 240 and noise identification 242 identify a noise level in the sensor signal using a frequency-domain analysis of the sensor signal.
  • FIG. 13 shows graphs 1300, 1302, 1304, 1306, and 1308 of a Fast Fourier Transform of sensor signals from a magnetic flow meter generated from a liquid flowing at 3 feet per second and containing respective amounts of gas void fractions of 20%, 10%, 5%, 1% and 0%.
  • the magnitude of the signal is shown along vertical axis 1310 and frequency is shown along horizontal axis 1312. As shown in FIG. 13, as the gas void fraction increases, the magnitude of the sensor signal increases across all frequencies.
  • FIG. 14 shows an expanded view of graph 1300 with dots positioned at each frequency that is used in the noise determination.
  • the drive frequency is 5 Hz and values at even and odd multiples of this frequency are not used to determine the noise level.
  • dots are not present on graph 1300.
  • the noise is distributed across many frequencies as indicated by the graphs of FIG. 15 where three separate graphs 1500, 1502, and 1504 of noise versus time are shown for an increase in gas void fraction from zero to thirty percent using three respective frequency bands: 2-50 Hz, 2-100 Hz, and 2-200 Hz.
  • the magnitude of the noise is shown along vertical axis 1506 and time is shown along horizontal axis 1508.
  • the noise level increases as the amount of gas in the liquid increases.
  • the noise level is seen to increase more for the wider band of frequencies 1504 than for the narrower band of frequencies 1500, indicating that the noise is distributed across a wide spectrum of frequencies.
  • the noise level is shown to increase 175 times for a 30% increase in gas void fraction.
  • three graphs 1600, 1602 and 1604 of noise versus time show an increase in noise as the percentage of oil in a water line is increased from zero to ten percent and then to twenty percent for respective frequency bands of 2-50 Hz, 2-100 Hz, and 2-200 Hz.
  • the magnitude of the noise is shown along vertical axis 1608 and time is shown along horizontal axis 1610.
  • the noise increases with each increase in the percentage of oil in the water line for each frequency band.
  • FIG. 18 provides a graph 1800 showing a relationship between frequency-domain determined noise and a percentage of oil added to a water flow.
  • the noise magnitude is shown along vertical axis 1802 and the oil percentage is shown along horizontal axis 1804.
  • Graph 1800 indicates that the noise level generally increases as the percentage of oil in the water flow increases.
  • FIG. 19 provides a graph 1900 showing the relationship between frequency-domain determined noise and pounds of sand in a water flow.
  • the noise magnitude is shown along vertical axis 1902 and the amount of sand is shown along horizontal axis 1904.
  • Graph 1900 indicates that the noise level increases as the amount of sand increases.
  • FIG. 20 provides a flow diagram of a method used by data collection module 240 to collect data for performing frequency-domain noise level identification.
  • FIG. 21 provides a block diagram of elements used in the method of FIG. 20.
  • analog-to-digital convertor 216 issues an interrupt indicating that a new digital sample has been produced from the magnetic flow meter sensor signal.
  • a decimator 2100 applies a decimation algorithm to the sample to determine if the sample should be stored in a rolling buffer 2102. The decimating algorithm selects a subset of the samples for storage in rolling buffer 2102 thereby acting as a low pass digital filter.
  • a monitor 2104 determines if enough samples have been added to rolling buffer 2102 to support a Fast Fourier Transform. If more samples are needed, the process of FIG. 20 returns to step 2000 to wait for another interrupt from analog-to-digital convertor 216.
  • step 2006 the process returns to step 2000 to wait for the next interrupt from analog-to-digital convertor 216.
  • FIG. 22 provides a flow diagram of a method performed by noise identification module 242 to identify the noise in the sensor signal using a frequency-domain technique.
  • FIG. 23 provides a block diagram of elements used in the method of FIG. 22.
  • step 2200 the start and end locations of the next set of data in rolling buffer 2102 to be processed are used to copy the data from rolling buffer 2102 to a selection buffer 2300. By copying these values, step 2200 is selecting a section or part of the sensor signal for conversion into the frequency domain.
  • step 2202 the data in selection buffer 2300 is applied to a DC filter 2302, which removes the DC component from each value of the data. In accordance with one embodiment, the DC component is simply an average of all of the data in selection buffer 2300.
  • the data are applied to a Hanning window 2304, which reduces the magnitudes of the data at the beginning and the end of the current section of the sensor signal to reduce frequency leakage when the Fast Fourier Transform is applied.
  • the resulting data values are applied to a Fast Fourier Transform 2306, which converts the time-domain data values into a set of frequency-domain data values, with each frequency-domain data value being a complex number representing the magnitude and phase of the sensor signal for a respective frequency.
  • each complex number is applied to a magnitude calculator 2308 to determine the magnitude for each frequency.
  • the magnitudes are applied to a harmonic filter 2310, which removes the magnitudes for frequencies that are even or odd harmonics of the coil drive frequency.
  • harmonic frequencies contain the liquid’s response to the drive signal as well as the noise in the signal due to a contaminant in the liquid.
  • the noise due to a contaminant can be isolated from the remainder of the sensor signal.
  • the filtered magnitudes are averaged by an average calculator 2312 and the average is stored in a noise buffer 2314 for the section of the sensor signal selected in step 2200.
  • noise values in noise buffer 2314 are then applied to a contaminant identification module 244 in the same manner as discussed above for the time-domain noise values.
  • the method of FIG. 11 and the block diagram of FIG. 12 can be used for the frequency-domain based noise values in the same way that they were used for the time-domain based noise values.
  • the noise in the magnetic flow meter sensor signal can additionally be used to detect valve chatter.
  • a relief valve in separator 100 rapidly opens and closes causing rapid fluctuations in the pressure within separator 100. This pressure fluctuation produces a corresponding fluctuation in the speed of the flow through conduits 140 and 146. Such fluctuations in the speed of the flow appear as noise in the magnetic flow meter sensor signal.
  • isolating and measuring the noise in the sensor signal using either of the embodiments discussed above allows the valve chatter to be detected since the noise level of the sensor signal will increase dramatically during valve chatter.

Landscapes

  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Pathology (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Fluid Mechanics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Electromagnetism (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Investigating Or Analyzing Materials By The Use Of Magnetic Means (AREA)
  • Measuring Volume Flow (AREA)
  • Geophysics And Detection Of Objects (AREA)

Abstract

A magnetic flow meter (200) includes electrode sensors (212, 214) generating a sensor signal indicative of flow of a liquid through a conduit (208). A noise identification module (242) identifies a noise level in the sensor signal and a contaminant identification module (244) uses the noise level to determine whether there is a contaminant in the liquid in the conduit (208).

Description

FLUID CONTAMINANT DETECTION USING NOISE LEVELS IN MAGNETIC FLOW
METER SENSOR SIGNALS
BACKGROUND
[0001] Oil wells bring fossil-fuels from underground to the surface. In many wells, the output of the well includes a combination of oil, natural gas, water and solid material, such as sand or silt. Separators reside on onshore well pads and offshore platforms and are used to separate the oil and natural gas from each other and from the water and solid debris.
[0002] There are many types of density separators but they all function in the same manner by using gravity and an emulsifier layer to separate the constituents of the well output. In particular, the separators slow the fluid flow to allow heavier sand and water to separate from the oil. The water and solid material pass through the emulsifier layer while the oil remains on top of the emulsifier layer. A space is provided above the oil that allows the natural gas to separate from the oil. One or more mist converters may be provided to collect oil droplets that may be suspended in the natural gas.
[0003] Separators include an inflow pipe that brings the output of the well into the separator, a natural gas output pipe, an oil output pipe and a water output pipe. If the oil level or water level drops too low, it is possible for natural gas to flow into the oil output pipe or the water output pipe. In addition, it is possible for oil or sand to enter the water output pipe. To prevent this, some separators place valves on the oil output pipe and the water output pipe that are designed to close when the oil level or the water level is too low. These valves, however, are susceptible to sticking due to sand and other debris present in the inflow to the separator. It would be useful to determine if gas, oil or sand is present in the water flow and to determine if gas is present in the oil flow.
SUMMARY
[0004] A magnetic flow meter includes electrode sensors generating a sensor signal indicative of flow of a liquid through a conduit. A noise identification module identifies a noise level in the sensor signal and a contaminant identification module uses the noise level to determine whether there is a contaminant in the liquid in the conduit. [0005] In accordance with a further embodiment, a drive signal is applied to generate a magnetic field in a conduit carrying a liquid. A sensor signal is received from electrodes positioned along the conduit and a noise level in the sensor signal is determined. The noise level is used to determine if the liquid contains a contaminant.
[0006] In accordance with a still further embodiment, a process transmitter includes a magnetic coil and electrode sensors configured to generate a sensor signal. A noise identification module is configured to determine a level of noise in the sensor signal and a contaminant identification module is configured to identify that a liquid contains a contaminant based on the determined level of noise.
[0007] This Summary and the Abstract are provided to introduce a selection of concepts in a simplified form that are further described below in the Detailed Description. The Summary and the Abstract are not intended to identify key features or essential features of the claimed subject matter, nor are they intended to be used as an aid in determining the scope of the claimed subject matter.
BRIEF DESCRIPTION OF THE DRAWINGS
[0008] FIG. 1 is a sectional view of a separator.
[0009] FIG. 2 is a block diagram of a flow meter in accordance with one embodiment.
[0010] FIG. 3 is a graph of a drive signal for a magnetic flow meter.
[0011] FIG. 4 is a graph of a magnetic flow meter sensor signal in response to the drive signal of FIG. 3 for a liquid that does not contain a contaminant.
[0012] FIG. 5 is a graph of a magnetic flow meter sensor signal in response to the drive signal of FIG. 3 for a liquid containing a contaminant.
[0013] FIG. 6 is a graph of the noise level in the magnetic flow meter sensor signal as a function of the gas void fraction in the liquid.
[0014] FIG. 7 is a flow diagram of a method of collecting data in accordance with one embodiment.
[0015] FIG. 8 is a block diagram of elements used in the method of FIG. 7.
[0016] FIG. 9 is a flow diagram of a method of identifying noise levels in a magnetic flow meter sensor signal in accordance with one embodiment. [0017] FIG. 10 is a block diagram of elements used in the method of FIG. 9.
[0018] FIG. 11 is a flow diagram of a method of identifying a contaminant using noise levels in accordance with one embodiment.
[0019] FIG. 12 is a block diagram of elements used in the method of FIG. 11.
[0020] FIG. 13 provides graphs of Fast Fourier Transforms of magnetic flow meter sensor signals for different percentages of gas void fraction.
[0021] FIG. 14 is an expanded view of one of the graphs of FIG. 13 showing samples used to determine a noise level in the magnetic flow meter sensor signal.
[0022] FIG. 15 are graphs of noise levels in magnetic flow meter sensor signals determined for different ranges of frequencies during an increase in gas void fractions.
[0023] FIG. 16 are graphs of noise levels in magnetic flow meter sensor signals determined for different ranges of frequencies during an increase in oil percentage in a water line.
[0024] FIG. 17 shows graphs of noise levels in magnetic flow meter sensor signals as a function of gas void fractions for two separate flow rates.
[0025] FIG. 18 shows a graph of noise levels in magnetic flow meter sensor signals as a function of oil levels in a water line.
[0026] FIG. 19 shows a graph of noise levels in magnetic flow meter sensor signals as a function of pounds of sand in a water line.
[0027] FIG. 20 is a flow diagram of a method of collecting noise data in accordance with a further embodiment.
[0028] FIG. 21 is a block diagram of the elements used in the method of FIG. 20.
[0029] FIG. 22 is a flow diagram of a method of identifying noise levels in a magnetic flow meter sensor signal in accordance with a further embodiment.
[0030] FIG. 23 is a block diagram of elements used in the method of FIG. 22.
DETAILED DESCRIPTION OF ILLUSTRATIVE EMBODIMENTS
[0031] Embodiments described below provide process transmitters that detect when a conductive liquid carried by a conduit contains a contaminant such as a gas, another liquid or particulates, such as sand, for example. The process transmitters make these determinations by monitoring the noise level in a magnetic flow meter’s sensor signal. The present inventors have discovered that as the amount of a contaminant in a liquid increases, the noise level of the magnetic flow meter’s sensor signal increases.
[0032] FIG. 1 provides an example environment 100 in which flow meter 104 of the various embodiments may be utilized. Environment 100 includes a separator tank 106 that is able to separate an inflow 108 into various constituents including water 110, oil 112, and gas 114. Inflow 108 may be from a well head, in some embodiments.
[0033] Separator tank 106 includes an inlet baffle 116 and a quieting baffle 118 that are used to reduce the velocity of inflow 108 to allow the constituents of inflow 108 to separate from each other to form a gas layer 122, an oil layer 124 and a water layer 126. A mist pad 120 collects water and oil droplets present in gas layer 122 and causes the collected oil and water to drop into oil layer 124 and water layer 126. Oil layer 124 and water layer 126 flow toward a weir 128 that separates oil layer 124 from water layer 126. In particular, oil layer 124 flows over the top of weir 128 into an oil chamber 130. Water layer 126 flows under oil chamber 130 and into a water chamber 132.
[0034] The level of oil in oil chamber 130 is controlled by a liquid level controller 134 and a valve 136. As liquid level controller 134 drops, valve 136 is closed to prevent fluid from flowing through valve 136. Examples of liquid level controller 134 include a mechanical controller, a pneumatic controller, and an electronic controller. When operating properly, liquid level controller 134 should completely close valve 136 when the oil level drops below the intake of a downcomer 138 thereby preventing gas 114 from flowing through an output oil conduit 140. Preventing gas from flowing through conduit 140 is important since such gas is valuable and can be dangerous if not handled properly.
[0035] The level of water in water chamber 132 is controlled by liquid level controller 142 and valve 144. As the water level in water chamber 132 drops, liquid level controller 142 closes valve 144 to prevent fluids from flowing through output water conduit 146. Liquid level controller 142 may be a mechanical controller, a pneumatic controller, or an electronic controller. By closing valve 144, liquid level controller 142 prevents gas 114 from flowing through conduit 146 when the water 110 in chamber 132 drops below an intake of a downcomer 148. This prevents gas from entering a water storage tank thereby preventing the loss of valuable gas and preventing explosive gases from developing within the water storage tank. [0036] For various reasons, it is possible for entrained gas and/or sand to occasionally flow through oil conduit 140 or water conduit 146 and it is possible for oil to flow through water conduit 146. In the embodiments described below, flow meter 104 detects when a contaminant such as gas, oil or sand is flowing in water conduit 146. Upon detecting that a contaminant is present in the conduit, flow meter 104 can provide an alert message and/or an indication of the amount of contaminant that is in the conduit.
[0037] FIG. 2 provides a schematic diagram of a process transmitter in the form of a magnetic flow meter 200, which is an example of flow meter 104, in accordance with the various embodiments. Magnetic flow meter 200 includes a coil driver 202, which drives electrical current through two coils 204 and 206 positioned on opposite sides of a conduit 208. The current in coils 204 and 206 generates a magnetic field 230 that passes through conduit 208. In accordance with most embodiments, the current in coils 204 and 206 is periodically reversed causing the direction of magnetic field 230 to alternate between extending from coil 204 to coil 206 to extending from coil 206 to coil 204.
[0038] Conduit 208 carries a conductive liquid that moves through conduit 208 in a flow direction 210. Polar molecules or charged molecules and atoms within the liquid experience a force that is orthogonal to magnetic field 230 due to their movement through magnetic field 230 in flow direction 210. In particular, positively charged molecules and atoms move in one direction and negatively charged molecules and atoms in an opposite direction. Polar molecules align such that the positive end of the molecules all point in one direction and the negative end of the molecules point in the opposite direction. When the direction of the magnetic field changes, the direction that the charged molecules and atoms move and the orientation of polar molecules switches. This results in an alternating voltage between two electrodes or electrode sensors 212 and 214 that are positioned along a line that is orthogonal to the direction of the magnetic field in the conduit. The magnitude of the voltage is affected by the flow rate of the liquid with faster flow rates resulting in larger voltages.
[0039] Electrodes 212 and 214 are connected to an analog-to-digital convertor 216 in a housing 228. Analog-to-digital convertor 216 samples the analog voltage between electrodes 212 and 214 to produce a series of digital samples for a data collection module 218. Data collection module 218 selectively stores some or all of the digital samples for use by a flow calculator 220, which uses the magnitude of the digital samples to estimate a flow rate for the liquid. This flow rate is periodically provided to an input/output circuit 224, which transmits the flow rate to a control room along a communication channel, such as a two- wire process loop 226.
[0040] FIG. 3 provides a graph 300 of a square wave drive signal that is applied to coils 204 and 206 to generate the magnetic field in accordance with one embodiment. In FIG. 3, the magnitude of the current is shown along vertical axis 302 and time is shown along horizontal axis 304. As shown in FIG. 3, the current alternates between a positive and a negative current of the same magnitude. In accordance with other embodiments, the drive signal is a sine wave or a multi-step pulsed DC wave such as a 75 Hz square wave superimposed on a 5Hz square wave, for example.
[0041] FIG. 4 provides a graph 400 of a sensor signal generated between electrodes 212 and 214 when a fluid without a contaminant is flowing through conduit 208 and drive signal 300 is applied to coils 204 and 206. In FIG. 4, the voltage between electrodes 212 and 214 is shown on vertical axis 402 in terms of counts generated by analog-to-digital convertor 216. Time is shown along horizontal axis 404. As shown in FIG. 4, the voltage alternates between positive and negative values of similar magnitudes and is relatively stable at each positive and negative value.
[0042] FIG. 5 provides a graph 500 of a sensor signal generated between electrodes 212 and 214 when a contaminant is present in the fluid and drive signal 300 is applied to coils 204 and 206. In FIG. 5, the voltage between electrodes 212 and 214 is shown on vertical axis 502 in terms of counts generated by analog-to-digital convertor 216 and time is shown along horizontal axis 504. In addition, the contaminant causes variations in the sensed voltage during the steady-state portions of drive signal 300. The present inventors refer to these variations in the voltage as noise in the sensor signal.
[0043] As discussed further below, the present inventors have developed several techniques for quantifying such noise in the sensor signal of a magnetic flow meter. Using one such technique, the inventors have discovered that the magnitude of the noise is correlated with the amount of a contaminant in a liquid. For example, FIG. 6 provides graphs 600 and 602 showing the correlation between gas void fractions in a liquid and noise levels in a sensor signal. Specifically, graph 600 shows a change in the gas void fraction over time during an experiment, with axis 604 showing the gas void fraction as a percentage of a volume in the conduit. Graph 602 shows the magnitude of the noise in the sensor signal formed during the change in gas void fraction shown in graph 600, with the magnitude of the noise depicted on vertical axis 606. In FIG. 6, it can be seen that soon after the gas void fraction begins to increase, the magnitude of the noise in the sensor signal also increases.
[0044] To identify the magnitude of the noise in the sensor signal, the digital values output by analog-to-digital converter 216 are provided to a data collection module 240, which selectively samples and filters the digital values to produce a set of digital values for a noise identification module 242. Noise identification module 242 uses the digital values to identify a sequence of noise values, representing the magnitude of the noise in each of a set of time periods or sections of the sensor signal. The sequence of noise values is provided to a contaminant /valve chatter identification module 244, which filters the sequence of noise values to remove spikes in the noise and uses the filtered noise values to determine if the liquid contains a contaminant or if a valve in the process system is experiencing valve chatter. If the filtered noise values indicate that the liquid contains a contaminant, contaminant/valve chatter identification module 244 optionally provides an estimate of the amount of contaminant in the liquid. When the liquid contains a contaminant or valve chatter is present, contaminant/valve chatter identification module 244 sends an alert through I/O circuit 224 and communication channel 226 indicating the contaminant and optionally the estimated amount of the contaminant.
[0045] FIG. 7 provides a flow diagram of a method implemented by data collection module 240 in accordance with one embodiment. FIG. 8 provides a block diagram of elements used in the method of FIG. 7. In step 700 of FIG. 7, analog-to-digital convertor 216 issues an interrupt signal indicating that analog-to-digital convertor 216 has a new digital sample of the sensor signal. In response to the interrupt, the digital sample output by analog-to-digital convertor 216 is stored in a rolling or circular buffer 800 at step 702. At step 704, a cycle monitor 802 determines if an end of a half-cycle of the drive signal has been reached, where the end of a half cycle is the point where the drive signal changes polarity. For example, time points 306 and 308 of FIG. 3 each mark the end of a half-cycle in drive signal 300. In accordance with one embodiment, cycle monitor 802 determines if the end of a half-cycle has been reached by comparing the polarity of the drive signal to the polarity determined at a previous time point to see if the polarity has changed. In accordance with other embodiments, the end of the half-cycle is determined by comparing the latest output value from analog-to-digital convertor 216 and a previous output of analog-to-digital convertor 216 to an average of the output values from analog-to-digital converter 216. If one of the values is greater than the average and the other is less than the average, the latest output value is considered to be part of the next half-cycle and the previous output value is considered to the last value in the previous half-cycle. For example, in FIG. 5, line 506 represents the average of the output values from analog-to-digital convertor 216. Sample 502 is shown to be at the end of a half-cycle 512 and is greater than average 506 while sample 504, the sample immediately after sample 502, is shown to be at the beginning of a next half-cycle 514 and is less than average 506. Similarly, sample 508 is shown to be at the end of half-cycle 514 and is less than average 506 while sample 510, which is immediately after sample 508, is shown to be at the beginning of the next half-cycle 516 and is greater than average 506.
[0046] If the end of the half-cycle has not been reached at step 704, the process returns to step 700 to await another interrupt from analog-to-digital convertor 216. When the end of the half-cycle has been reached, a sample selection module 806 is triggered to select a percentage of the samples generated during the last half-cycle at step 706. In accordance with one embodiment, the last twenty percent of the samples in the half-cycle are selected. For example, in FIG. 5 the set of samples 520 at the end of half-cycle 512 are selected during a first pass through step 706 and the set of samples 522 at the end of half-cycle 514 are selected during the next pass through step 706. This ensures that the drive signal on the coils and the sensor signal have settled after the previous switch in polarity of the drive signal before using the samples to detect noise in the sensor signal. Although twenty percent of the samples have been used in one embodiment, in other embodiments other percentages are used. The selection of the samples in step 706 is a selection of a portion of the sensor signal for determining a noise level and separate noise levels are determined for each portion of the sensor signal selected with each execution of step 706.
[0047] In the embodiment of FIG. 7 a square wave is used as the drive signal. In embodiments where a multi-step pulsed DC wave is used as the drive signal, samples for the last 20% of each half-cycle of the higher-frequency square wave are selected by sample selection module 806. (for example, the 75 Hz square wave when a 75 Hz square wave is superimposed on a 5 Hz square wave to form the pulsed DC wave). In embodiments where the drive signal is a sine wave, a high pass filter is used to by sample selection module 806 to select a subset of the samples for measuring noise.
[0048] The selected samples are then processed in noise identification module 242 using the method of FIG. 9 and the elements in the block diagram of FIG. 10 to identify the level of noise in the selected samples. At step 900, the samples selected by data collection 240 are ready to be processed. At step 902, the samples are applied to a DC filter 1000, which subtracts a DC value from the samples. In accordance with one embodiment, the DC value is an average of the selected samples. In step 904, the DC filtered samples are applied to a high-pass filter 1002, which removes low frequency signals common to sensor signals generated from pure liquids that do not contain a contaminant.
[0049] After the filtering, the level of noise in the filtered signal can be determined using one or more of a standard deviation calculator 1004 in step 906, a range calculator 1006 in step 908, an average movement per step calculator 1008 in step 910 and/or a maximum movement per step calculator 1010 in step 912. Standard deviation calculator 1004 determines the standard deviation of the filtered samples and sets the noise level to the standard deviation. Range calculator 1006 determines the difference between the largest filtered sample and the smallest filtered sample in the set of samples selected for the half-cycle and sets the noise level to the difference. Average movement per step calculator 1008 determines the average difference between successive filtered samples in the set of samples selected for the half-cycle and sets the noise level to this average difference. Max movement per step calculator 1010 determines the largest difference between successive filtered samples in the set of samples selected for the half cycle and sets the noise level to this largest difference. In some embodiments, two or more of these noise levels are combined by, for example, averaging the two or more noise levels together.
[0050] The noise levels for each half-cycle are provided to contaminant identification module 244. FIG. 11 provides a flow diagram of a method of identifying a contaminant for the noise levels in accordance with one embodiment. FIG. 12 provides a block diagram of elements used in the method of FIG. 11.
[0051] In step 1100 of FIG. 11, the noise levels are applied to a median filter 1200 which forms a window of successive noise levels, such as four successive noise levels, and selects the median of those noise levels as the noise level for the window. At step 1102, the noise levels output by median filter 1200 are applied to a low pass filter 1202 to remove high-frequency noise. At step 1104, the filtered noise levels are applied to a comparator 1204, which compares the filtered noise levels to a threshold 1206. If the filtered noise level does not exceed the threshold, the process of FIG. 11 ends at step 1112. If the filtered noise levels exceed threshold 1206 at step 1104, an alert is sent by alert generation 1212 to a host system through I/O circuit 224 and communication channel 226 at step 1106. Alternatively or additionally, the filtered noise levels are applied to a contaminant estimator 1210, which estimates the amount of contaminant in the liquid using a noise-to-contaminant function 1208 at step 1108. Noise-to- contaminant function 1208 describes the relationship between the filtered noise levels and the amount of contaminant in the liquid and can be determined from experimental data. For example, contaminant estimator 1210 can estimate an amount of gas in a liquid, an amount of oil in a liquid and/or an amount of solid particles in a liquid At step 1110, contaminant estimator 248 sends the amount of contaminant in the liquid to alert generation 1212, which forwards the amount of contaminant to the host through I/O circuit 224 and communication channel 226. In accordance with one embodiment, a single alert is sent by alert generation 1212 to convey that the liquid contains a contaminant and the amount of the contaminant in the liquid.
[0052] In accordance with a second embodiment, data collection 240 and noise identification 242 identify a noise level in the sensor signal using a frequency-domain analysis of the sensor signal. FIG. 13 shows graphs 1300, 1302, 1304, 1306, and 1308 of a Fast Fourier Transform of sensor signals from a magnetic flow meter generated from a liquid flowing at 3 feet per second and containing respective amounts of gas void fractions of 20%, 10%, 5%, 1% and 0%. In FIG. 13, the magnitude of the signal is shown along vertical axis 1310 and frequency is shown along horizontal axis 1312. As shown in FIG. 13, as the gas void fraction increases, the magnitude of the sensor signal increases across all frequencies.
[0053] To simplify identifying the contaminant’s contribution to the sensor signal, the magnitudes of the signal at harmonic frequencies of the drive frequency are ignored since those frequencies include large magnitudes due to the response of the liquid to the magnetic field. For example, FIG. 14 shows an expanded view of graph 1300 with dots positioned at each frequency that is used in the noise determination. In graph 1300, the drive frequency is 5 Hz and values at even and odd multiples of this frequency are not used to determine the noise level. Thus, at 10, 20, 30, and 40 Hz, dots are not present on graph 1300. (Note that in FIG. 14 the magnitude of the frequency-domain signal at the odd multiples exceeds the scale of the drawing, but if the magnitudes could be seen there would be no dots and no values taken at 5, 15, 25, 35, and 45 Hz.)
[0054] In general, the noise is distributed across many frequencies as indicated by the graphs of FIG. 15 where three separate graphs 1500, 1502, and 1504 of noise versus time are shown for an increase in gas void fraction from zero to thirty percent using three respective frequency bands: 2-50 Hz, 2-100 Hz, and 2-200 Hz. In FIG. 15, the magnitude of the noise is shown along vertical axis 1506 and time is shown along horizontal axis 1508. For each frequency band, the noise level increases as the amount of gas in the liquid increases. In addition, the noise level is seen to increase more for the wider band of frequencies 1504 than for the narrower band of frequencies 1500, indicating that the noise is distributed across a wide spectrum of frequencies. For the 2-200 Hz frequency band, the noise level is shown to increase 175 times for a 30% increase in gas void fraction.
[0055] Similarly, in FIG. 16, three graphs 1600, 1602 and 1604 of noise versus time show an increase in noise as the percentage of oil in a water line is increased from zero to ten percent and then to twenty percent for respective frequency bands of 2-50 Hz, 2-100 Hz, and 2-200 Hz. In FIG. 16, the magnitude of the noise is shown along vertical axis 1608 and time is shown along horizontal axis 1610. As shown in FIG. 16, the noise increases with each increase in the percentage of oil in the water line for each frequency band.
[0056] The relationship between the frequency-domain determined noise level and the gas void fraction in the liquid has also been found by the inventors to be independent of the flow rate of the liquid. For example, in FIG. 17 two graphs 1700 and 1702 are shown for two respective flow rates of three feet per second and ten feet per second. Graphs 1700 and 1702 show the relationship between noise on vertical axis 1704 and gas void fraction on horizontal axis 1706. As shown in FIG. 17, graphs 1700 and 1702 have similar slopes and intercepts, which indicates that the relationship between noise and gas void fraction is independent of flow rate.
[0057] FIG. 18 provides a graph 1800 showing a relationship between frequency-domain determined noise and a percentage of oil added to a water flow. In FIG. 18, the noise magnitude is shown along vertical axis 1802 and the oil percentage is shown along horizontal axis 1804. Graph 1800 indicates that the noise level generally increases as the percentage of oil in the water flow increases.
[0058] FIG. 19 provides a graph 1900 showing the relationship between frequency-domain determined noise and pounds of sand in a water flow. In FIG. 19, the noise magnitude is shown along vertical axis 1902 and the amount of sand is shown along horizontal axis 1904. Graph 1900 indicates that the noise level increases as the amount of sand increases.
[0059] FIG. 20 provides a flow diagram of a method used by data collection module 240 to collect data for performing frequency-domain noise level identification. FIG. 21 provides a block diagram of elements used in the method of FIG. 20.
[0060] At step 2000, analog-to-digital convertor 216 issues an interrupt indicating that a new digital sample has been produced from the magnetic flow meter sensor signal. In response, at step 2002, a decimator 2100 applies a decimation algorithm to the sample to determine if the sample should be stored in a rolling buffer 2102. The decimating algorithm selects a subset of the samples for storage in rolling buffer 2102 thereby acting as a low pass digital filter. At step 2004, a monitor 2104 determines if enough samples have been added to rolling buffer 2102 to support a Fast Fourier Transform. If more samples are needed, the process of FIG. 20 returns to step 2000 to wait for another interrupt from analog-to-digital convertor 216. If rolling buffer 2102 contains enough samples for the Fast Fourier Transform, the location of the last sample placed in rolling buffer 2102 is recorded and the noise identification module 242 is signaled to begin the noise identification task at step 2006. After step 2006, the process returns to step 2000 to wait for the next interrupt from analog-to-digital convertor 216.
[0061] FIG. 22 provides a flow diagram of a method performed by noise identification module 242 to identify the noise in the sensor signal using a frequency-domain technique. FIG. 23 provides a block diagram of elements used in the method of FIG. 22.
[0062] At step 2200, the start and end locations of the next set of data in rolling buffer 2102 to be processed are used to copy the data from rolling buffer 2102 to a selection buffer 2300. By copying these values, step 2200 is selecting a section or part of the sensor signal for conversion into the frequency domain. At step 2202, the data in selection buffer 2300 is applied to a DC filter 2302, which removes the DC component from each value of the data. In accordance with one embodiment, the DC component is simply an average of all of the data in selection buffer 2300. After the DC component has been removed from the data, the data are applied to a Hanning window 2304, which reduces the magnitudes of the data at the beginning and the end of the current section of the sensor signal to reduce frequency leakage when the Fast Fourier Transform is applied. At step 2204, the resulting data values are applied to a Fast Fourier Transform 2306, which converts the time-domain data values into a set of frequency-domain data values, with each frequency-domain data value being a complex number representing the magnitude and phase of the sensor signal for a respective frequency. At step 2206, each complex number is applied to a magnitude calculator 2308 to determine the magnitude for each frequency. At step 2208, the magnitudes are applied to a harmonic filter 2310, which removes the magnitudes for frequencies that are even or odd harmonics of the coil drive frequency. Such harmonic frequencies contain the liquid’s response to the drive signal as well as the noise in the signal due to a contaminant in the liquid. By removing the magnitudes for the harmonic frequencies, the noise due to a contaminant can be isolated from the remainder of the sensor signal. At step 2210, the filtered magnitudes are averaged by an average calculator 2312 and the average is stored in a noise buffer 2314 for the section of the sensor signal selected in step 2200.
[0063] The noise values in noise buffer 2314 are then applied to a contaminant identification module 244 in the same manner as discussed above for the time-domain noise values. In particular, the method of FIG. 11 and the block diagram of FIG. 12 can be used for the frequency-domain based noise values in the same way that they were used for the time-domain based noise values.
[0064] The various modules and functional blocks discussed above can be implemented as dedicated circuits, microcontrollers executing instructions written into one or more RAM or ROM devices within process transmitter 200 or one or more microprocessors executing instructions stored in one or more RAM or ROM devices within process transmitter 200.
[0065] In accordance with a further embodiment, the noise in the magnetic flow meter sensor signal can additionally be used to detect valve chatter. During valve chatter, a relief valve in separator 100 rapidly opens and closes causing rapid fluctuations in the pressure within separator 100. This pressure fluctuation produces a corresponding fluctuation in the speed of the flow through conduits 140 and 146. Such fluctuations in the speed of the flow appear as noise in the magnetic flow meter sensor signal. As such, isolating and measuring the noise in the sensor signal using either of the embodiments discussed above allows the valve chatter to be detected since the noise level of the sensor signal will increase dramatically during valve chatter.
[0066] Although the present invention has been described with reference to preferred embodiments, workers skilled in the art will recognize that changes may be made in form and detail without departing from the spirit and scope of the invention.

Claims

WHAT IS CLAIMED IS:
1. A magnetic flow meter comprising:
electrode sensors generating a sensor signal indicative of flow of a conductive liquid through a conduit;
a noise identification module identifying a noise level in the sensor signal; and
a contaminant identification module using the noise level to determine whether a contaminant is in the conductive liquid in the conduit.
2. The magnetic flow meter of claim 1 wherein the sensor signal comprises a periodic square wave and the magnetic flow meter further comprises a data collection module that selects samples of the sensor signal by limiting the selected samples to samples that occur at an end portion of each half-cycle of the square wave.
3. The magnetic flow meter of claim 1 wherein the sensor signal comprises a multi-step pulsed DC wave having a first frequency square wave superimposed on a second frequency square wave and wherein the magnetic flow meter further comprises a data collection module that selects samples of the sensor signal by limiting the selected samples to samples that occur at an end portion of each half-cycle of the first frequency square wave.
4. The magnetic flow meter of claim 1 wherein the sensor signal comprises a sine wave and the magnetic flow meter further comprises a data collection module that applies samples of the sensor signal to a high pass filter.
5. The magnetic flow meter of claim 1 wherein the noise identification module identifies a plurality of noise levels.
6. The magnetic flow meter of claim 5 wherein the contaminant identification module further comprises a filter that filters the plurality of noise levels to produce a filtered noise level and wherein the contaminant identification module uses the filtered noise levels to determine whether a contaminant is in the conductive liquid.
7. The magnetic flow meter of claim 1 wherein the noise identification module identifies the noise level in a frequency-domain representation of the sensor signal.
8. The magnetic flow meter of claim 7 wherein the frequency-domain representation of the sensor signal is a filtered representation wherein harmonics of a drive signal and line noise frequencies have been removed from the filtered representation.
9. The magnetic flow meter of claim 1 wherein a portion of the noise level is due to a gas contaminant.
10. The magnetic flow meter of claim 9 wherein the conductive liquid is water.
11. The magnetic flow meter of claim 1 wherein the conductive liquid is water and a portion of the noise level is due to an oil contaminant.
12. The magnetic flow meter of claim 1 wherein a portion of the noise level is due to a solid contaminant.
13. A method comprising:
applying a drive signal to generate a magnetic field in a conduit carrying a conductive liquid;
receiving a sensor signal from electrodes positioned along the conduit;
determining a noise level in the sensor signal; and
using the noise level to determine whether the conductive liquid contains a contaminant.
14. The method of claim 13 wherein determining a noise level in the sensor signal comprises converting the sensor signal to a frequency-domain representation and determining the noise level from the frequency-domain representation.
15. The method of claim 14 wherein determining the noise level from the frequency-domain representation further comprises applying the frequency-domain representation to a filter to remove values for frequencies that are harmonics of the drive signal and line noise frequencies.
16. The method of claim 13 wherein determining a noise level in the sensor signal comprises selecting samples of the sensor signal at the end of half-cycles in the sensor signal and using the selected samples to determine the noise level.
17. The method of claim 16 wherein determining the noise level further comprises determining a difference between a maximum and a minimum of the selected samples.
18. The method of claim 13 wherein determining a noise level comprises determining separate noise levels for each of a plurality of sections of the sensor signal to form a plurality of noise levels and filtering the plurality of noise levels.
19. The method of claim 13 wherein determining whether the conductive liquid contains a contaminant comprises determining whether the conductive liquid contains a gas.
20. The method of claim 13 wherein determining whether the conductive liquid contains a contaminant comprises determining whether the conductive liquid contains an oil.
21. The method of claim 13 wherein determining whether the conductive liquid contains a contaminant comprises determining whether the conductive liquid contains a solid particulate.
22. A process transmitter comprising:
a magnetic coil;
electrode sensors configured to generate a sensor signal;
a noise identification module configured to determine a level of noise in the sensor signal; and
a contaminant identification module configured to identify that a conductive liquid contains a contaminant based on the determined level of noise.
23. The process transmitter of claim 22 wherein the noise identification module is further configured to convert a section of the sensor signal to a frequency-domain representation and identifies the noise level in the frequency-domain representation.
24. The process transmitter of claim 23 wherein the noise identification module is further configured to remove values associated with line noise frequencies and harmonic frequencies of a drive signal frequency applied to the magnetic coil before identifying the noise level.
25. The process transmitter of claim 22 wherein the noise identification module is further configured to select samples of the sensor signal to use to determine the level of noise in the sensor signal, wherein the selected samples exclude samples at the beginning of half-cycles of a period signal in the sensor signal.
26. The process transmitter of claim 22 wherein the contaminant comprises gas.
27. The process transmitter of claim 22 wherein the contaminant comprises oil.
28. The process transmitter of claim 22 wherein the contaminant comprises sand.
29. A magnetic flow meter comprising:
electrode sensors generating a sensor signal indicative of flow of a conductive liquid through a conduit in a process system;
a noise identification module identifying a noise level in the sensor signal; and a valve chatter identification module using the noise level to determine whether to issue an alert indicating valve chatter in the process system.
EP19735093.7A 2018-09-06 2019-06-18 Fluid contaminant detection using noise levels in magnetic flow meter sensor signals Active EP3830527B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US16/123,495 US10935402B2 (en) 2018-09-06 2018-09-06 Fluid contaminant detection using noise levels in magnetic flow meter sensor signals
PCT/US2019/037680 WO2020050892A1 (en) 2018-09-06 2019-06-18 Fluid contaminant detection using noise levels in magnetic flow meter sensor signals

Publications (2)

Publication Number Publication Date
EP3830527A1 true EP3830527A1 (en) 2021-06-09
EP3830527B1 EP3830527B1 (en) 2023-07-26

Family

ID=67138154

Family Applications (1)

Application Number Title Priority Date Filing Date
EP19735093.7A Active EP3830527B1 (en) 2018-09-06 2019-06-18 Fluid contaminant detection using noise levels in magnetic flow meter sensor signals

Country Status (5)

Country Link
US (1) US10935402B2 (en)
EP (1) EP3830527B1 (en)
JP (1) JP7126608B2 (en)
CN (2) CN209821150U (en)
WO (1) WO2020050892A1 (en)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10935402B2 (en) * 2018-09-06 2021-03-02 Micro Motion, Inc. Fluid contaminant detection using noise levels in magnetic flow meter sensor signals
WO2021061111A1 (en) * 2019-09-25 2021-04-01 Micro Motion, Inc. Notification of events and apportioning of process data in a meter
CN111780817B (en) * 2020-06-07 2022-02-11 承德石油高等专科学校 Algorithm for detecting and processing noise signal of low-frequency excitation electromagnetic flowmeter
CA3191438A1 (en) * 2020-08-13 2022-02-17 Alarm.Com Incorporated Periodic water leak detection
DE102021208598A1 (en) * 2021-08-06 2023-02-09 Siemens Aktiengesellschaft Noisy flow measurement method, electromagnetic flowmeter and computer program product
CN113866259B (en) * 2021-12-02 2022-03-22 中国核电工程有限公司 Electromagnetic detection method and system for stainless steel pipeline weld defects
WO2024040341A1 (en) * 2022-08-22 2024-02-29 Gea Farm Technologies Canada Inc./Division Gea Houle Loading pipe, agricultural equipment provided with the same, kit for assembling, and corresponding methods of manufacturing, assembling and operating associated thereto
DE102023102673B3 (en) 2023-02-03 2024-05-16 Krohne Messtechnik Gmbh Method for operating a magnetic-inductive flow meter and a corresponding magnetic-inductive flow meter
DE102023105640B3 (en) 2023-03-07 2024-07-18 Krohne Messtechnik Gmbh Method for operating a magnetic-inductive flow meter and magnetic-inductive flow meter

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3847020A (en) * 1973-01-26 1974-11-12 J Jurschak Flow meter
JP2856521B2 (en) 1990-08-23 1999-02-10 株式会社日立製作所 Electromagnetic flow meter
JPH06300595A (en) * 1993-04-13 1994-10-28 Aichi Tokei Denki Co Ltd Electromagnetic flowmeter
JP3020772B2 (en) 1993-07-09 2000-03-15 株式会社東芝 Electromagnetic flow meter
US6505517B1 (en) * 1999-07-23 2003-01-14 Rosemount Inc. High accuracy signal processing for magnetic flowmeter
JP3915459B2 (en) 2001-09-20 2007-05-16 横河電機株式会社 Electromagnetic flow meter
DE102007015368A1 (en) * 2007-03-28 2008-10-02 Endress + Hauser Flowtec Ag Method for operating a magnetic-inductive flowmeter
DE102007052047B4 (en) * 2007-10-31 2014-06-26 Abb Ag Method and device for measuring foreign bodies in the measuring medium
GB2513678B (en) 2013-04-30 2017-02-22 Iphase Ltd Oil well system and operating method including monitoring multi-phase flow in a pipe
GB201416287D0 (en) 2014-09-15 2014-10-29 Univ Leeds Tomography apparatus, multi-phase flow monitoring system and corresponding methods
JP6229852B2 (en) * 2015-03-05 2017-11-15 横河電機株式会社 Electromagnetic flow meter
CN108828057A (en) 2018-06-26 2018-11-16 西安石油大学 A kind of oil-water two-phase flow Multi-parameter detection device and method based on electromagnetism acoustical coupling
US10935402B2 (en) * 2018-09-06 2021-03-02 Micro Motion, Inc. Fluid contaminant detection using noise levels in magnetic flow meter sensor signals

Also Published As

Publication number Publication date
JP2022500629A (en) 2022-01-04
WO2020050892A1 (en) 2020-03-12
CN110879274B (en) 2023-01-10
JP7126608B2 (en) 2022-08-26
CN110879274A (en) 2020-03-13
US10935402B2 (en) 2021-03-02
CN209821150U (en) 2019-12-20
EP3830527B1 (en) 2023-07-26
US20200080877A1 (en) 2020-03-12

Similar Documents

Publication Publication Date Title
US10935402B2 (en) Fluid contaminant detection using noise levels in magnetic flow meter sensor signals
CN104170244B (en) Submersible electric pump monitors and failure predication
CN102341720B (en) System and method for motor fault detection using stator current noise cancellation
EP1877877B1 (en) Diagnostic device for a process control system
US20190033898A1 (en) System and method for assessing sand flow rate
GB2434645A (en) Acoustic sand detection
Droubi et al. Flow noise identification using acoustic emission (AE) energy decomposition for sand monitoring in flow pipeline
CN109577957A (en) A kind of annular space flow electromagnetic measurement device and measurement method based on related transducer array
EP3140505B1 (en) Anomaly fluid detection
GB2486799A (en) Hydrocyclone wear monitoring
JP6248933B2 (en) Leakage inspection apparatus, leakage inspection method, and leakage inspection program
Liu et al. Flow regime identification for air valves failure evaluation in water pipelines using pressure data
WO2019040639A1 (en) System and method for assessing sand flow rate
EP4165390A1 (en) Systems and methods for continuous measurement of erosion and corrosion in oil and gas facilities
Durdevic et al. Operational performance of offshore de-oiling hydrocyclone systems
JP2017083292A (en) Method for determining abnormality of pipe line
Hansen et al. Comparison of Inlet Observers for a De-Oiling Gravity Separator
Li et al. Experimental study on inductive method for online material loss detection with high debris concentration
Qazi Modelling of an axial flow compact separator using neural network

Legal Events

Date Code Title Description
STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: UNKNOWN

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: THE INTERNATIONAL PUBLICATION HAS BEEN MADE

PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: REQUEST FOR EXAMINATION WAS MADE

17P Request for examination filed

Effective date: 20210302

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR

DAV Request for validation of the european patent (deleted)
DAX Request for extension of the european patent (deleted)
STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: EXAMINATION IS IN PROGRESS

17Q First examination report despatched

Effective date: 20220509

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: GRANT OF PATENT IS INTENDED

INTG Intention to grant announced

Effective date: 20230210

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: THE PATENT HAS BEEN GRANTED

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR

REG Reference to a national code

Ref country code: CH

Ref legal event code: EP

REG Reference to a national code

Ref country code: DE

Ref legal event code: R096

Ref document number: 602019033545

Country of ref document: DE

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

REG Reference to a national code

Ref country code: LT

Ref legal event code: MG9D

REG Reference to a national code

Ref country code: NL

Ref legal event code: MP

Effective date: 20230726

REG Reference to a national code

Ref country code: AT

Ref legal event code: MK05

Ref document number: 1592408

Country of ref document: AT

Kind code of ref document: T

Effective date: 20230726

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: NL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20231027

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20231126

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: RS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: PT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20231127

Ref country code: NO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20231026

Ref country code: LV

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: LT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: IS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20231126

Ref country code: HR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20231027

Ref country code: FI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: AT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: PL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: ES

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

REG Reference to a national code

Ref country code: DE

Ref legal event code: R097

Ref document number: 602019033545

Country of ref document: DE

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SM

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: RO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: ES

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: EE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: DK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: CZ

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

Ref country code: SK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20230726

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

26N No opposition filed

Effective date: 20240429

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20240521

Year of fee payment: 6