EP3802948B1 - Waschdüsenanordnung für atmosphärische diffusoren in der zellstoffherstellung - Google Patents

Waschdüsenanordnung für atmosphärische diffusoren in der zellstoffherstellung Download PDF

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Publication number
EP3802948B1
EP3802948B1 EP19735610.8A EP19735610A EP3802948B1 EP 3802948 B1 EP3802948 B1 EP 3802948B1 EP 19735610 A EP19735610 A EP 19735610A EP 3802948 B1 EP3802948 B1 EP 3802948B1
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Prior art keywords
nozzle
wash
orifice
assembly
orifice plate
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EP19735610.8A
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English (en)
French (fr)
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EP3802948A1 (de
Inventor
Paavo Tolonen
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Andritz Oy
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Andritz Oy
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    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C9/00After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
    • D21C9/02Washing ; Displacing cooking or pulp-treating liquors contained in the pulp by fluids, e.g. wash water or other pulp-treating agents
    • D21C9/04Washing ; Displacing cooking or pulp-treating liquors contained in the pulp by fluids, e.g. wash water or other pulp-treating agents in diffusers ; Washing of pulp of fluid consistency without substantially thickening

Definitions

  • the present invention relates to a wash nozzle assembly in atmospheric diffuser washers for washing cellulose pulp in the production of chemical cellulose pulp at a pulp mill.
  • the wash nozzle assembly according to the invention may be applied in all types of atmospheric diffusers used for brown stock washing, oxygen delignification and pulp bleaching.
  • the following description assumes a two-stage atmospheric brown stock diffuser following a continuous digester. Digester pressure is used to blow the pulp through the blow line into the two-stage diffusion washer.
  • the conical section of the diffuser tank is designed to allow the up-flowing stock to be evenly distributed across the diffuser.
  • Inside the diffuser tank are concentric screen rings arranged about a common vertical axis. The lower row of screen rings forms the first washing stage, and the upper row constitutes the second stage. Each washing stage consists of screen rings equally spaced. Between each screen ring there are 1-2 pcs. of wash nozzles, which are rotating in order to supply wash water or wash liquor into pulp between the screen rings.
  • Each screen ring is comprised of two screen plates spaced approximately 50-60 mm apart.
  • the number of rings per row and their height are dependent upon the design production of the diffuser and stock drainage characteristics.
  • Three, four or six arms located between the first and second stages serve to support the screen assembly and transport extracted filtrate from the screens.
  • These arms radiate from the diffuser center to the tank's outside wall, where they are supported by vertical tie rods which are coupled to hydraulic cylinders. These cylinders give the screen assembly a vertical stroking cycle.
  • the upstroke speed is adjusted to be slightly higher than the up-flow rate of the pulp mass.
  • the diffuser is held at the top of its stroke for some time, and is then down-stroked rapidly (approximately one second) in order to clean the screens from fibers.
  • the extraction flow is shut off and the wash flow reduced during the top delay and down stroke.
  • wash filtrate displaces the dirtier filtrate, which is extracted through the screens and arms to a filtrate tank.
  • First-stage extracted liquor is pumped to the cold blow pump or previous stage washer.
  • Second-stage extracted filtrate is returned to the diffuser and is used as first-stage wash filtrate.
  • Heated wash water (decker filtrate, evaporator condensate, etc.) is used for washing in the second stage. Wash filtrate/water for each stage enters the diffuser through a wide slot in the trailing edge of the wash nozzles.
  • Both first- and second-stage wash nozzles rotate with the hollow central shaft in circular paths centered between the screen rings.
  • wash filtrate flow to each of the pulp segments created by the screen rings is controlled by orifice plates in the wash nozzles and is proportional to the volume of pulp between each ring.
  • Wash nozzles for the first stage are mounted on a common arm located below the screen rings. This arm is attached to the central shaft. The central shaft serves to transport wash filtrate for both the first and second stages.
  • Second-stage wash nozzles are attached to the top scraper assembly above the screen rings.
  • a novel wash nozzle assembly for atmospheric diffusers has been developed so that it prevents pulp fibers from getting from the diffuser tank into the nozzles. This is arranged so that the orifices for adjusting the desired flow of filtrate or water are located right at the point where the wash liquid is released from the nozzle into the pulp, preferably at the trailing edge of the nozzles.
  • the orifice plate/orifice assembly may also be located elsewhere on the nozzle to release the wash liquid directly into the pulp mass.
  • the nozzle assembly according to the invention is characterized by the characterizing features of the independent claim.
  • the new nozzle type gives a significantly more even wash liquid distribution into the pulp as the liquid may be spread on the full height of the screen unit and screen area and thus displacement is more efficient. This means an improvement in the washing results.
  • a washing stage of the atmospheric diffuser consists of screen rings equally spaced and arranged about a common vertical axis.
  • the wash nozzles are arranged between the screen rings so that the nozzles supply wash liquid evenly into pulp between the screen rings.
  • the nozzle is typically vertically elongated and oblong in cross-section. It has a vertically elongated outlet opening, which is provided with an orifice plate or an orifice assembly.
  • the opening edges in the nozzle wall are provided with vertical grooves for disposing and attaching the orifice plate to the nozzle body.
  • the vertically elongated nozzle body has a first end and a second end.
  • the first end is provided with a plate-like extension for the attachment of the nozzle to a nozzle arm in the diffuser vessel.
  • the first end is open so that wash liquid can be led from the nozzle arm to the nozzle interior.
  • the elongated opening with an orifice plate starts at a distance from the first end and may extend up to the second end. The length of the elongated opening depends on the required liquid flow.
  • the nozzle moves in the direction of rotation, and so it has a leading edge, a trailing edge and side edges.
  • the orifice plate/orifice assembly is preferably located at the trailing edge. It may also be located at the leading edge, in which case a shielding element is needed in front of the leading edge so that the pulp flowing against the nozzle will not prevent the liquid outflow from the nozzle.
  • the shielding element may be a V-shaped plate.
  • the orifice plate/orifice assembly may be located at the side edge(s) of the nozzle, in which case a shielding element may also be needed.
  • the wash nozzle assembly typically comprises a nozzle, an orifice plate with or without a non-return device, which may be a lip-type non-return device.
  • a pair of lips releases a wash liquid flow from the orifice into the pulp because wash water or wash filtrate pressure opens the lips.
  • the pair of lips is closed due to the flexibility of the lips immediately once the wash flow is stopped, thereby preventing pulp from entering the nozzle.
  • the orifice is preferably either a perforated plate with small holes creating a sufficient open area for the required flow and also preventing, due to the small holes, pulp fibers from entering the nozzle, or an orifice plate with a certain number of holes having a diameter of 5-30 millimeters (mm), preferably 8-20 mm, for the flow adjustment and a lip-type non-return device for preventing fibers from entering the nozzle.
  • the size and number of the holes depend on the open area required for the desired wash liquid flow.
  • the perforated plate has a plurality of small holes with a diameter of 0.4-5 mm, typically 1-2 mm. Pulp creates a mat on the perforated plate if there is no liquid outflow. Thus, it is prevented fibers from entering the nozzle.
  • the orifice assembly may further include a non-return device comprising flexible, impervious members of complementary shapes.
  • the non-return device is formed of a pair of lips which are disposed face-to-face in surface contact, so that there is no through passage between them when the wash liquid is not introduced into the pulp. In-flowing liquid will force the lips apart to permit flow between them from the nozzle through the orifice plate holes to the pulp. Flow in the opposite direction is prevented by the close surface contact between the lips.
  • the mutually contacting lips prevent fiber flow between them towards the holes and the interior of the nozzle, but the liquid entering the pulp can force the lips apart and flow between them.
  • the lips are typically made of a thin plate of hardened stainless steel and fixed to the orifice plate with screws or corresponding fastening means.
  • the lips may also be made of plastic or another flexible material.
  • the orifice plate may also have a slot or slots whose size is sufficient for a certain wash liquid flow.
  • the wash nozzle may also have an orifice assembly comprising a plurality of non-return valves attached to the orifice plate, which valves prevent fibers from entering the nozzle.
  • the non-return valves may be commercial products or prepared for the new nozzle.
  • the wash nozzle wall has preferably vertical grooves, typically two, for an orifice plate/orifice assembly and a locking plate and screws for keeping said plate/assembly in place.
  • the new wash nozzle assembly gives a better washing result, because the wash liquid is distributed more evenly into the pulp and the displacement of the dirty liquor is therefore improved.
  • the new wash nozzle assembly significantly reduces the cleaning and replacement time of nozzles in two ways. Firstly, the nozzles are kept clean for a long time as they cannot be clogged by the pulp from the diffuser tank. Secondly, the orifice plates/orifice assemblies are detachable from the nozzle body and, therefore, easy to withdraw out of the nozzles. Thus, the possible cleaning of nozzles can be done without detaching the whole heavy nozzles. These are the significant advantages which decrease the downtime needed.
  • the new wash nozzle is similar for all stages of diffuser washers and acts as the lower and upper nozzle. It can also be used in a one-stage diffuser.
  • the new wash nozzle assembly can be installed without any changes for all types of existing nozzle arms by replacing the existing nozzles.
  • the nozzles are arranged in an atmospheric diffuser, which typically comprises a generally upright vessel with a central vertical shaft; a plurality of annular screens which have been mounted concentric with the central vertical shaft; and an arm assembly which has been mounted vertically spaced from the screens.
  • the arm assembly is connected to the central shaft and is rotated by the shaft.
  • the vertically elongated nozzles are connected to the arm assembly. The nozzles are moved by the shaft in the direction of rotation between the screens, and they introduce wash liquid into the pulp between the screens.
  • Fig. 1 shows an exemplary atmospheric diffuser in which the present invention may be applied.
  • the diffuser is shown generally by reference numeral 1.
  • the conventional components of the diffuser 1 include a generally upright vessel having a pulp inlet 3 at the bottom and a pulp outlet 4 at the top.
  • Extraction arms 17 ( Fig. 2 ) are mounted within the vessel, extending radially outwardly from a central shaft 9, which defines the central vertical axis of the vessel.
  • the shaft end is connected to a conventional drive 15.
  • Outlets for displaced filtrate from the extraction arms are provided at 7 and 8.
  • the first outlet 7 is for 2nd stage filtrate and the second outlet 8 for 1st stage filtrate.
  • a hydraulic cylinder 14, or a similar mechanism, is provided to effect up and down reciprocation of the extraction arms 17.
  • the reciprocation is essentially at the pulp flow velocity in the direction 19 of pulp flow movement, and at a much higher speed opposite to the direction of pulp flow, as is conventional.
  • a back flush tank is illustrated with reference number 18 and
  • first and second screens 2 Figs. 1 and 2
  • first and second screens 2 Figs. 1 and 2
  • the shaft 9, to which the arm assembly 10 is connected is driven by a motor connected to the drive end, so that the arm assembly 10 rotates in the first direction of rotation, shown by arrows 19 in Fig. 2 .
  • a plurality of treatment fluid introducing nozzles 11 Connected to the arm assembly 10 is a plurality of treatment fluid introducing nozzles 11, which are vertically elongated and disposed between the screens 2.
  • the nozzles 11 are typically oblong in cross-section 22 (see Fig. 4 ), and at the second end thereof, remote from the arm assembly 10, have means of defining at least one fluid introducing opening 23, typically at the side of the nozzle 11 that trails as the nozzle 11 moves in the direction of rotation 19.
  • Washing liquid is supplied to the nozzles 11 from a conduit 5 ( Fig. 1 ), which extends interiorly of the shaft 9, and to the rotating arms 10, the treatment liquid - typically wash liquid or bleach liquid - flowing through the arm assembly 10 and then to nozzles 11, to be introduced through the openings, as shown by arrows 5'.
  • a second conduit 6 is provided for introducing a second washing fluid, that liquid flowing through a conduit within the shaft 9 to the arm assembly 12 to which the nozzles 13 are mounted.
  • the nozzles 13 for introducing wash liquid 6' are disposed between the bottom set of annular screens 2 and the arm 12, which is located below the lower screens 2. Both first- and second-stage wash nozzles 11, 13 rotate with the hollow central shaft 9 in circular paths centered between the screen rings.
  • Heated wash water (filtrate, evaporator condensate, etc.) is typically used for washing in the second stage. Wash filtrate/water for each stage enters the diffuser through a wide slot 20 in the trailing edge of the wash nozzles 11, 13 ( Fig. 2 ). The wash filtrate flow to each of the pulp segments created by the screen rings is controlled by orifice plates in the wash nozzles and is proportional to the volume of pulp between each ring.
  • Figs. 3-5 show the details of known nozzles.
  • the lower nozzle 13 is elongated and oblong in cross-section 22 ( Fig. 3 ).
  • the nozzle has a first end 13a and a second end 13b.
  • the wash liquid flows through the first end into the nozzle and is discharged from the nozzle through a slot 24 located at distances from the first end and the second end.
  • Fig. 4 shows the upper nozzle 11, which is also elongated and oblong in cross-section, and it has a first end and a second end.
  • the wash liquid flows through the first end into the nozzle and is discharged through a slot 23, which is located at the second end, as shown by arrows 6'.
  • the nozzles are attached to the nozzle arms so that there is an orifice plate 25 between the nozzle and the arm.
  • the orifice plate 25 has holes 26, the cross-sectional area of which is predetermined in relation to the desired liquid flow passing through the nozzle. This way, the liquid flow is adjusted.
  • Fig. 6 illustrates how the lower nozzle 13 is attached to the arm 12.
  • the orifice plate 25 is located between the nozzle 13 and the arm 12, to which arm the nozzle will be attached.
  • the wash liquid 6' flows from the arm 12 through the orifice plate holes to the nozzle 13.
  • the first end of the nozzle is provided with a plate-like extension 21 for the attachment ( Figs. 3, 4 and 6 ).
  • the upper nozzle 11 is connected to the arm 10 in the corresponding way.
  • a problem with the known wash nozzles is their tendency to become clogged by fibers coming from the diffuser tank and entering backwards into the nozzles. This can be avoided by using a nozzle according to the present invention shown in Figs. 7 -16, which illustrate a lower nozzle of the two-stage diffuser, but an upper nozzle may have the same configuration.
  • a nozzle 27 is elongated and oblong in cross-section. It has a vertically elongated opening 38, which is provided with an orifice plate 28 having a plurality of holes for introducing wash liquid into the pulp.
  • the diameter of the holes is 5-35 millimeters (mm), preferably 8-20 mm. The size and number of the holes depend on the open area required for the desired wash liquid flow.
  • the orifice assembly further includes a non-return device 30 comprising flexible, impervious members of complementary shapes.
  • the non-return device is formed of a pair of lips which are disposed face-to-face in surface contact, so that there is no through passage between them when the wash liquid is not introduced into the pulp. In-flowing liquid will force the lips 35 ( Fig. 10 and 11 ) apart to permit flow between them from the nozzle through the orifice plate holes to the pulp. Flow in the opposite direction is prevented by the close surface contact between the lips.
  • the mutually contacting lips prevent fiber flow between them towards the holes and the interior of the nozzle, but the liquid entering the pulp can force the lips apart and flow between them.
  • the opening edges in the nozzle wall are provided with vertical grooves 34 for disposing and attaching the orifice plate 28 to the nozzle body 27 ( Fig. 8 ).
  • the lips 30 are attached to the orifice plate with screws 29 or corresponding fastening means.
  • the orifice plate assembly is locked into place by means of a locking plate 31 and locking screws 32.
  • the nozzle body 27 has a first end 27a and a second end 27b.
  • the first end is provided with a plate-like extension for the attachment of the nozzle to the nozzle arm, such as the arm 12 in Fig. 1 .
  • the first end is open for leading wash liquid from the nozzle arm to the nozzle interior.
  • the elongated opening 38 with the orifice plate 28 starts at a distance from the first end 27a and extends up to the second end 27b. The length of the elongated opening may be shorter depending on the required liquid flow.
  • Fig. 9 shows the orifice plate/lip assembly when it is withdrawn partially out.
  • the orifice plate with or without lips may simply be removed from the nozzle if there is any need for cleaning or replacing them with new ones.
  • Fig. 10 shows a top view of the orifice plate/lip assembly at the trailing edge of the nozzle.
  • the orifice plate has been disposed in the grooves in the wall of the nozzle body 27. Wash liquid flows through the hole 28 of the orifice plate and further from between the two mutually opposite lips 35, as shown with arrows 33. This way, the wash liquid is introduced evenly along the length of the nozzle to the pulp, as illustrated in Fig. 7 .
  • Fig. 11 shows an embodiment in which the orifice assembly 28, 35 is located at the leading edge of the nozzle 27.
  • the nozzle is provided with a shielding element, which is a V-shaped plate 40. It is attached to the nozzle so that there is a gap between the plate and the nozzle. Wash liquid flows from the nozzle and through the gap into the pulp, as shown with arrows 33'.
  • the shielding element may be needed in front of the leading edge so that the pulp flowing against the nozzle will not prevent the outflow of the liquid from the nozzle.
  • Figs. 12 shows another embodiment of the new nozzle.
  • the orifice plate is a perforated plate 36.
  • the holes of the plate are smaller than those in the embodiment of Figs. 7-11 so that their diameter is 0.4-5 mm, typically 1-2 mm, creating a sufficient open area for the required flow. Such small holes prevent pulp fibers from entering the nozzle.
  • Figs. 13 and 14 show yet another embodiment of the new nozzle 27.
  • the orifice plate is provided with a plurality of non-return valves 37, which allow the wash liquid to flow in only one direction. This way, any clogging caused by pulp fibers may be prevented.
  • Fig. 15 illustrates a wash liquid distribution to diffuser screens 2 by using the prior art nozzle 13 and the new nozzle 27.
  • the new nozzle distributes wash liquid 33 more evenly along the screen height 39 and the screen area, whereas the known nozzle is only able to distribute wash liquid to a smaller area.
  • the new nozzle type gives a significantly more even wash liquid distribution into the pulp, thereby making the displacement washing of pulp more efficient. This improves the washing results.

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Paper (AREA)
  • Nozzles (AREA)

Claims (11)

  1. Düsenanordnung zur Einleitung von Waschflüssigkeit für einen atmosphärischen Diffusor, wobei die Anordnung eine längliche vertikale Düse (27) umfasst, dadurch gekennzeichnet, dass die Düsenwand eine längliche Öffnung (38) aufweist, die mit einer Öffnungsplatte (28) oder einer Öffnungsanordnung, umfassend eine Öffnungsplatte, bereitgestellt ist, um Flüssigkeit aus der Düse (27) abzugeben.
  2. Waschdüsenanordnung nach Anspruch 1, wobei die Öffnungsplatte (28) einen offenen Bereich zum Einleiten eines vorbestimmten Stroms der Waschflüssigkeit aus der Düse in Zellstoff in dem Diffusorgefäß aufweist.
  3. Waschdüsenanordnung nach Anspruch 1 oder 2, wobei die Düse Nuten (34) in der Düsenwand zur Befestigung der Öffnungsplatte / Öffnungsanordnung aufweist.
  4. Waschdüsenanordnung nach Anspruch 1, 2 oder 3, wobei die Öffnungsanordnung eine Öffnungsplatte mit einer Vielzahl von Löchern mit einem Durchmesser von 5-35 mm, bevorzugt 8-20 mm, und eine Lippenart (35) von Nicht-Rücklaufvorrichtung (30) aufweist.
  5. Waschdüsenanordnung nach Anspruch 1, 2 oder 3, wobei die Öffnungsanordnung eine Öffnungsplatte mit einem Schlitz oder Schlitzen mit einer ausreichenden Größe für erforderlichen Waschstrom und Lippenart von Nicht-Rücklaufvorrichtung (30) umfasst.
  6. Waschdüsenanordnung nach Anspruch 1, 2 oder 3, wobei die Öffnungsplatte aus einer perforierten Platte (36) mit einer Vielzahl von Löchern mit einem Durchmesser von 0,4-5 mm, typischerweise 1-2 mm, gebildet ist.
  7. Waschdüsenanordnung nach Anspruch 1, 2 oder 3, wobei die Öffnungsanordnung eine Öffnungsplatte mit einer Vielzahl von Nicht-Rücklauf Rückschlagventilen (37) umfasst.
  8. Waschdüsenanordnung nach einem der Ansprüche 1-7, wobei die Düse eine Vorderkante, eine Hinterkante und Seitenkanten aufweist und die Öffnungsplatte / Öffnungsanordnung an der Hinterkante der Düse angeordnet ist.
  9. Waschdüsenanordnung nach einem der Ansprüche 1-7, wobei die Düse eine Vorderkante, eine Hinterkante und Seitenkanten aufweist und die Öffnungsplatte / Öffnungsanordnung an der Vorderkante der Düse angeordnet ist.
  10. Waschdüsenanordnung nach einem der Ansprüche 1-7, wobei die Düse eine Vorderkante, eine Hinterkante und Seitenkanten aufweist und die Öffnungsplatte / Öffnungsanordnung an einer Seitenkante der Düse angeordnet ist.
  11. Waschdüsenanordnung nach einem der vorhergehenden Ansprüche, wobei die Düse eine Düse für eine Waschstufe des atmosphärischen Diffusors ist.
EP19735610.8A 2018-06-08 2019-06-07 Waschdüsenanordnung für atmosphärische diffusoren in der zellstoffherstellung Active EP3802948B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI20185526A FI129135B (en) 2018-06-08 2018-06-08 WASH NOZZLE ASSEMBLY FOR ATMOSPHERIC DIFFUSORS IN MASS MANUFACTURE
PCT/FI2019/050445 WO2019234306A1 (en) 2018-06-08 2019-06-07 Wash nozzle assembly for atmospheric diffusers in pulp production

Publications (2)

Publication Number Publication Date
EP3802948A1 EP3802948A1 (de) 2021-04-14
EP3802948B1 true EP3802948B1 (de) 2023-02-22

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Application Number Title Priority Date Filing Date
EP19735610.8A Active EP3802948B1 (de) 2018-06-08 2019-06-07 Waschdüsenanordnung für atmosphärische diffusoren in der zellstoffherstellung

Country Status (4)

Country Link
EP (1) EP3802948B1 (de)
JP (1) JP7495357B2 (de)
FI (2) FI129135B (de)
WO (1) WO2019234306A1 (de)

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02175985A (ja) * 1988-12-26 1990-07-09 Mitsubishi Paper Mills Ltd フィルター用洗浄シャワー
SE501863C2 (sv) * 1993-09-22 1995-06-06 Kvaerner Pulping Tech Anordning för fördelning av tvättvätska för tvättning av pappersmassa
SE502274E (sv) * 1994-01-24 1999-08-09 Kvaerner Pulping Tech Diffusör samt packbox avsedd att mottaga en stång för höjning och sänkning av ett silpaket hos en sådan diffusör
US6892969B2 (en) 2001-06-05 2005-05-17 Oramac, Inc. Pulp washing shower
US20150034733A1 (en) 2013-08-02 2015-02-05 Andritz Inc. Assembly for washer shower pipe and method to adjust open area of orifices in the pipe

Also Published As

Publication number Publication date
JP7495357B2 (ja) 2024-06-04
FI20185526A1 (en) 2019-12-09
FI3802948T3 (fi) 2023-05-16
FI129135B (en) 2021-08-13
JP2021527174A (ja) 2021-10-11
WO2019234306A1 (en) 2019-12-12
EP3802948A1 (de) 2021-04-14

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