EP3722405A1 - Composition solide contenant du parfum - Google Patents
Composition solide contenant du parfum Download PDFInfo
- Publication number
- EP3722405A1 EP3722405A1 EP19168929.8A EP19168929A EP3722405A1 EP 3722405 A1 EP3722405 A1 EP 3722405A1 EP 19168929 A EP19168929 A EP 19168929A EP 3722405 A1 EP3722405 A1 EP 3722405A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- weight
- composition
- composition according
- water
- fragrance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 246
- 239000002304 perfume Substances 0.000 title claims description 15
- 239000003205 fragrance Substances 0.000 claims abstract description 83
- 239000004753 textile Substances 0.000 claims abstract description 72
- 150000001875 compounds Chemical class 0.000 claims abstract description 57
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 53
- 239000007787 solid Substances 0.000 claims abstract description 42
- 239000012876 carrier material Substances 0.000 claims abstract description 26
- 150000003839 salts Chemical class 0.000 claims abstract description 21
- 238000000034 method Methods 0.000 claims abstract description 10
- 239000012047 saturated solution Substances 0.000 claims abstract description 8
- 239000006254 rheological additive Substances 0.000 claims description 42
- 235000017281 sodium acetate Nutrition 0.000 claims description 31
- 239000000126 substance Substances 0.000 claims description 29
- 238000005406 washing Methods 0.000 claims description 21
- BDKLKNJTMLIAFE-UHFFFAOYSA-N 2-(3-fluorophenyl)-1,3-oxazole-4-carbaldehyde Chemical compound FC1=CC=CC(C=2OC=C(C=O)N=2)=C1 BDKLKNJTMLIAFE-UHFFFAOYSA-N 0.000 claims description 16
- 229940087562 sodium acetate trihydrate Drugs 0.000 claims description 16
- 229920001296 polysiloxane Polymers 0.000 claims description 10
- 235000012216 bentonite Nutrition 0.000 claims description 9
- 239000011734 sodium Substances 0.000 claims description 9
- 239000002775 capsule Substances 0.000 claims description 8
- 239000003960 organic solvent Substances 0.000 claims description 8
- 229920006317 cationic polymer Polymers 0.000 claims description 6
- 239000002280 amphoteric surfactant Substances 0.000 claims description 4
- 239000003093 cationic surfactant Substances 0.000 claims description 4
- 229920013822 aminosilicone Polymers 0.000 claims description 3
- 229910052615 phyllosilicate Inorganic materials 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 230000008569 process Effects 0.000 abstract description 4
- 239000003921 oil Substances 0.000 description 40
- 235000019198 oils Nutrition 0.000 description 40
- -1 iso-damascone Chemical compound 0.000 description 32
- 239000000049 pigment Substances 0.000 description 26
- 239000000975 dye Substances 0.000 description 21
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 20
- 239000000155 melt Substances 0.000 description 20
- 239000002245 particle Substances 0.000 description 18
- 239000001632 sodium acetate Substances 0.000 description 15
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 14
- 239000003795 chemical substances by application Substances 0.000 description 14
- LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical compound OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 description 14
- 239000006185 dispersion Substances 0.000 description 13
- 229920002678 cellulose Polymers 0.000 description 12
- 235000010980 cellulose Nutrition 0.000 description 12
- 239000012459 cleaning agent Substances 0.000 description 12
- 239000007788 liquid Substances 0.000 description 12
- 238000001816 cooling Methods 0.000 description 11
- 230000000694 effects Effects 0.000 description 11
- 239000002202 Polyethylene glycol Substances 0.000 description 10
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 10
- 229920001223 polyethylene glycol Polymers 0.000 description 10
- 239000000243 solution Substances 0.000 description 10
- 230000000875 corresponding effect Effects 0.000 description 9
- 229910000831 Steel Inorganic materials 0.000 description 8
- 239000000872 buffer Substances 0.000 description 8
- 239000001913 cellulose Substances 0.000 description 8
- XCJYREBRNVKWGJ-UHFFFAOYSA-N copper(II) phthalocyanine Chemical compound [Cu+2].C12=CC=CC=C2C(N=C2[N-]C(C3=CC=CC=C32)=N2)=NC1=NC([C]1C=CC=CC1=1)=NC=1N=C1[C]3C=CC=CC3=C2[N-]1 XCJYREBRNVKWGJ-UHFFFAOYSA-N 0.000 description 8
- ZRSNZINYAWTAHE-UHFFFAOYSA-N p-methoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C=C1 ZRSNZINYAWTAHE-UHFFFAOYSA-N 0.000 description 8
- FZUOVNMHEAPVBW-UHFFFAOYSA-L quinoline yellow ws Chemical compound [Na+].[Na+].O=C1C2=CC=CC=C2C(=O)C1C1=NC2=C(S([O-])(=O)=O)C=C(S(=O)(=O)[O-])C=C2C=C1 FZUOVNMHEAPVBW-UHFFFAOYSA-L 0.000 description 8
- 239000010959 steel Substances 0.000 description 8
- OSCJHTSDLYVCQC-UHFFFAOYSA-N 2-ethylhexyl 4-[[4-[4-(tert-butylcarbamoyl)anilino]-6-[4-(2-ethylhexoxycarbonyl)anilino]-1,3,5-triazin-2-yl]amino]benzoate Chemical compound C1=CC(C(=O)OCC(CC)CCCC)=CC=C1NC1=NC(NC=2C=CC(=CC=2)C(=O)NC(C)(C)C)=NC(NC=2C=CC(=CC=2)C(=O)OCC(CC)CCCC)=N1 OSCJHTSDLYVCQC-UHFFFAOYSA-N 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 7
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 7
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 7
- VWTINHYPRWEBQY-UHFFFAOYSA-N denatonium Chemical compound [O-]C(=O)C1=CC=CC=C1.C=1C=CC=CC=1C[N+](CC)(CC)CC(=O)NC1=C(C)C=CC=C1C VWTINHYPRWEBQY-UHFFFAOYSA-N 0.000 description 7
- 239000004744 fabric Substances 0.000 description 7
- 239000003094 microcapsule Substances 0.000 description 7
- 239000008247 solid mixture Substances 0.000 description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
- 125000000217 alkyl group Chemical group 0.000 description 6
- 230000001580 bacterial effect Effects 0.000 description 6
- 239000007853 buffer solution Substances 0.000 description 6
- 239000013078 crystal Substances 0.000 description 6
- 150000002148 esters Chemical class 0.000 description 6
- MTZQAGJQAFMTAQ-UHFFFAOYSA-N ethyl benzoate Chemical compound CCOC(=O)C1=CC=CC=C1 MTZQAGJQAFMTAQ-UHFFFAOYSA-N 0.000 description 6
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 6
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 6
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 6
- 239000007937 lozenge Substances 0.000 description 6
- ZWRUINPWMLAQRD-UHFFFAOYSA-N nonan-1-ol Chemical compound CCCCCCCCCO ZWRUINPWMLAQRD-UHFFFAOYSA-N 0.000 description 6
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 6
- UJMBCXLDXJUMFB-GLCFPVLVSA-K tartrazine Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-GLCFPVLVSA-K 0.000 description 6
- SWGJCIMEBVHMTA-UHFFFAOYSA-K trisodium;6-oxido-4-sulfo-5-[(4-sulfonatonaphthalen-1-yl)diazenyl]naphthalene-2-sulfonate Chemical compound [Na+].[Na+].[Na+].C1=CC=C2C(N=NC3=C4C(=CC(=CC4=CC=C3O)S([O-])(=O)=O)S([O-])(=O)=O)=CC=C(S([O-])(=O)=O)C2=C1 SWGJCIMEBVHMTA-UHFFFAOYSA-K 0.000 description 6
- YGFGZTXGYTUXBA-UHFFFAOYSA-N (±)-2,6-dimethyl-5-heptenal Chemical compound O=CC(C)CCC=C(C)C YGFGZTXGYTUXBA-UHFFFAOYSA-N 0.000 description 5
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 5
- QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 description 5
- 235000019445 benzyl alcohol Nutrition 0.000 description 5
- 239000011248 coating agent Substances 0.000 description 5
- 239000003599 detergent Substances 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 235000012752 quinoline yellow Nutrition 0.000 description 5
- 238000007711 solidification Methods 0.000 description 5
- 230000008023 solidification Effects 0.000 description 5
- 235000012756 tartrazine Nutrition 0.000 description 5
- 239000004149 tartrazine Substances 0.000 description 5
- 125000000954 2-hydroxyethyl group Chemical group [H]C([*])([H])C([H])([H])O[H] 0.000 description 4
- NFAVNWJJYQAGNB-UHFFFAOYSA-N 2-methylundecanal Chemical compound CCCCCCCCCC(C)C=O NFAVNWJJYQAGNB-UHFFFAOYSA-N 0.000 description 4
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 4
- IHZXTIBMKNSJCJ-UHFFFAOYSA-N 3-{[(4-{[4-(dimethylamino)phenyl](4-{ethyl[(3-sulfophenyl)methyl]amino}phenyl)methylidene}cyclohexa-2,5-dien-1-ylidene)(ethyl)azaniumyl]methyl}benzene-1-sulfonate Chemical compound C=1C=C(C(=C2C=CC(C=C2)=[N+](C)C)C=2C=CC(=CC=2)N(CC)CC=2C=C(C=CC=2)S([O-])(=O)=O)C=CC=1N(CC)CC1=CC=CC(S(O)(=O)=O)=C1 IHZXTIBMKNSJCJ-UHFFFAOYSA-N 0.000 description 4
- NTPLXRHDUXRPNE-UHFFFAOYSA-N 4-methoxyacetophenone Chemical compound COC1=CC=C(C(C)=O)C=C1 NTPLXRHDUXRPNE-UHFFFAOYSA-N 0.000 description 4
- KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 4
- RTMBGDBBDQKNNZ-UHFFFAOYSA-L C.I. Acid Blue 3 Chemical compound [Ca+2].C1=CC(N(CC)CC)=CC=C1C(C=1C(=CC(=C(O)C=1)S([O-])(=O)=O)S([O-])(=O)=O)=C1C=CC(=[N+](CC)CC)C=C1.C1=CC(N(CC)CC)=CC=C1C(C=1C(=CC(=C(O)C=1)S([O-])(=O)=O)S([O-])(=O)=O)=C1C=CC(=[N+](CC)CC)C=C1 RTMBGDBBDQKNNZ-UHFFFAOYSA-L 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- LHXDLQBQYFFVNW-UHFFFAOYSA-N Fenchone Chemical compound C1CC2(C)C(=O)C(C)(C)C1C2 LHXDLQBQYFFVNW-UHFFFAOYSA-N 0.000 description 4
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 239000013543 active substance Substances 0.000 description 4
- 150000001299 aldehydes Chemical class 0.000 description 4
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 4
- AKGGYBADQZYZPD-UHFFFAOYSA-N benzylacetone Chemical compound CC(=O)CCC1=CC=CC=C1 AKGGYBADQZYZPD-UHFFFAOYSA-N 0.000 description 4
- OIQPTROHQCGFEF-UHFFFAOYSA-L chembl1371409 Chemical compound [Na+].[Na+].OC1=CC=C2C=C(S([O-])(=O)=O)C=CC2=C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 OIQPTROHQCGFEF-UHFFFAOYSA-L 0.000 description 4
- 238000000576 coating method Methods 0.000 description 4
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 description 4
- HFJRKMMYBMWEAD-UHFFFAOYSA-N dodecanal Chemical compound CCCCCCCCCCCC=O HFJRKMMYBMWEAD-UHFFFAOYSA-N 0.000 description 4
- CBOQJANXLMLOSS-UHFFFAOYSA-N ethyl vanillin Chemical compound CCOC1=CC(C=O)=CC=C1O CBOQJANXLMLOSS-UHFFFAOYSA-N 0.000 description 4
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 description 4
- 230000006870 function Effects 0.000 description 4
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 4
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 4
- UWKAYLJWKGQEPM-LBPRGKRZSA-N linalyl acetate Chemical compound CC(C)=CCC[C@](C)(C=C)OC(C)=O UWKAYLJWKGQEPM-LBPRGKRZSA-N 0.000 description 4
- SXQCTESRRZBPHJ-UHFFFAOYSA-M lissamine rhodamine Chemical compound [Na+].C=12C=CC(=[N+](CC)CC)C=C2OC2=CC(N(CC)CC)=CC=C2C=1C1=CC=C(S([O-])(=O)=O)C=C1S([O-])(=O)=O SXQCTESRRZBPHJ-UHFFFAOYSA-M 0.000 description 4
- 235000019645 odor Nutrition 0.000 description 4
- 150000002892 organic cations Chemical class 0.000 description 4
- 235000012736 patent blue V Nutrition 0.000 description 4
- DTUQWGWMVIHBKE-UHFFFAOYSA-N phenylacetaldehyde Chemical compound O=CCC1=CC=CC=C1 DTUQWGWMVIHBKE-UHFFFAOYSA-N 0.000 description 4
- SATCULPHIDQDRE-UHFFFAOYSA-N piperonal Chemical compound O=CC1=CC=C2OCOC2=C1 SATCULPHIDQDRE-UHFFFAOYSA-N 0.000 description 4
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 4
- 150000003856 quaternary ammonium compounds Chemical class 0.000 description 4
- 230000003068 static effect Effects 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- MGSRCZKZVOBKFT-UHFFFAOYSA-N thymol Chemical compound CC(C)C1=CC=C(C)C=C1O MGSRCZKZVOBKFT-UHFFFAOYSA-N 0.000 description 4
- 150000004684 trihydrates Chemical class 0.000 description 4
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 description 4
- 235000013311 vegetables Nutrition 0.000 description 4
- 229920003169 water-soluble polymer Polymers 0.000 description 4
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 3
- UEGBWDUVDAKUGA-UHFFFAOYSA-N 2,6,10-trimethylundec-9-enal Chemical compound CC(C)=CCCC(C)CCCC(C)C=O UEGBWDUVDAKUGA-UHFFFAOYSA-N 0.000 description 3
- XSAYZAUNJMRRIR-UHFFFAOYSA-N 2-acetylnaphthalene Chemical compound C1=CC=CC2=CC(C(=O)C)=CC=C21 XSAYZAUNJMRRIR-UHFFFAOYSA-N 0.000 description 3
- PUAQLLVFLMYYJJ-UHFFFAOYSA-N 2-aminopropiophenone Chemical compound CC(N)C(=O)C1=CC=CC=C1 PUAQLLVFLMYYJJ-UHFFFAOYSA-N 0.000 description 3
- PRNCMAKCNVRZFX-UHFFFAOYSA-N 3,7-dimethyloctan-1-ol Chemical compound CC(C)CCCC(C)CCO PRNCMAKCNVRZFX-UHFFFAOYSA-N 0.000 description 3
- ORMHZBNNECIKOH-UHFFFAOYSA-N 4-(4-hydroxy-4-methylpentyl)cyclohex-3-ene-1-carbaldehyde Chemical compound CC(C)(O)CCCC1=CCC(C=O)CC1 ORMHZBNNECIKOH-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 3
- 244000223760 Cinnamomum zeylanicum Species 0.000 description 3
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 3
- HMEKVHWROSNWPD-UHFFFAOYSA-N Erioglaucine A Chemical compound [NH4+].[NH4+].C=1C=C(C(=C2C=CC(C=C2)=[N+](CC)CC=2C=C(C=CC=2)S([O-])(=O)=O)C=2C(=CC=CC=2)S([O-])(=O)=O)C=CC=1N(CC)CC1=CC=CC(S([O-])(=O)=O)=C1 HMEKVHWROSNWPD-UHFFFAOYSA-N 0.000 description 3
- 229920002444 Exopolysaccharide Polymers 0.000 description 3
- LCTONWCANYUPML-UHFFFAOYSA-M Pyruvate Chemical compound CC(=O)C([O-])=O LCTONWCANYUPML-UHFFFAOYSA-M 0.000 description 3
- 150000001450 anions Chemical class 0.000 description 3
- 239000000440 bentonite Substances 0.000 description 3
- 229910000278 bentonite Inorganic materials 0.000 description 3
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 3
- 229940007550 benzyl acetate Drugs 0.000 description 3
- 235000017803 cinnamon Nutrition 0.000 description 3
- NEHNMFOYXAPHSD-UHFFFAOYSA-N citronellal Chemical compound O=CCC(C)CCC=C(C)C NEHNMFOYXAPHSD-UHFFFAOYSA-N 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- KSMVZQYAVGTKIV-UHFFFAOYSA-N decanal Chemical compound CCCCCCCCCC=O KSMVZQYAVGTKIV-UHFFFAOYSA-N 0.000 description 3
- PXEDJBXQKAGXNJ-QTNFYWBSSA-L disodium L-glutamate Chemical compound [Na+].[Na+].[O-]C(=O)[C@@H](N)CCC([O-])=O PXEDJBXQKAGXNJ-QTNFYWBSSA-L 0.000 description 3
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 description 3
- 150000002170 ethers Chemical class 0.000 description 3
- 238000000855 fermentation Methods 0.000 description 3
- 230000004151 fermentation Effects 0.000 description 3
- 235000011187 glycerol Nutrition 0.000 description 3
- WPFVBOQKRVRMJB-UHFFFAOYSA-N hydroxycitronellal Chemical compound O=CCC(C)CCCC(C)(C)O WPFVBOQKRVRMJB-UHFFFAOYSA-N 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 3
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 3
- 150000002576 ketones Chemical class 0.000 description 3
- 229940041616 menthol Drugs 0.000 description 3
- 150000004702 methyl esters Chemical class 0.000 description 3
- 235000013923 monosodium glutamate Nutrition 0.000 description 3
- 229910052901 montmorillonite Inorganic materials 0.000 description 3
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 3
- 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 3
- GYHFUZHODSMOHU-UHFFFAOYSA-N nonanal Chemical compound CCCCCCCCC=O GYHFUZHODSMOHU-UHFFFAOYSA-N 0.000 description 3
- BOPPSUHPZARXTH-UHFFFAOYSA-N ocean propanal Chemical compound O=CC(C)CC1=CC=C2OCOC2=C1 BOPPSUHPZARXTH-UHFFFAOYSA-N 0.000 description 3
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 3
- 229960004889 salicylic acid Drugs 0.000 description 3
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 3
- 235000017557 sodium bicarbonate Nutrition 0.000 description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 description 3
- 229940073490 sodium glutamate Drugs 0.000 description 3
- WTWSHHITWMVLBX-DKWTVANSSA-M sodium;(2s)-2-aminobutanedioate;hydron Chemical compound [Na+].[O-]C(=O)[C@@H](N)CC(O)=O WTWSHHITWMVLBX-DKWTVANSSA-M 0.000 description 3
- KYWIYKKSMDLRDC-UHFFFAOYSA-N undecan-2-one Chemical compound CCCCCCCCCC(C)=O KYWIYKKSMDLRDC-UHFFFAOYSA-N 0.000 description 3
- KMPQYAYAQWNLME-UHFFFAOYSA-N undecanal Chemical compound CCCCCCCCCCC=O KMPQYAYAQWNLME-UHFFFAOYSA-N 0.000 description 3
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 description 3
- 235000012141 vanillin Nutrition 0.000 description 3
- ZFNVDHOSLNRHNN-UHFFFAOYSA-N xi-3-(4-Isopropylphenyl)-2-methylpropanal Chemical compound O=CC(C)CC1=CC=C(C(C)C)C=C1 ZFNVDHOSLNRHNN-UHFFFAOYSA-N 0.000 description 3
- LHXDLQBQYFFVNW-XCBNKYQSSA-N (+)-Fenchone Natural products C1C[C@]2(C)C(=O)C(C)(C)[C@H]1C2 LHXDLQBQYFFVNW-XCBNKYQSSA-N 0.000 description 2
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 description 2
- NFLGAXVYCFJBMK-RKDXNWHRSA-N (+)-isomenthone Natural products CC(C)[C@H]1CC[C@@H](C)CC1=O NFLGAXVYCFJBMK-RKDXNWHRSA-N 0.000 description 2
- CRDAMVZIKSXKFV-FBXUGWQNSA-N (2-cis,6-cis)-farnesol Chemical compound CC(C)=CCC\C(C)=C/CC\C(C)=C/CO CRDAMVZIKSXKFV-FBXUGWQNSA-N 0.000 description 2
- MBDOYVRWFFCFHM-SNAWJCMRSA-N (2E)-hexenal Chemical compound CCC\C=C\C=O MBDOYVRWFFCFHM-SNAWJCMRSA-N 0.000 description 2
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- 229940061629 trideceth-9 Drugs 0.000 description 1
- JLGLQAWTXXGVEM-UHFFFAOYSA-N triethylene glycol monomethyl ether Chemical compound COCCOCCOCCO JLGLQAWTXXGVEM-UHFFFAOYSA-N 0.000 description 1
- 150000004072 triols Chemical class 0.000 description 1
- ASTWEMOBIXQPPV-UHFFFAOYSA-K trisodium;phosphate;dodecahydrate Chemical compound O.O.O.O.O.O.O.O.O.O.O.O.[Na+].[Na+].[Na+].[O-]P([O-])([O-])=O ASTWEMOBIXQPPV-UHFFFAOYSA-K 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0034—Fixed on a solid conventional detergent ingredient
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/08—Silicates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2079—Monocarboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/373—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicones
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
- C11D3/502—Protected perfumes
- C11D3/505—Protected perfumes encapsulated or adsorbed on a carrier, e.g. zeolite or clay
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/62—Quaternary ammonium compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/12—Soft surfaces, e.g. textile
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3723—Polyamines or polyalkyleneimines
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/373—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicones
- C11D3/3742—Nitrogen containing silicones
Definitions
- the present invention relates to a solid, particulate composition
- a solid, particulate composition comprising at least one water-soluble carrier material, at least one fragrance and at least one textile care compound, the carrier material being a water-containing salt (hydrate) whose water vapor partial pressure is in the range from 30 to 100 ° at a certain temperature C corresponds to the H 2 O partial pressure of the saturated solution of this salt, so that the salt melts in its own crystal water at this temperature.
- the invention also relates to a method for producing the solid composition and a washing or cleaning agent which contains the solid composition.
- the present invention also relates to the use of such a washing or cleaning agent for cleaning textiles and corresponding methods for cleaning textiles using such a washing or cleaning agent.
- fragrances in the form of fragrance particles are either used as an integral component of a washing or cleaning agent, or are metered into the washing drum in a separate form at the beginning of a washing cycle. In this way, the consumer can control the scenting of the laundry to be washed through individual dosing.
- One form of supply that enables the separate dosage of fragrances is the fragrance lozenge.
- the main component of such fragrant lozenges known in the art is typically a water-soluble or at least water-dispersible carrier polymer, such as polyethylene glycol (PEG), which serves as a vehicle for the integrated fragrances and which is more or less completely absorbed in the wash liquor during the course of the waxing process dissolves in order to release the contained fragrances and possibly other components into the wash liquor.
- PEG polyethylene glycol
- a melt is produced from the carrier polymer, which contains the other ingredients or these are then added, and the resulting melt is then fed to a shaping process, in the course of which it cools down, solidifies and takes on the desired shape.
- the known products have the disadvantage that the polymer materials used, in particular PEG, have a delayed solubility, which can lead to residues on the laundry or in the washing machine, especially in the case of short wash cycles, low temperature or other unfavorable conditions.
- scented lozenges described in the prior art generally have no additional function, that is to say, they are generally used exclusively for scenting. From the consumer's point of view, however, a second or third function is desirable in addition to the scenting.
- a particularly relevant secondary function in connection with scented lozenges is textile care.
- the object of the present invention was therefore to identify an alternative composition which shows a suitable processing range and at the same time has improved water solubility in the usual temperature ranges in which work is carried out and, in addition to the fragrance effect, also has a textile care effect.
- the solid, particulate composition as described herein is produced from a solution of the carrier material in the water / water of crystallization contained in the composition, the term “melt” also being used herein for such a solution in contrast to the established use, to describe the state in which the carrier material dissolves in its own crystal water through the splitting off of water and thus forms a liquid.
- the term “melt”, as used herein, thus denotes the liquid state of the composition which arises when the temperature is exceeded at which the carrier material splits off water of crystallization and then dissolves in the water contained in the composition.
- the corresponding dispersion, which contains the (solids) substances described herein, dispersed in the melt of the carrier material is thus also the subject of the invention.
- melt / melt dispersion from which it can be obtained is also always included. Since these do not differ in terms of their composition, with the exception of their physical state, the terms are used synonymously herein.
- melt body is used herein to describe the solid particles obtainable from the liquid composition by solidification / reshaping on cooling.
- the main component of the particulate, solid composition as described herein is at least one water-soluble carrier material.
- the water-soluble carrier material is contained in an amount of 30 to 95% by weight, preferably 40 to 90% by weight, in particular 45 to 90% by weight, based on the total weight of the composition .
- the at least one carrier material is characterized in that it is selected from hydrous salts whose water vapor partial pressure at a temperature in the range from 30 to 100 ° C. corresponds to the H 2 O partial pressure of the saturated solution of this salt at the same temperature.
- hydrous salts whose water vapor partial pressure at a temperature in the range from 30 to 100 ° C. corresponds to the H 2 O partial pressure of the saturated solution of this salt at the same temperature.
- the corresponding water-containing salt also referred to herein as "hydrate” dissolves in its own crystal water when this temperature is reached or exceeded and thus changes from a solid to a liquid aggregate state.
- the carrier materials according to the invention preferably show this behavior at a temperature in the range from 40 to 90.degree. C., particularly preferably between 50 and 85.degree. C., even more preferably between 55 and 80.degree.
- the above-described water-soluble carrier materials from the group of water-containing salts include in particular sodium acetate trihydrate (Na (CH 3 COO) 3H 2 O), Glauber's salt (Na 2 SO 4 ⁇ 10H 2 O), trisodium phosphate dodecahydrate (Na 3 PO 4 ⁇ 12 H 2 O) and strontium chloride hexahydrate (SrCl 2 ⁇ 6 H 2 O).
- sodium acetate trihydrate Na (CH 3 COO) 3H 2 O
- Glauber's salt Na 2 SO 4 ⁇ 10H 2 O
- trisodium phosphate dodecahydrate Na 3 PO 4 ⁇ 12 H 2 O
- strontium chloride hexahydrate strontium chloride hexahydrate
- the use of sodium acetate trihydrate (Na (CH 3 COO) .3H 2 O) is particularly preferred.
- the particulate composition contains sodium acetate trihydrate
- such compositions are particularly advantageous with regard to their producibility, formulability and handling, which contain the sodium acetate trihydrate in an amount of 30 to 95% by weight, preferably 40 to 90% by weight, in particular from 45 to 90% by weight based on the total weight of the composition.
- a particularly suitable carrier material is sodium acetate trihydrate (Na (CH 3 COO) 3H 2 O), since it dissolves in its own crystal water in the particularly preferred temperature range of 55 to 80 ° C, specifically at around 58 ° C.
- the sodium acetate trihydrate can be used directly as such, but alternatively the use of anhydrous sodium acetate in combination with free water is possible, the trihydrate then being formed in situ .
- the water is used in an under- or over-stoichiometric amount based on the amount necessary to convert all of the sodium acetate into sodium acetate trihydrate, preferably in an amount of at least 60% by weight, preferably at least 70% by weight %, more preferably at least 80% by weight, most preferably 90% by weight, 100% by weight or more, of the amount theoretically required to convert all of the sodium acetate to sodium acetate trihydrate (Na (CH 3 COO) 3H 2 O).
- the overstoichiometric use of water is particularly preferred.
- composition that contains 50% by weight of anhydrous sodium acetate and no hydrate thereof, at least 19.8% by weight of water (60% of 33% by weight that would theoretically be necessary to make all the sodium acetate to be converted into the trihydrate), contains.
- compositions which contain sodium acetate in an amount of 18 to 57% by weight, preferably 24 to 48% by weight, are particularly advantageous with regard to their producibility, configurability and handling. in particular from 27 to 45% by weight based on the total weight of the composition.
- the solid particulate compositions contain a fragrance b) as a second essential component.
- the proportion by weight of the fragrance in the total weight of the composition is preferably 1 to 15% by weight, more preferably 3 to 12% by weight.
- a fragrance is a chemical substance that stimulates the sense of smell.
- the chemical substance should be at least partially dispersible in the air, i.e. the fragrance should be at least slightly volatile at 25 ° C. If the fragrance is now very volatile, the odor intensity then quickly subsides again. With a lower volatility, however, the odor impression is more lasting, i.e. it doesn't go away anytime soon.
- the fragrance therefore has a melting point which is in the range from -100 ° C to 100 ° C, preferably from -80 ° C to 80 ° C, even more preferably from -20 ° C to 50 ° C, in particular from - 30 ° C to 20 ° C.
- the fragrance has a boiling point which is in the range from 25 ° C. to 400 ° C., preferably from 50 ° C. to 380 ° C., more preferably from 75 ° C. to 350 ° C., in particular from 100 ° C. to 330 ° C.
- the fragrance has a molecular weight of 40 to 700 g / mol, more preferably 60 to 400 g / mol.
- fragrances can also be used to mask unpleasant odors or to provide a non-odorous substance with a desired odor.
- Individual fragrance compounds e.g. the synthetic products of the type of esters, ethers, aldehydes, ketones, alcohols and hydrocarbons are used.
- Fragrance compounds of the aldehyde type are, for example, adoxal (2,6,10-trimethyl-9-undecenal), anisaldehyde (4-methoxybenzaldehyde), cymal (3- (4-isopropyl-phenyl) -2-methylpropanal), ethylvanillin, florhydral ( 3- (3-isopropylphenyl) butanal), helional (3- (3,4-methylenedioxyphenyl) -2-methylpropanal), heliotropin, hydroxycitronellal, lauraldehyde, lyral (3- and 4- (4-hydroxy-4-methylpentyl) - 3- cyclohexene-1-carboxaldehyde), methylnonylacetaldehyde, Lilial (3- (4-tert-butylphenyl) -2-methylpropanal), phenylacetaldehyde, undecylenealdehyde, vanillin
- Fragrance compounds of the ketone type are, for example, methyl beta-naphthyl ketone, musk indanone (1,2,3,5,6,7-hexahydro-1,1,2,3,3-pentamethyl-4H-inden-4-one), Tonalid (6-acetyl-1,1,2,4,4,7-hexamethyltetralin), alpha-damascone, beta-damascone, delta-damascone, iso-damascone, damascenone, methyl dihydrojasmonate, menthone, carvone, camphor, coavone (3 , 4,5,6,6-pentamethylhept-3-en-2-one), fenchone, alpha-ionone, beta-ionone, gamma-methyl-ionone, fleuramon (2-heptylcyclopen-tanone), dihydrojasmone, cis-jasmone , iso-E-Super (1
- Fragrance compounds of the alcohol type are for example 10-undecen-1-ol, 2,6-dimethylheptan-2-ol, 2-methyl-butanol, 2-methylpentanol, 2-phenoxyethanol, 2-phenylpropanol, 2-tert.-butycyclohexanol, 3,5,5-trimethylcyclohexanol, 3-hexanol, 3-methyl-5-phenyl-pentanol, 3-octanol, 3-phenyl-propanol, 4-heptenol, 4-isopropyl-cyclohexanol, 4-tert.-butycyclohexanol, 6 , 8-dimethyl-2-nona-nol, 6-nonen-1-ol, 9-decen-1-ol, ⁇ -methylbenzyl alcohol, ⁇ -terpineol, amyl salicylate, benzyl alcohol, benzyl salicylate, ⁇ -terpineol
- Fragrance compounds of the ester type are e.g. Benzyl acetate, phenoxyethyl isobutyrate, p-tert-butylcyclohexyl acetate, linalyl acetate, dimethylbenzylcarbinylacetate (DMBCA), phenylethyl acetate, benzyl acetate, ethylmethylphenylglycinate, allylcyclohexylpropionate, styrallylpropionate, cyclohexylate, melacylsalicylate, and jasiclohexylate.
- DMBCA dimethylbenzylcarbinylacetate
- the ethers include, for example, benzyl ethyl ether and ambroxan.
- the hydrocarbons mainly include terpenes such as limonene and pinene.
- fragrances are preferably used, which together produce an appealing fragrance note.
- a mixture of fragrances can also be referred to as perfume or perfume oil.
- perfume oils can also contain natural fragrance mixtures, such as are available from vegetable sources.
- the fragrances of vegetable origin include essential oils such as angelica root oil, anise oil, arnica flower oil, basil oil, bay oil, champaca flower oil, citrus oil, noble fir oil, noble fir cone oil, elemi oil, eucalyptus oil, fennel oil, spruce needle oil, guajun oil, gourd oil, gjajun oil, galbanum oil, gourd oil, gjajun oil , Ginger oil, iris oil, jasmine oil, kajeput oil, calamus oil, chamomile oil, camphor oil, kanaga oil, cardamom oil, cassia oil, pine needle oil, copaiva balsam oil, Coriander oil, spearmint oil, caraway oil, cumin oil, labdanum oil, lavender oil, lemongrass oil, linden blossom oil, lime oil, mandarin oil, lemon balm oil, mint oil, musk seed oil, muscatel oil, myrrh oil, clove oil, neroli oil
- fragrance capsules encapsulated form
- the entire fragrance can also be used in encapsulated form.
- the microcapsules can be water-soluble and / or water-insoluble microcapsules.
- melamine-urea-formaldehyde microcapsules, melamine-formaldehyde microcapsules, urea-formaldehyde microcapsules or starch microcapsules can be used.
- “Fragrance precursors” refers to compounds which only release the actual fragrance after chemical conversion / cleavage, typically through exposure to light or other environmental conditions such as pH, temperature, etc. Such compounds are often referred to as fragrance storage substances or "pro-fragrance”.
- the fragrance is selected from the group of perfume oils and fragrance capsules.
- the use of a combination of perfume oil and fragrance capsules is very particularly preferred. Owing to their persistent, uniform fragrance effect, those compositions are particularly preferred in which the weight ratio of perfume oil to fragrance capsules is 30: 1 to 1:20, preferably 20: 1 to 1:15 and in particular 15: 1 to 1:10.
- the third essential component of the solid particulate composition contains a textile care compound.
- the textile care compound is different from the previously described water-soluble carrier material and the previously described fragrance.
- the proportion by weight of the textile care compound in the total weight of the composition is preferably 0.2 to 20% by weight and in particular 0.5 to 15% by weight.
- the group of textile care compounds includes textile softening compounds and anti-crease compounds.
- the textile care compound is selected from polysiloxanes, textile-softening clays, cationic polymers and mixtures thereof.
- polysiloxanes and / or cationic polymers as textile care compounds in the composition is advantageous because they not only have a softening effect, but also enhance the perfume impression on the laundry.
- softening clays as a textile care compound in the composition is advantageous because they also have a water-softening effect and thus, for example, can prevent limescale deposits on the laundry.
- the composition contains a combination of at least two textile care compounds.
- Polydimethylpolysiloxanes are known to be efficient textile care compounds. Suitable polydimethysiloxanes include DC-200 (ex Dow Corning), Baysilone® M 50, Baysilone® M 100, Baysilone® M 350, Baysilone® M 500, Baysilone® M 1000, Baysilone® M 1500, Baysilone® M 2000 or Baysilone® M 5000 (all ex GE Bayer Silicones).
- a particularly preferred polysiloxane has the following structure: (CH 3 ) 3 Si- [O-Si (CH 3 ) 2 ] n - [O-Si (CH 3 ) ⁇ (CH 2 ) 3 -NH- (CH 2 ) 2 -NH 2 ⁇ ] x -OSi ( CH 3 ) 3 , where the sum n + x is a number between 2 and 10,000.
- the compositions can contain at least one aminosiloxane as silicone oil.
- This can be selected, for example, from the group comprising Amodimethicone / Morpholinomethyl Silsesquioxane Copolymer ( CAS No. 1293390-78-9 ), Trideceth-9 PG-Amodimethicone ( CAS No. 943769-53-7 ), dimethyl hydroxy-limited with methylsilsesquioxane, methyl (aminoethylaminoisobutyl) siloxane ( CAS No. 863918-80-3 ) and dimethyl, methyl (aminoethylaminoisobutyl) siloxane ( CAS No.
- the aminosiloxanes also serve to improve the water absorption capacity, the rewettability of the treated textiles and to facilitate ironing of the treated textiles. In addition, they improve the rinsing behavior of the agent according to the invention through their foam-inhibiting properties. If an agent is mentioned in the present application, this is to be understood as the fabric softener.
- a suitable textile-softening sheet silicate is, for example, a smectite clay.
- Preferred smectite clays are beidellite clays, hectorite clays, laponite clays, montmorillonite clays, nontronite clays, Saponite clays, sauconite clays and mixtures thereof.
- Montmorillonite clays are the preferred emollient clays.
- Bentonites contain mainly montmorillonites and can serve as the preferred source of the fabric softening clay. The bentonites can be used as powder or crystals.
- Suitable bentonites are sold, for example, under the names Laundrosil® by Süd-Chemie or under the name Detercal by Laviosa. It is preferred that the textile care composition contains a powdered bentonite as a textile care compound.
- Suitable cationic polymers include in particular those in " CTFA International Cosmetic Ingredient Dictionary, “Fourth Edition, JM Nikitakis, et al, Editors , published by the Cosmetic, Toiletry, and Fragrance Association, 1991 are described and are summarized under the collective name "Polyquaternium”.
- Polyquaternium compounds are detailed below: POLYQUATERNIUM-1 ( CAS number: 68518-54-7 ), POLYQUATERNIUM-2 ( CAS number: 63451-27-4 ), POLYQUATERNIUM-3, POLYQUATERNIUM-4 ( CAS number: 92183-41-0 ), POLYQUATERNIUM-5 ( CAS number: 26006-22-4 ), POLYQUATERNIUM-6 ( CAS number: 26062-79-3 ), POLYQUATERNIUM-7 ( CAS number: 26590-05-6 ), POLYQUATERNIUM-8, POLYQUATERNIUM-9, POLYQUATERNIUM-11 ( CAS number: 53633-54-8 ), POLYQUATERNIUM-12 ( CAS number: 68877-50-9 ), POLYQUATERNIUM-13 ( CAS number: 68877-47-4 ), POLYQUATERNIUM-14 ( CAS number: 27103-90-8 ), POLYQUATERNIUM-15 ( CAS number: 3
- the textile care compound is selected from the group of cationic surfactants, in particular from the group of esterquats.
- esterquat as used herein relates to esters of quaternary ammonium polyols, in particular quaternary ammonium diols and / or triols, such as, for example, triethanolmethylammonium or diethanoldimethylammonium, with fatty acids.
- esterquats in cosmetic products, detergents and aftertreatment agents, in particular in fabric softeners, is known in the prior art. There they help to improve the soft hand, reduce the static charge on the textile fabrics and reduce the drying time.
- esterquats used according to the invention are ideally liquid to pasty at temperatures around 20 ° C.
- the composition contains at least one ester quat of the formula N + (R 1 ) 4-n ((CH 2 ) m -OC (O) -R 2 ) n X - , where each R 1 is independently a substituted or unsubstituted, linear or branched alkyl or alkenyl, preferably an unsubstituted or hydroxy-substituted alkyl having 1 to 10 carbon atoms; each R 2 is a linear or branched, substituted or unsubstituted alkyl or alkenyl or a substituted or unsubstituted (hetero) aryl having up to 26 carbon atoms, preferably linear unsubstituted C10-26 alkyl; n is 1, 2, 3 or 4, preferably 1, 2 or 3; m is an integer from 1 to 20, preferably 1 to 4; and X - is any anion.
- n is 2 or 3, preferably 2; and / or m 1, 2, 3 or 4, preferably 2 and / or each R 1 independently selected from the group consisting of methyl, ethyl, n-propyl, iso-propyl, n-butyl, iso-butyl, hydroxymethyl, 2-hydroxyethyl, 2-hydroxypropyl and 3-hydroxypropyl, preferably a first R 1 is selected from methyl, ethyl, n-propyl, iso-propyl, n-butyl and iso-butyl and a second R 1 is selected from methyl , Ethyl, n-propyl, iso-propyl, n-butyl, iso-butyl, hydroxymethyl, 2-hydroxyethyl, 2-hydroxypropy
- esterquats are bis (acyloxyethyl) hydroxyethylmethylammonium compounds.
- the counterion is preferably methosulfate.
- esterquats are commercially available, for example, under the trade name Dehyquart® AU-57 (BASF SE, DE).
- alkylamidopropyl betaines preferably linear C8 or C10 alkylamidopropyl betaines, ie caprylamidopropyl betaine (N- (3-octanoyl) aminopropyl) -N-carboxymethyl-N, N-dimethyl-1-propanaminium ) or capramidopropyl betaine (N- (3-decanoyl) aminopropyl) -N-carboxymethyl-N, N-dimethyl-1-propanaminium), or, very particularly preferably, mixtures of linear C8 and C10 alkyl amidopropyl betaines.
- Such a betaine mixture is commercially available, for example, as Tegotens® B 810 from Evonik Industries.
- Particularly preferred solid, particulate compositions contain drawing aids from a further constituent, in particular cellulose derivatives or cationically modified guar.
- the solid particulate composition can contain further optional components.
- the particulate, solid composition if it further comprises at least one rheology modifier, preferably a solid rheology modifier.
- the preferably solid rheology modifier is preferably used in such a manner and amount that a melt obtained by heating the composition to 70 ° C. has a flow limit above 1 Pa, preferably above 5 Pa and in particular above 10 Pa.
- the flow limit is measured with a rotational rheometer (AR G2 from TA Instruments or a "Kinexus” from Malvern), using a plate-plate measuring system with a diameter of 40 mm and a plate spacing of 1.1 mm.
- the yield point is determined in a step-flow procedure in which the shear stress is quasi-static, i.e. while waiting for the equilibrium deformation or steady flow is increased from the smallest possible value to a value above the flow limit.
- the deformation is plotted against the shear stress in a logarithmic diagram. If there is a flow limit, the curves obtained in this way show a characteristic kink. An exclusively elastic deformation takes place below the kink.
- the slope of the curve in the logarithmic representation is ideally one.
- the slope of the curve increases sharply and steady flow occurs.
- the shear stress value of the kink corresponds to the yield point. If the kink is not quite sharp, the intersection of the tangents of the two curve sections can be used to determine the yield point. In the case of liquids that do not have a flow limit, the graph described above is usually curved to the right.
- Inorganic as well as organic substances with corresponding properties influencing the rheology of the molten composition can be used as rheology modifiers. These substances can contain solid (at 20 ° C. and 1 bar) or liquid ingredients, the use of solid rheology modifiers being preferred.
- the proportion by weight of the inorganic rheology modifier in the total weight of the composition can be 0.1 to 25% by weight, but is preferably 0.5 to 3% by weight, more preferably 1 to 2.5% by weight and in particular 1.2 to 2.0% by weight.
- the group of inorganic rheology modifiers includes, for example, pyrogenic silica, which is particularly preferred because of its advantageous technical effect.
- the silicas used preferably have a BET surface area of more than 50 m 2 / g, preferably more than 100 m 2 / g, more preferably 150 to 250 m 2 / g, in particular 175 to 225 m 2 / g.
- Suitable silicas are commercially available from Evonik under the trade names Aerosil® and Sipernat®. Aerosil® 200 is particularly preferred.
- the proportion by weight of the organic rheology modifier in the total weight of the composition can be 0.1 to 25% by weight, but is preferably 0.5 to 3% by weight, more preferably 1 to 2.5% by weight and in particular 1.2 to 2.0% by weight.
- MFC microfibrillated cellulose
- FMC Avicel®
- heteroglycans are polysaccharides that are made up of more than one type of monomeric simple sugar.
- Suitable rheology modifiers are heteroglycans of different origin, in particular heteroglycans of bacterial origin, heteroglycans of algic origin and heteroglycans of vegetable origin. These heteroglycans can be used individually or in combination.
- heteroglycans of bacterial origin are particularly preferred.
- the use of heteroglycans which are obtained by bacterial fermentation is particularly preferred.
- Heteroglycans from the group of exopolysaccharides in particular have proven effective as rheology modifiers.
- Preferred rheology modifiers from the group of heteroglycans are furthermore functionalized by at least one non-saccharidic group, preferably by at least one non-saccharidic group selected from acetate, pyruvate, phosphate and succinate.
- compositions contain a compound with the INCI name succinoglycan as a rheology modifier.
- compositions include tablets containing active substances, dyes, preservatives, bitter substances or buffer systems.
- the active substance-containing shaped bodies preferably comprise at least one dye.
- the shaped bodies comprise at least one water-soluble dye, particularly preferably a water-soluble polymer dye.
- Such dyes are known in the art and are used, based on the total weight of the composition, typically in concentrations of 0.001 to 0.5% by weight, preferably 0.01 to 0.3% by weight.
- Preferred dyes should have high storage stability and insensitivity to the other ingredients of the detergents or cleaning agents and to light and not have any pronounced substantivity towards textile fibers in order not to stain them.
- the dye is a common dye that can be used for various detergents or cleaning agents.
- the dye is preferably selected from Acid Red 18 (CI 16255), Acid Red 26, Acid Red 27, Acid Red 33, Acid Red 51, Acid Red 87, Acid Red 88, Acid Red 92, Acid Red 95, Acid Red 249 ( CI 18134), Acid Red 52 (CI 45100), Acid Violet 126, Acid Violet 48, Acid Violet 54, Acid Yellow 1, Acid Yellow 3 (CI 47005), Acid Yellow 11, Acid Yellow 23 (CI 19140), Acid Yellow 3, Direct Blue 199 (CI 74190), Direct Yellow 28 (CI 19555), Food Blue 2 (CI 42090), Food Blue 5: 2 (CI 42051: 2), Food Red 7 (01 16255), Food Yellow 13 (CI 47005), Food Yellow 3 (CI 15985), Food Yellow 4 (CI 19140), Reactive Green 12, Solvent Green 7 (CI 59040).
- Particularly preferred dyes are water-soluble acid dyes, for example Food Yellow 13 (Acid Yellow 3, CI 47005), Food Yellow 4 (Acid Yellow 23, CI 19140), Food Red 7 (Acid Red 18, CI 16255), Food Blue 2 (Acid Blue 9, CI 42090), Food Blue 5 (Acid Blue 3, CI 42051), Acid Red 249 (CI 18134), Acid Red 52 (CI 45100), Acid Violet 126, Acid Violet48, Acid Blue 80 (01 61585), Acid Blue 182, Acid Blue 182, Acid Green 25 (CI 61570), Acid Green 81.
- Food Yellow 13 Acid Yellow 3, CI 47005
- Food Yellow 4 Acid Yellow 23, CI 19140
- Food Red 7 Acid Red 18, CI 16255
- Food Blue 2 Acid Blue 9, CI 42090
- Food Blue 5 Acid Blue 3, CI 42051
- Acid Red 249 CI 18134
- Acid Red 52 CI 45100
- Acid Violet 126 Acid Violet48
- Acid Blue 80 01 61585
- Acid Blue 182 Acid Blue 18
- Water-soluble direct dyes for example Direct Yellow 28 (CI 19555), Direct Blue 199 (CI 74190) and water-soluble reactive dyes, for example Reactive Green 12, and the dyes Food Yellow 3 (CI 15985), Acid Yellow 184 are also preferably used.
- Aqueous dispersions of the following pigment dyes Pigment Black 7 (CI 77266), Pigment Blue 15 (CI 74160), Pigment Blue 15: 1 (CI 74160), Pigment Blue 15: 3 (CI 74160), Pigment Green 7 are also preferably used (CI 74260), Pigment Orange 5, Pigment Red 112 (CI 12370), Pigment Red 112 (CI 12370), Pigment Red 122 (CI 73915), Pigment Red 179 (CI 71130), Pigment Red 184 (CI 12487), Pigment Red 188 (CI 12467), Pigment Red 4 (CI 12085), Pigment Red 5 (CI 12490), Pigment Red 9, Pigment Violet 23 (CI 51319), Pigment Yellow 1 (CI 28 11680), Pigment Yellow 13 (CI 21100 ), Pigment Yellow 154, Pigment Yellow 3 (CI 11710), Pigment Yellow 74, Pigment Yellow 83 (CI 21108), Pigment Yellow 97.
- pigment dyes are used in the form of dispersions: Pigment Yellow 1 (CI 11680), Pigment Yellow 3 (CI 11710), Pigment Red 112 (CI 12370), Pigment Red 5 (CI 12490), Pigment Red 181 (CI 73360), Pigment Violet 23 (CI 51319), Pigment Blue 15: 1 (CI 74160), Pigment Green 7 (CI 74260), Pigment Black 7 (CI 77266).
- water-soluble polymer dyes for example Liquitint, Liquitint Blue HP, Liquitint Blue MC, Liquitint Blue 65, Liquitint Cyan 15, Liquitint Patent Blue, Liquitint Violet 129, Liquitint Royal Blue, Liquitint Experimental Yellow 8949-43, Liquitint Green HMC, Liquitint Yellow LP, Liquitint Yellow II and mixtures thereof are used.
- the use of water-soluble polymer dyes is preferred.
- the group of very particularly preferred dyes includes Acid Blue 3, Acid Yellow 23, Acid Red 33, Acid Violet 126, Liquitint Yellow LP, Liquitint Cyan 15, Liquitint Blue HP and Liquitint Blue MC.
- bitter substances primarily serves to avoid oral ingestion of the tablets containing active substances.
- Preferred moldings contain at least one bitter substance in an amount of 0.0001 to 0.05% by weight, based on the total weight of the composition. Quantities from 0.0005 to 0.02% by weight are particularly preferred. According to the present invention, those bitter substances are particularly preferred which are soluble in water at 20 ° C. to the extent of at least 5 g / l. With regard to an undesirable interaction with the fragrance components also contained in the composition, in particular a change in the fragrance note perceived by the consumer, the ionic bitter substances have proven to be superior to the non-ionic, ionic bitter substances, consisting of organic cation (s) and organic (n) Anion (s) are consequently preferred for the composition according to the invention.
- the at least one bitter substance is therefore an ionogenic bitter substance.
- quaternary ammonium compounds which contain an aromatic group both in the cation and in the anion are eminently suitable.
- the at least one bitter substance is therefore a quaternary ammonium compound.
- a suitable quaternary ammonium compound is, for example, without limitation, commercially available e.g. Benzyldiethyl ((2,6-xylylcarbamoyl) methyl) ammonium benzoate available under the trademarks Bitrex® and Indige-stin®. This compound is also known as Denatonium Benzoate.
- the at least one bitter substance is benzyl diethyl ((2,6-xylylcarbamoyl) methyl) ammonium benzoate (Bitrex®). If Bitrex® is used, proportions by weight of 0.0001 to 0.05% by weight are preferred. The information is based on the active ingredient content and the total weight.
- the composition also contains at least one buffer system.
- the buffer system is preferably solid, ie it is a solid (mixture) under standard conditions.
- the term "buffer capacity” refers to the amount of hydrogen chloride (HCl) in mg that is necessary to maintain the pH value of a solution of 1 g of the solid composition in 50 g of deionized water under standard conditions (20 ° C, 1013 mbar) lower to below 6.75.
- the buffer systems used according to the invention are preferably characterized in that they have a pKa value of at least 5.75, preferably at least 6.25, more preferably at least 6.75, and preferably not more than 12, more preferably less than 11.5, more preferably 11 or less, most preferably 10.5 or less.
- the buffer capacity of the resulting solution is preferably at least 2 mg HCl / g composition, preferably at least 3 mg HCl / g composition, more preferably at least 4 mg HCl / g composition.
- Suitable buffer substances are, for example, without restriction, sodium hydrogen carbonate, sodium carbonate, disodium hydrogen phosphate, sodium glutamate, sodium aspartate, tris (hydroxymethyl) aminomethane (TRIS) and other organic and inorganic buffer substances known in the art that meet the above criteria, as well as mixtures of the aforementioned. TRIS is particularly preferred.
- the buffer substances are used in the compositions according to the invention, for example, in amounts of 0.1 to 10% by weight, preferably 0.5 to 7.5% by weight, more preferably 1 to 5% by weight, each based on the total weight of the composition used and are preferably selected from sodium hydrogen carbonate, sodium carbonate, disodium hydrogen phosphate, sodium glutamate, sodium aspartate, tris (hydroxymethyl) aminomethane (TRIS) and combinations thereof, preferably tris (hydroxymethyl) aminomethane.
- TIS tris (hydroxymethyl) aminomethane
- the composition preferably does not contain a polyethylene glycol (PEG) solid at room temperature (25 ° C) in the form of a coating, more preferably the composition as a whole does not contain PEG solid at room temperature (25 ° C), i. the content of PEG which is solid at room temperature (25 °) is less than 1% by weight based on the composition.
- PEG polyethylene glycol
- compositions according to the invention are distinguished from the known compositions of the prior art by an improved solubility profile and an improved fragrance effect.
- these compositions tend to have unaesthetic "salt efflorescence" on their surface. These changes in the particle surface particularly affect the appearance of dye-containing compositions. Another task was therefore to prevent or at least alleviate this efflorescence through formulation measures.
- compositions according to the invention contain at least one water-miscible organic solvent as a further optional component.
- the water-miscible organic solvents are preferably not very volatile and odorless. Suitable water-miscible organic solvents are, for example, monohydric and polyhydric alcohols, alkyl ethers, di- or low molecular weight polyalkylene ethers which are liquid at room temperature.
- the solvents are preferably selected from ethanol, n-propanol, i-propanol, butanols, glycol, propanediol, butanediol, methylpropanediol, diglycol, butyl diglycol, hexylene glycol, Ethylene glycol methyl ether, ethylene glycol ethyl ether, Ethylenglykolpropylether, ethylene glycol mono-n-butyl ether, diethylene glycol methyl ether, diethylene glycol ethyl ether, propylene glycol methyl ether, propylene glycol ethyl ether, propylene glycol propyl ether, dipropylene glycol monomethyl ether, dipropylene glycol monoethyl ether, methoxytriglycol, ethoxytriglycol, Butoxytriglykol, 1-butoxyethoxy-2-propanol, 3-methyl-3-methoxybutan
- Dipropylene glycol, 1,2-propylene glycol and glycerine are particularly preferred, since these are particularly readily miscible with water and do not otherwise react with the other constituents of the composition.
- Dipropylene glycol is particularly preferred.
- the proportion by weight of the water-miscible organic solvent in the total weight of the composition is preferably 0.1 to 20% by weight, more preferably 0.1 to 10% by weight, particularly preferably 0.5 to 8% by weight and in particular 1 to 6% by weight .-%.
- the composition can possibly also contain free water.
- free water denotes water which is not bound as crystal water in any of the salts contained in the composition.
- the solid, particulate composition can be in any form.
- spherical, figurative, flake, cuboid, cylinder, cone, spherical cap or lens, hemispherical, disc or needle-shaped particles are preferred.
- Exemplary particles can have a gummy bear-like, figural design.
- Hemispherical particles are particularly preferred because of their packaging properties and their performance profile.
- the composition consists of at least 20% by weight, preferably at least 40% by weight, particularly preferably at least 60% by weight and particularly preferably at least 80% by weight, of particles which are present in each any spatial direction have a spatial extent between 0.5 to 10 mm, in particular 0.8 to 7 mm and particularly preferably 1 to 5 mm.
- the composition consists of at least 20% by weight, preferably at least 40% by weight, particularly preferably at least 60% by weight and particularly preferably at least 80% by weight, of particles in which the Ratio of the longest particle diameter determined in any spatial direction to the shortest in one any direction in space between 3: 1 and 1: 1, preferably between 2.5: 1 and 1.2: 1 and in particular between 2.2: 1 and 1.4: 1.
- compositions can also vary within wide limits. With regard to the producibility and dosing properties, however, compositions have proven to be advantageous which contain at least 20% by weight, preferably at least 40% by weight, particularly preferably at least 60% by weight and particularly preferably at least 80% by weight.
- -% consists of particles which have a particle weight between 2 and 150 mg, preferably between 8 and 120 mg and in particular between 20 and 100 mg.
- the solid particulate composition can be marketed or used alone or in combination with a further preparation.
- the solid particulate composition is a component of a washing or cleaning agent.
- the composition is primarily suitable for scenting textiles.
- the use of the solid composition or of a washing or cleaning agent which contains this composition as a textile care agent for scenting textile fabrics is therefore a further aspect of this application.
- the solid, particulate composition can also be used as a textile care agent for rinsing textile fabrics or for anti-crease finishing of textile fabrics.
- a composition as described herein can, for example, be used in the wash cycle of a laundry cleaning process and thus transport the perfume to the laundry right at the start of the washing process. Furthermore, the composition is easier and easier to handle than liquid compositions, since no drops remain on the edge of the bottle which, when the bottle is subsequently stored, lead to edges on the substrate or to unsightly deposits in the area of the closure. The same is true in the event that some of the composition is accidentally spilled during dosing. The spilled amount can also be cleaned up more easily and cleanly.
- a method for treating textiles in the course of which a composition according to the invention or a washing or cleaning agent comprising such a composition is metered into the washing liquor of a textile washing machine, is a further subject of this application.
- composition of some preferred compositions can be found in the following tables (data in% by weight based on the total weight of the agent unless otherwise stated).
- the fusible bodies according to the invention are coated in various embodiments of the invention.
- Tablet coatings known from the pharmaceutical literature, for example, are suitable as coating agents.
- the lozenges can also be waxed, i.e. coated with a wax or powdered with a powdery material, for example a release agent, to protect against caking (agglomeration). It is preferred that the coating does not consist of PEG or that it comprises a significant amount (> 10% by weight based on the coating).
- the melt dispersion produced in step a) is discharged from the first container by means of a pipeline and fed to the drop former. It is also preferred that the fragrance is introduced continuously into the outlet stream of the first container from a corresponding storage container by means of a further pipeline.
- a liquid preparation of the fragrance for example in the form of a solution, is particularly suitable for this.
- the temperature of the fragrance or the liquid preparation of the fragrance is preferably at least 10 ° C., preferably at least 20 ° C. and in particular at least 30 ° C. below the temperature of the melt dispersion forming the outlet flow before it is introduced into the outlet stream of the first container.
- Mixing is preferably carried out by means of a static mixer which is located in the pipeline in the direction of flow of the melt dispersion downstream of the entry point of the fragrance and before the entry point of the mixture into the drop former.
- the length of the static mixer installed in the pipeline in the flow direction of the melt dispersion is preferably at least 10 times, preferably at least 20 times and in particular at least 50 times the diameter of the pipeline.
- the distance between the end of the static mixer and the entry point of the pipeline into the drop former is less than 500 times, preferably less than 200 times and in particular less than 100 times the diameter of the pipeline.
- the inner diameter of the pipeline is referred to as the diameter of the pipeline, regardless of the wall thickness.
- the mixture of melt dispersion and fragrance enters the drop former with a rotating, perforated outer drum from the pipeline.
- the section of the pipeline which is located inside the drum of the drop former is referred to below as the feed channel to distinguish it from the previous pipeline.
- the feed channel extends preferably over at least 80%, particularly preferably over at least 90% and in particular over 100% of the length of the drum of the drop former.
- the mixture introduced into the feed channel exits the feed channel, preferably through bores located on the underside of the feed channel, from the feed channel onto a distributor or nozzle bar, which in turn rests against the inside of the rotating, perforated outer drum.
- the mixture runs through the distributor or nozzle bar and is then transferred from the holes in the rotating outer drum onto a steel belt located below these holes applied.
- the distance between the outside of the rotating, perforated outer drum and the surface of the steel belt is preferably between 5 and 20 mm.
- another mixer can be arranged in the feed channel.
- This is preferably a dynamic mixer, for example a helix that is rotatably arranged within the feed channel.
- the dwell time of the mixture of melt dispersion and fragrance in the pipeline until it exits the rotating, perforated outer drum of the drop former is preferably less than 20 seconds, particularly preferably less than 10 seconds and in particular between 0.5 and 5 Seconds.
- the viscosity (Texas Instruments AR-G2 rheometer; plate / plate, 4 cm diameter, 1100 ⁇ m gap; shear rate 10 / 1sec) of the mixture when it emerges from the rotating, perforated outer drum is preferably between 1000 and 10000 mPas.
- the drops of the mixture discharged from the drop former are solidified into solid melt bodies on the steel belt.
- the time between the dropping of the mixture on the steel strip and the complete solidification of the mixture is preferably between 5 and 60 seconds, particularly preferably between 10 and 50 seconds and in particular between 20 and 40 seconds.
- the solidification of the mixture is preferably supported and accelerated by cooling.
- the drops applied to the steel strip can be cooled directly or indirectly. Cooling by means of cold air, for example, can be used as direct cooling. However, indirect cooling of the droplets by cooling the underside of the steel strip using cold water is preferred.
- compositions according to the invention contains example formulations of compositions according to the invention (all data in% by weight) Table 1: Compositions V1 E2 E3 Sodium acetate (anhydrous) 54.1% 53.9% 53.8% water 12.4% 12.3% 12.2% Rheology modifier (2% in water) 24.3% 24.2% 24.1% Tris (hydroxymethyl) aminomethane (TRIS) 2.0% 2.0% 2.0% Fragrance 5.0% 5.0% 5.0% dye 2.0% 2.0% 2.0% Belsil ADM 8301 E. 0.0% 0.35% 0.70% Bitter substance, others ad 100 ad 100 ad 100 ad 100 ad 100
- the sodium acetate was dissolved in water at a temperature of 70 ° C. with stirring. The other components were then incorporated. Pastilles were produced by dripping the liquid mixture ("melt") onto a cooling plate heated to room temperature (23 ° C.).
- the active ingredient Belsil ADM 8301 produced a laundry-softening effect after a wash cycle in a household washing machine, which can be demonstrated in a pair comparison test with the help of a sensory assessment.
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- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
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Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
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EP19168929.8A EP3722405A1 (fr) | 2019-04-12 | 2019-04-12 | Composition solide contenant du parfum |
US16/846,506 US11549085B2 (en) | 2019-04-12 | 2020-04-13 | Solid perfume-containing composition |
Applications Claiming Priority (1)
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EP19168929.8A EP3722405A1 (fr) | 2019-04-12 | 2019-04-12 | Composition solide contenant du parfum |
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EP19168929.8A Withdrawn EP3722405A1 (fr) | 2019-04-12 | 2019-04-12 | Composition solide contenant du parfum |
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EP (1) | EP3722405A1 (fr) |
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US11834636B1 (en) * | 2023-05-24 | 2023-12-05 | Tufco, L.P. | Scent booster comprising polyethylene glycol, sodium bicarbonate, and sodium acetate for laundry |
US12077733B1 (en) | 2023-05-24 | 2024-09-03 | Tulco, L.P. | Scent booster for laundry comprising a sodium bicarbonate/sodium acetate trihydrate mixture |
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DE19530999A1 (de) * | 1995-08-23 | 1997-02-27 | Henkel Kgaa | Verfahren zum Aufbringen von Duftstoffen auf Textilgut |
WO2007113326A1 (fr) * | 2006-04-06 | 2007-10-11 | Henkel Ag & Co. Kgaa | Composition solide, permettant de prendre soin des textiles comprenant un polymère soluble dans l'eau |
WO2018055111A1 (fr) * | 2016-09-26 | 2018-03-29 | Henkel Ag & Co. Kgaa | Compositions particulaires solides comprenant un polymère support soluble dans l'eau et du parfum |
EP3476927A1 (fr) * | 2017-10-24 | 2019-05-01 | Henkel AG & Co. KGaA | Composition de parfum solide |
Family Cites Families (2)
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GB9911949D0 (en) * | 1999-05-21 | 1999-07-21 | Unilever Plc | Detergent compositions |
US20040152616A1 (en) * | 2003-02-03 | 2004-08-05 | Unilever Home & Personal Care Usa, Division Of Conopco, Inc. | Laundry cleansing and conditioning compositions |
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2019
- 2019-04-12 EP EP19168929.8A patent/EP3722405A1/fr not_active Withdrawn
-
2020
- 2020-04-13 US US16/846,506 patent/US11549085B2/en active Active
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DE19530999A1 (de) * | 1995-08-23 | 1997-02-27 | Henkel Kgaa | Verfahren zum Aufbringen von Duftstoffen auf Textilgut |
WO2007113326A1 (fr) * | 2006-04-06 | 2007-10-11 | Henkel Ag & Co. Kgaa | Composition solide, permettant de prendre soin des textiles comprenant un polymère soluble dans l'eau |
WO2018055111A1 (fr) * | 2016-09-26 | 2018-03-29 | Henkel Ag & Co. Kgaa | Compositions particulaires solides comprenant un polymère support soluble dans l'eau et du parfum |
EP3476927A1 (fr) * | 2017-10-24 | 2019-05-01 | Henkel AG & Co. KGaA | Composition de parfum solide |
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US11549085B2 (en) | 2023-01-10 |
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