EP3646942A1 - Device for mixing cement slurry, and method and appratus for producing cement slurry - Google Patents
Device for mixing cement slurry, and method and appratus for producing cement slurry Download PDFInfo
- Publication number
- EP3646942A1 EP3646942A1 EP19204692.8A EP19204692A EP3646942A1 EP 3646942 A1 EP3646942 A1 EP 3646942A1 EP 19204692 A EP19204692 A EP 19204692A EP 3646942 A1 EP3646942 A1 EP 3646942A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- mixture
- mixing
- tank
- cement slurry
- centrifugal impeller
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000002156 mixing Methods 0.000 title claims abstract description 75
- 239000004568 cement Substances 0.000 title claims abstract description 71
- 239000002002 slurry Substances 0.000 title claims abstract description 56
- 238000000034 method Methods 0.000 title claims description 13
- 239000000203 mixture Substances 0.000 claims abstract description 50
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000004519 manufacturing process Methods 0.000 claims abstract description 15
- 239000012530 fluid Substances 0.000 claims description 9
- 239000000654 additive Substances 0.000 claims description 4
- 238000011144 upstream manufacturing Methods 0.000 abstract description 3
- 239000000843 powder Substances 0.000 description 10
- 239000000047 product Substances 0.000 description 6
- 238000001035 drying Methods 0.000 description 4
- 238000012545 processing Methods 0.000 description 3
- 238000004891 communication Methods 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- -1 paving Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000011505 plaster Substances 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28C—PREPARING CLAY; PRODUCING MIXTURES CONTAINING CLAY OR CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28C5/00—Apparatus or methods for producing mixtures of cement with other substances, e.g. slurries, mortars, porous or fibrous compositions
- B28C5/08—Apparatus or methods for producing mixtures of cement with other substances, e.g. slurries, mortars, porous or fibrous compositions using driven mechanical means affecting the mixing
- B28C5/0887—Apparatus or methods for producing mixtures of cement with other substances, e.g. slurries, mortars, porous or fibrous compositions using driven mechanical means affecting the mixing provided with sieves or filters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/50—Circulation mixers, e.g. wherein at least part of the mixture is discharged from and reintroduced into a receptacle
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
- B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
- B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
- B01F27/2713—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator the surfaces having a conical shape
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
- B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
- B01F27/2714—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator the relative position of the stator and the rotor, gap in between or gap with the walls being adjustable
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28C—PREPARING CLAY; PRODUCING MIXTURES CONTAINING CLAY OR CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28C5/00—Apparatus or methods for producing mixtures of cement with other substances, e.g. slurries, mortars, porous or fibrous compositions
- B28C5/08—Apparatus or methods for producing mixtures of cement with other substances, e.g. slurries, mortars, porous or fibrous compositions using driven mechanical means affecting the mixing
- B28C5/10—Mixing in containers not actuated to effect the mixing
- B28C5/12—Mixing in containers not actuated to effect the mixing with stirrers sweeping through the materials, e.g. with incorporated feeding or discharging means or with oscillating stirrers
- B28C5/1238—Mixing in containers not actuated to effect the mixing with stirrers sweeping through the materials, e.g. with incorporated feeding or discharging means or with oscillating stirrers for materials flowing continuously through the mixing device and with incorporated feeding or discharging devices
- B28C5/1253—Mixing in containers not actuated to effect the mixing with stirrers sweeping through the materials, e.g. with incorporated feeding or discharging means or with oscillating stirrers for materials flowing continuously through the mixing device and with incorporated feeding or discharging devices with discharging devices
- B28C5/1261—Applying pressure for discharging
Abstract
Description
- This invention relates to a method for producing cement slurry, and a device for mixing cement slurry usable in that method, as well as an apparatus for producing cement slurry which incorporates the device.
- As is known, cement slurry is a viscous liquid product which comprises a mixture of water and powdered cement, if necessary with the addition of specific additives (for example pigments).
- It may be used either as the base for producing concrete by adding aggregate, or on its own for making various types of construction products (such as paving, plaster, etc.).
- Cement slurry is commonly made by simply mixing water and powdered cement. However, it is known that, the composition being the same, cement slurry obtainable with different mixing actions may have considerably different characteristics. In particular, the composition being the same, the mixing method and its duration may have a major impact both on the workability and cohesion of the cement slurry, and on the mechanical properties of the product after drying. Indeed, cement slurry is not a simple dispersion of solid cement particles in water, but also involves the development of chemical reactions between water and cement, which are rendered evident by the development of heat inside the mass being processed.
- In particular, what the Applicant has observed, is also that, depending on the mixing method adopted (and consequently its duration), it is possible to obtain the same results in terms of both workability (or consistency) and cohesion of the cement slurry, and of mechanical properties of the product after drying.
- Since the main operating cost linked to producing cement slurry is that of the powdered cement used, it immediately appears evident that managing to mix water and cement powder in the optimum way could allow savings in cement powder, and considerably reduce the operating cost of producing the cement slurry.
- However, so far, in most real applications the poor quality of mixing is such that it always requires the use of a quantity of powdered cement much greater than that strictly necessary.
- In this context the technical purpose which forms the basis of this invention is to provide a method for producing cement slurry and to make a device for mixing cement slurry, which overcome the above-mentioned disadvantages. In particular, the technical purpose of this invention is to provide a method for producing cement slurry, and to make a device for mixing cement slurry, which allow the obtainment of cement slurries with optimum characteristics in terms of both workability (or consistency) and cohesion of the cement slurry, and of mechanical strength properties of the product obtainable after drying, using quantities of cement powder significantly lower than in the methods and devices currently commonly used in the sector.
- A further technical purpose of this invention is to provide a method for producing cement slurry, and to make a device for mixing cement slurry, which allow the production of cement slurry of optimum quality in shorter times than in the plants commonly used.
- The technical purpose and the aims indicated are substantially achieved by a method for producing cement slurry and by a device for mixing cement slurry as described in appended claims.
- Further characteristics and the advantages of this invention will be more apparent from the detailed description of several preferred, non-limiting embodiments of this invention, with reference to the accompanying drawings, in which:
-
Figure 1 shows, in vertical axial section (except for some details such as the driving shaft), a device for mixing cement slurry made in accordance with this invention; -
Figure 2 shows an enlarged detail ofFigure 1 ; -
Figure 3 is a front view (from the right compared withFigure 1 ) of an impeller which is part of the device ofFigure 1 ; -
Figure 4 shows the impeller ofFigure 3 in cross-section according to the line IV - IV; -
Figure 5 shows, in an axonometric view, a fixed pierced wall which is part of the device ofFigure 1 ; -
Figure 6 shows the pierced wall ofFigure 5 in side view; -
Figure 7 shows, in schematic side view, with some parts transparent, an apparatus for producing cement slurry comprising the device ofFigure 1 ; -
Figure 8 shows, in front view with some parts transparent, the apparatus ofFigure 7 ; -
Figure 9 shows, enlarged, the detail IX of the apparatus ofFigure 7 ; -
Figure 10 shows in schematic side view a part of the apparatus ofFigure 7 , illustrating several tubes for introducing slurry into the tank; and -
Figure 11 shows, in horizontal section view, perpendicular to the generatrix of the tank and at one of the tubes ofFigure 10 , a possible distribution of tubes for introducing slurry around the tank. - Hereinafter there is initially a description of the innovative mixing device which is the subject matter of this invention, followed by the apparatus which comprises it, and finally the method for producing the cement slurry disclosed by this invention.
- It should be noticed that hereinafter in the description of this patent application "cement slurry" and "mixture of water and cement powder" will often be used interchangeably with reference to all of the intermediate production steps. Indeed, whilst it is proper to refer only to "mixture of water and cement powder" before its processing in accordance with this invention beings, and only to refer to "cement slurry" after the end of the processing, in all of the intermediate processing steps it is possible to consider the product as a mixture being converted into an actual slurry.
- With reference to the figures indicated, the device for mixing cement slurry according to this invention has been labelled with the
reference number 1 as a whole. - As shown in
Figure 1 and2 , thedevice 1 comprises first acontainment structure 2 which forms amixing chamber 3 inside it. - A
driving shaft 4 is mounted with a liquid-tight seal through thecontainment structure 2, and has afirst end 5 positioned in themixing chamber 3, and asecond end 6 which is outside thecontainment structure 2. Thesecond end 6 is connectable in use to a driving motor suitable for driving the rotation of thedriving shaft 4 about its axis ofrotation 41. - In the preferred embodiment, illustrated in the accompanying figures, there is also a supporting
structure 7 which is fixed to thecontainment structure 2 and is suitable for supporting, centring, and keeping in position axially, thedriving shaft 4 at an intermediate portion thereof between thefirst end 5 and thesecond end 6. - The
containment structure 2 comprises aninlet 8 and anoutlet 9, which allow fluid communication between themixing chamber 3 and the outside. Theinlet 8 is aligned with the axis ofrotation 41 and is centred on it. Mounted in themixing chamber 3 there is apierced wall 10, which is centred on the axis ofrotation 41, and which divides themixing chamber 3 into aninner part 11 and anouter part 12 which are coaxial. Theouter part 12 advantageously extends in an annular fashion and surrounds theinner part 11, being positioned in a position radially further out relative to the axis ofrotation 41. - The
inlet 8 is directly facing theinner part 11 of themixing chamber 3, whilst theoutlet 9 is facing theouter part 12 of themixing chamber 3. Therefore, the piercedwall 10 intercepts the fluid paths which extend from theinlet 8 to theoutlet 9. - In the preferred embodiment (
Figures 4 and5 ), thepierced wall 10 has frustoconical extension coaxial with the axis ofrotation 41, and with the larger base of the truncated cone towards theinlet 8 of themixing chamber 3. - Advantageously, the pierced
wall 10 has a plurality of throughholes 13 evenly distributed along the entire extent of the self-same piercedwall 10. In particular, in the embodiment illustrated, the throughholes 13 are organised along four circular rows each of sixty equally spaced holes, centred on the axis ofrotation 41 and spaced from each other, parallel to the axis ofrotation 41, with a constant pitch. Moreover, preferably, the piercedwall 10 has a plurality of throughholes 13 each with a passage area of between 40 and 200 mm2, advantageously of between 60 and 130 mm2. Moreover, in the preferred embodiments, the piercedwall 10 is made in such a way as to have a ratio of pierced surface area to total surface area facing themixing chamber 3, of between 1 to 5 and 1 to 3. - The
first end 5 of thedriving shaft 4 is positioned at theinner part 11 of themixing chamber 3, and fixed to it there is acentrifugal impeller 14 also positioned in theinner part 11 of themixing chamber 3. In use, as described in more detail below, thecentrifugal impeller 14, driven to rotate by means of thedriving shaft 4, forces the water-based mixture (slurry) to pass from theinner part 11 to theouter part 12 of themixing chamber 3, through the throughholes 13 of the piercedwall 10. - In general, the
centrifugal impeller 14 comprises a plurality ofblades 15, but advantageously their number is between 3 and 9. As shown in the accompanying figures, eachblade 15 preferably extends cantilever-style, towards theinlet 8, starting from a circular supportingplate 16 located near a wall of themixing chamber 3. Eachblade 15 also has an external edge 17 (that is to say, the edge radially furthest from the axis of rotation 41) which is substantially shaped to match thepierced wall 10 and near it (advantageously the distance between theexternal edge 17 and thepierced wall 10 is less than 2 mm, preferably less than 1 mm). The profile of theblade 15 is also such that theblade 15 has a height decreasing from itsinternal edge 18 towards theexternal edge 17. - Moreover, in accordance with the preferred embodiments, in use the
centrifugal impeller 14 is activated with a speed of rotation of between 500 and 5000 revolutions per minute, and/or a maximum tangential speed of between 10 and 80 m/s. - Joined to the
inlet 8 there is afeed duct 19 and, in accordance with a further innovative aspect of this invention, thefeed duct 19 and/or the inlet 8 (theinlet 8 inFigure 1 , but in general the one of the two which effectively guides the flow of cement slurry entering the mixing chamber 3) are shaped in such a way as to form at least one introducingduct 20. That introducingduct 20 has a cross-section increasing towards thecentrifugal impeller 14, and is directly facing theinner part 11 of themixing chamber 3 and thecentrifugal impeller 14. The aim of the introducingduct 20 is to cause a sudden increase in the pressure of the mixture, faced with a sudden reduction in speed compared with the speed which, the mixture itself, has upstream of the introducing duct 20 (in the accompanying figures thefeed duct 19 has astretch 21 with constant cross-section immediately upstream of the introducingduct 20 with increasing cross-section). - In particular, in the preferred embodiments, the introducing
duct 20 is sized in such a way as to cause, in use, an increase in the pressure of between 0.1 and 1 bar, in the fluid to be mixed which passes through it (that is to say, between entering and exiting the self-same introducing duct 20). - The
mixing device 1 described so far may be inserted in various types ofapparatuses 22 for producing cement slurry, and in particular inapparatuses 22 both of the continuous type (solution not illustrated), and of the batch type (solution illustrated in the accompanying figures). - In general, all of the
apparatuses 22 comprise at least onefirst mixing device 1, and afeeder 23 of a fluid mixture connected to thefeed duct 19. Depending on requirements, theapparatus 22 may also comprise, connected in series to theoutlet 9 of thefirst mixing device 1, one or morefurther mixing devices 1 which are also mounted in series relative to one another. The use ofmultiple mixing devices 1 in series is preferably always applied in the case ofcontinuous type apparatuses 22, whilst in the case ofbatch type apparatuses 22 the use of asingle mixing device 1 combined with a system for recirculating the mixture is the preferred solution for limiting the costs of theapparatus 22. - In the case of
continuous type apparatuses 22, theapparatus 22 will comprise a number ofmixing devices 1 equal to the number of mixing actions which, at the design stage, has been considered optimal. In contrast, in the case of batch type plants, the slurry will advantageously be made to pass in the mixing device or devices 1 a number of times equal to the number of mixing actions which, at the design stage, has been considered optimal, divided by the number of mixingdevices 1 positioned in series which are present. - In the case of a
batch type apparatus 22, thefeeder 23 comprises at least onetank 24 connected to thefeed duct 19, and at least one return duct 25 (visible only inFigure 10 ) connected between theoutlet 9 of the mixing device 1 (or of the last mixing device 1) and thetank 24. Moreover, advantageously, astirrer 26 is mounted in thetank 24 for mixing the mixture contained therein, before the mixture is sent to themixing device 1. - In the preferred embodiment, illustrated in the accompanying figures, the
tank 24 is equipped with one ormore delivery openings 27 positioned at its bottom portion, and thestirrer 26 is positioned near the one ormore delivery openings 27, in particular just above them. In the case of the embodiment illustrated in the accompanying figures, thestirrer 26 consists of a plurality ofangled vanes 28, which are fixed to avertical shaft 29 which passes through theentire tank 24 and which is driven at the top by an auxiliaryelectric motor 30 of theapparatus 22. Thevanes 28 extend downward from a lower end of thevertical shaft 29, and each of them is adjacent to an underlyingconical wall 31 of thetank 24, whose axis coincides with the axis of thevertical shaft 29. The one ormore delivery openings 27 which put thetank 24 in fluid communication with thefeed duct 19 are made along the perimeter of the lower part of theconical wall 31. It should be noticed that, advantageously, at thestirrer 26, the lateral wall of thetank 24 is near the conical wall 31 (in the embodiment illustrated this stretch of lateral wall is a cylindrical wall with internal diameter equal to the external diameter of the base of the conical wall 31). - Indeed, advantageously, the
tank 24 has a funnel-shaped lateral wall 32 with a cylindrical-shapedupper containment part 33 and alower part 34 which is also cylindrical which houses thestirrer 26. - Moreover, preferably, the
stirrer 26 is activated with a speed of rotation of between 150 and 500 revolutions per minute, and/or with a maximum tangential speed (at the lower tip of the vanes 28) of between 3 and 50 m/s. As regards operation of thecentrifugal impeller 14 of themixing device 1, abelt drive 35 connects the drivingshaft 4 to a mainelectric motor 36. - As is schematically illustrated in
Figure 10 and 11 , in a preferred embodiment of this invention, thereturn duct 25 comprises amain duct 37 connected to theoutlet 9 of themixing device 1, from which main duct a plurality oftubes 38 branches in parallel, those tubes reaching thetank 24 at different heights (heights measured vertically relative to a common reference). - Moreover, each
tube 38 opens into thetank 24 at the cylindrical lateral wall 32 and according to an introducing line at a tangent to the cylindrical lateral wall 32 (Figure 11 ). - Depending on requirements, at a predetermined height there may be a
single tube 38 which enters thetank 24, just as it may be the case that thetubes 38 are grouped in groups, with thetubes 38 of each group opening into thetank 24 at the same height, and thetubes 38 of different groups in contrast opening into thetank 24 at different heights.Figure 11 schematically illustrates a group comprising threetubes 38 which enter thetank 24 at the same height. - Moreover, preferably, the
tubes 38 are not all the same as each other; thetubes 38 which open into the tank at a predetermined height have larger cross-sections than thetubes 38 which open into the tank at lower heights. Moreover, in the preferred embodiment, thereturn duct 25 is as a whole suitable for dividing the flow rate of fluid which passes through it, in such a way that the speed of the mixture which enters thetank 24 through thetubes 38 located at a predetermined height, is greater than the speed of the mixture which enters thetank 24 through thetubes 38 located at higher heights. - Operation of the
apparatus 22 and of themixing device 1 described above correspond to specific embodiments respectively of the entire method for producing cement slurry according to this invention and of several steps thereof. - In its most general embodiment, the method comprises first the operating step of incorporating a predetermined quantity of powdered cement, and additives if necessary, in a predetermined volume of water, creating a mixture. During implementation of this step it is appropriate to pay attention to the fact that the cement powder (and additives if necessary) mix with the water, avoiding, or in any case minimising, the formation of lumps or the powder floating on the water. Since the step of incorporating the cement powder in the water while avoiding lumps and floating is in itself part of the normal know-how of the cement slurry production sector, it will not be described in further detail herein.
- Once the cement powder has been incorporated in the water and the mixture has been formed, the mixture is subjected to a mixing step (carried out with the
stirrer 26 in theapparatus 22 described above) and, then, to a step during which the mixture is fed along a duct (thefeed duct 19 in theapparatus 22 described above) and is fed to a centrifugal impeller 14 (that of themixing device 1 described above). - However, in accordance with this invention, at mixture entry into the
centrifugal impeller 14, there is a step of varying the pressure and the average feed speed of the mixture, during which the average feed speed of the mixture is reduced, with simultaneous generation of an increase in the pressure of the mixture which will strike thecentrifugal impeller 14. Preferably, the pressure increase which is generated during this step is between 0.1 and 1 bar. - Finally, the method comprises a step during which the mixture exiting the
centrifugal impeller 14 is forced through a fixed piercedwall 10 which radially surrounds thecentrifugal impeller 14, partly reducing its tangential motion components and increasing the counter-pressure downstream of the self-samecentrifugal impeller 14. - In most embodiments, the steps described above of feeding the mixture, reducing the speed, increasing the pressure and pushing the mixture, are repeated a plurality of times. Advantageously, the repetition may be performed either by making the mixture circulate a plurality of times through the
same mixing device 1, or making it pass in sequence throughvarious mixing devices 1 in series. - Particularly in the case of use of multiple passes in a
single mixing device 1, it is advantageously the case that the step of mixing the mixture is also repeated before each repetition of the step of feeding the mixture. Moreover, in the preferred embodiment, the (or each) step of mixing the mixture is advantageously carried out using astirrer 26 located in a lower part of acylindrical tank 24 having a predetermined internal diameter, and keeping a height of the mixture above thestirrer 26 which is in a ratio relative to the internal diameter, of between 3 to 1 and 5 to 1. - This invention brings important advantages.
- First, thanks to this invention it has been possible to provide a method for producing cement slurry, and to make a device for mixing cement slurry, which according to the results of experimental tests carried out by the Applicant, allow the obtainment of cement slurries with optimum characteristics in terms of both workability (consistency) and cohesion, and of mechanical properties of the product after drying, using quantities of cement powder significantly lower than in the methods and devices currently commonly used in the sector.
- Second, thanks to this invention it is possible to produce cement slurries of optimum quality in shorter times than in the plants commonly used. Therefore, thanks to this invention, it has been possible to provide a method for producing cement slurry, and to make a device for mixing cement slurry, which allow the obtainment of greater economies in the production of cement slurry and if necessary of concrete than has been possible until now, as well as allowing a more favourable water/cement ratio (understood to be the quantity by weight) than the prior art methods and devices, by virtue of the improved homogenisation which can be achieved between cement and water.
- Finally, it should be noticed that this invention is relatively easy to produce and that even the cost linked to implementing the invention is not very high. The invention described above may be modified and adapted in several ways without thereby departing from the scope of the inventive concept.
- All details of the invention may be substituted with other technically equivalent elements and the materials used, as well as the shapes and dimensions of the various components, may vary according to requirements.
Claims (17)
- A device for mixing cement slurry, comprising:a containment structure (2) which forms a mixing chamber (3) inside it;a driving shaft (4) mounted through the containment structure (2), and which has a first end (5) positioned in the mixing chamber (3), and a second end (6) outside the containment structure (2) and in use connectable to a driving motor, the driving shaft (4) having an axis of rotation (41);a pierced wall (10) mounted in the mixing chamber (3), the pierced wall (10) being centred on the axis of rotation (41) and dividing the mixing chamber (3) into an inner part (11) and an annular outer part (12) which are coaxial; anda centrifugal impeller (14), fixed to the first end (5) of the driving shaft (4) and positioned in the inner part (11) of the mixing chamber (3), in use the centrifugal impeller (14) forcing a water-based mixture to pass through the pierced wall (10);wherein moreover:the containment structure (2) comprises an inlet (8), centred relative to the axis of rotation (41) and facing the inner part (11) of the mixing chamber (3), and an outlet (9) facing the outer part (12) of the mixing chamber (3), the pierced wall (10) intercepting a fluid path which extends from the inlet (8) to the outlet (9);a feed duct (19) is joined to the inlet (8); andthe feed duct (19) and/or the inlet (8) are shaped in such a way as to form at least one introducing duct (20) with cross-section increasing towards the centrifugal impeller (14), directly facing the inner part (11) of the mixing chamber (3).
- The device according to claim 1, wherein the pierced wall (10) has frustoconical extension coaxial with the axis of rotation (41), with a larger base of the truncated cone towards the inlet (8).
- The device according to claim 1 or 2, wherein the pierced wall (10) has a plurality of evenly distributed through holes (13), and/or has a plurality of through holes (13) each with a passage area of between 40 and 200 mm2, preferably between 60 and 130 mm2, and/or has a ratio of pierced surface area to total surface area of between 1 to 5 and 1 to 3.
- The device according to any of claims 1 to 3, wherein the centrifugal impeller (14) comprises a plurality of blades (15), each having a radially external edge which is substantially shaped to match the pierced wall (10) and near it.
- The device according to any of claims 1 to 4, wherein the centrifugal impeller (14) comprises between 3 and 9 blades (15), and/or has a speed of rotation of between 500 and 5000 revolutions per minute, and/or has a maximum tangential speed of between 10 and 80 m/s.
- The device according to any of claims 1 to 5, wherein the introducing duct (20) is sized in such a way as to cause, in use, an increase in the pressure in the fluid to be mixed which passes through it, of between 0.1 and 1 bar.
- An apparatus for producing cement slurry comprising:at least one first mixing device (1) according to any of the preceding claims; anda feeder (23) of a fluid mixture connected to said feed duct (19).
- The apparatus for producing cement slurry according to claim 7, also comprising, connected to the outlet (9) of the first mixing device (1), one or more further mixing devices (1) mounted in series relative to one another.
- The apparatus for producing cement slurry according to claim 7, wherein the apparatus (22) is of the batch type, wherein the feeder (23) comprises at least one tank (24), at least one return duct (25) connected between the outlet (9) of the mixing device (1) and the tank (24), and a stirrer (26) mounted in the tank (24), and wherein the tank (24) is connected to the feed duct (19).
- The apparatus for producing cement slurry according to claim 9, wherein the tank (24) is equipped with one or more delivery openings (27) positioned at its bottom portion, and wherein the stirrer (26) is positioned near the delivery opening.
- The apparatus for producing cement slurry according to claim 9 or 10, wherein the tank (24) has a cylindrical lateral wall (32), wherein the return duct (25) comprises a main duct (37) connected to the outlet (9) from which main duct a plurality of tubes (38) branches in parallel, and wherein each tube (38) opens into the tank (24), at the cylindrical lateral wall (32) and according to an introducing line at a tangent to the cylindrical lateral wall (32).
- The apparatus for producing cement slurry according to claim 11, wherein said tubes (38) are grouped in groups, wherein the tubes (38) of each group open into the tank (24) at the same height, wherein the tubes (38) of different groups open into the tank (24) at different heights, and wherein the tubes (38) which open into the tank at greater heights, have larger cross-sections than the tubes (38) which open into the tank at lower heights.
- A method for producing cement slurry comprising the operating steps of:incorporating a predetermined quantity of powdered cement, and additives if necessary, in a predetermined volume of water, creating a mixture;mixing the mixture;then feeding the mixture along a duct for feeding it to a centrifugal impeller (14);at mixture entry into the centrifugal impeller (14), reducing the average feed speed of the mixture and generating an increase in the pressure of the mixture; andby means of the centrifugal impeller (14), pushing the mixture through a fixed pierced wall (10) which radially surrounds the centrifugal impeller (14).
- The method according to claim 13, wherein the steps of feeding the mixture, reducing the speed, increasing the pressure and pushing the mixture, are repeated a plurality of times.
- The method according to claim 14, wherein the step of mixing the mixture is also repeated before each repetition of the step of feeding the mixture.
- The method according to claim 15, wherein the step of mixing the mixture is carried out using a stirrer (26) located in a lower part of a cylindrical tank (24) having an internal diameter, and keeping a height of the mixture above the stirrer (26) which is in a ratio relative to the internal diameter, of between 3 to 1 and 5 to 1.
- The method according to any of claims 13 to 16, wherein during the step of generating an increase in the pressure of the mixture the pressure is increased by a value of between 0.1 and 1 bar.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT102018000010036A IT201800010036A1 (en) | 2018-11-05 | 2018-11-05 | DEVICE FOR THE MIXING OF CEMENTITIOUS SLURRY, AND METHOD AND EQUIPMENT FOR THE PRODUCTION OF CEMENTITIOUS SLURRY |
Publications (2)
Publication Number | Publication Date |
---|---|
EP3646942A1 true EP3646942A1 (en) | 2020-05-06 |
EP3646942B1 EP3646942B1 (en) | 2021-12-01 |
Family
ID=65409274
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP19204692.8A Active EP3646942B1 (en) | 2018-11-05 | 2019-10-22 | Device for mixing cement slurry, and method and apparatus for producing cement slurry |
Country Status (2)
Country | Link |
---|---|
EP (1) | EP3646942B1 (en) |
IT (1) | IT201800010036A1 (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113134908A (en) * | 2021-05-26 | 2021-07-20 | 铜陵有色股份安庆月山矿业有限公司 | A compounding device for preparing mine underground filling mortar |
CN113752380A (en) * | 2021-09-08 | 2021-12-07 | 金川集团股份有限公司 | Negative pressure type cement paste mixer and cement paste preparation method |
CN114953179A (en) * | 2022-06-08 | 2022-08-30 | 中国建筑第五工程局有限公司 | Blending device is used in preparation of gypsum base light plastering mortar |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4904089A (en) * | 1988-05-16 | 1990-02-27 | Standard Concrete Products, Inc. | Particle wetting process and apparatus |
WO2001028671A1 (en) * | 1999-10-19 | 2001-04-26 | Westpark Financial Group S.A.H. | Hydraulic shock rotary apparatus |
US20080236160A1 (en) * | 2007-03-29 | 2008-10-02 | Victor Nikolaevich Glotov | Continuous flow sonic reactor |
US20150266206A1 (en) * | 2014-03-20 | 2015-09-24 | Annix Systems Ltd | Colloidal Mixing Method for Slurries |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE8618798U1 (en) * | 1986-07-12 | 1987-02-05 | Fried. Krupp Gmbh, 4300 Essen, De |
-
2018
- 2018-11-05 IT IT102018000010036A patent/IT201800010036A1/en unknown
-
2019
- 2019-10-22 EP EP19204692.8A patent/EP3646942B1/en active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4904089A (en) * | 1988-05-16 | 1990-02-27 | Standard Concrete Products, Inc. | Particle wetting process and apparatus |
WO2001028671A1 (en) * | 1999-10-19 | 2001-04-26 | Westpark Financial Group S.A.H. | Hydraulic shock rotary apparatus |
US20080236160A1 (en) * | 2007-03-29 | 2008-10-02 | Victor Nikolaevich Glotov | Continuous flow sonic reactor |
US20150266206A1 (en) * | 2014-03-20 | 2015-09-24 | Annix Systems Ltd | Colloidal Mixing Method for Slurries |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113134908A (en) * | 2021-05-26 | 2021-07-20 | 铜陵有色股份安庆月山矿业有限公司 | A compounding device for preparing mine underground filling mortar |
CN113752380A (en) * | 2021-09-08 | 2021-12-07 | 金川集团股份有限公司 | Negative pressure type cement paste mixer and cement paste preparation method |
CN114953179A (en) * | 2022-06-08 | 2022-08-30 | 中国建筑第五工程局有限公司 | Blending device is used in preparation of gypsum base light plastering mortar |
Also Published As
Publication number | Publication date |
---|---|
IT201800010036A1 (en) | 2020-05-05 |
EP3646942B1 (en) | 2021-12-01 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
EP3646942B1 (en) | Device for mixing cement slurry, and method and apparatus for producing cement slurry | |
KR101566240B1 (en) | Aeration impeller and agitator for water treatment having the same | |
CN211329377U (en) | Emulsified asphalt reaction kettle | |
US4357111A (en) | Continuous mixing device and process | |
US9169505B2 (en) | High solids enzyme reactor mixer with vertical paddle and method | |
CN207929074U (en) | Powder and oil material mixer | |
CN211612398U (en) | Big monomer mixing stirring equipment | |
CN216367573U (en) | Double-spiral cone dye mixing device | |
US3871625A (en) | Continuous flow jet mixer | |
CN111251486A (en) | Mixing equipment for producing eraser | |
PL124781B1 (en) | Method of continuously mixing together pulverized solids and liquids and vertical mixer therefor | |
CN107261948A (en) | It is a kind of to facilitate the agitating device fed in the process of running | |
CN207591684U (en) | A kind of high-speed mixer | |
WO2022202489A1 (en) | Crystallization device, crystallization system, and crystallization method | |
CN102513016B (en) | L-type two-stage homogenizer | |
RU2686944C1 (en) | Centrifugal mixer for loose materials | |
CN211415830U (en) | Be used for plastic granules production mixer | |
US3318579A (en) | Apparatus for mixing floury materials such as plaster | |
CN208302709U (en) | Produce the apparatus for feeding of chelating agent | |
CN110370451A (en) | Continuous mixer is used in a kind of mixing of multicomponent high viscosity material containing sand material | |
CN205614922U (en) | Exit mechanism of mixing head in polyurethane blendor | |
CN219209738U (en) | Quantitative mixing equipment | |
CN220425072U (en) | Feed mixing stirring device | |
CN210905993U (en) | A quick homogenization device for macromolecular material | |
CN209362397U (en) | Silk fiber mixing impurity removal mechanism |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
|
STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE APPLICATION HAS BEEN PUBLISHED |
|
AK | Designated contracting states |
Kind code of ref document: A1 Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR |
|
AX | Request for extension of the european patent |
Extension state: BA ME |
|
RIN1 | Information on inventor provided before grant (corrected) |
Inventor name: SPANOS, ODYSSEAS Inventor name: CARLOTTO, MARIO FLAVIO Inventor name: BARAGETTI, SERGIO |
|
STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: REQUEST FOR EXAMINATION WAS MADE |
|
17P | Request for examination filed |
Effective date: 20201103 |
|
RBV | Designated contracting states (corrected) |
Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR |
|
RIC1 | Information provided on ipc code assigned before grant |
Ipc: B28C 5/12 20060101ALI20210325BHEP Ipc: B28C 5/08 20060101ALI20210325BHEP Ipc: B28C 9/00 20060101ALI20210325BHEP Ipc: B01F 7/00 20060101ALI20210325BHEP Ipc: B01F 5/10 20060101AFI20210325BHEP |
|
GRAP | Despatch of communication of intention to grant a patent |
Free format text: ORIGINAL CODE: EPIDOSNIGR1 |
|
STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: GRANT OF PATENT IS INTENDED |
|
INTG | Intention to grant announced |
Effective date: 20210511 |
|
GRAS | Grant fee paid |
Free format text: ORIGINAL CODE: EPIDOSNIGR3 |
|
GRAA | (expected) grant |
Free format text: ORIGINAL CODE: 0009210 |
|
STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE PATENT HAS BEEN GRANTED |
|
REG | Reference to a national code |
Ref country code: DE Ref legal event code: R079 Ref document number: 602019009709 Country of ref document: DE Free format text: PREVIOUS MAIN CLASS: B01F0005100000 Ipc: B01F0025500000 |
|
AK | Designated contracting states |
Kind code of ref document: B1 Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR |
|
REG | Reference to a national code |
Ref country code: GB Ref legal event code: FG4D |
|
REG | Reference to a national code |
Ref country code: AT Ref legal event code: REF Ref document number: 1451232 Country of ref document: AT Kind code of ref document: T Effective date: 20211215 Ref country code: CH Ref legal event code: EP |
|
REG | Reference to a national code |
Ref country code: IE Ref legal event code: FG4D |
|
REG | Reference to a national code |
Ref country code: DE Ref legal event code: R096 Ref document number: 602019009709 Country of ref document: DE |
|
REG | Reference to a national code |
Ref country code: LT Ref legal event code: MG9D |
|
REG | Reference to a national code |
Ref country code: NL Ref legal event code: MP Effective date: 20211201 |
|
REG | Reference to a national code |
Ref country code: AT Ref legal event code: MK05 Ref document number: 1451232 Country of ref document: AT Kind code of ref document: T Effective date: 20211201 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: RS Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: LT Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: FI Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: BG Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20220301 Ref country code: AT Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: SE Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: PL Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: NO Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20220301 Ref country code: LV Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: HR Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: GR Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20220302 Ref country code: ES Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: NL Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: SM Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: SK Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: RO Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: PT Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20220401 Ref country code: EE Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: CZ Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 |
|
REG | Reference to a national code |
Ref country code: DE Ref legal event code: R097 Ref document number: 602019009709 Country of ref document: DE |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: IS Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20220401 |
|
PLBE | No opposition filed within time limit |
Free format text: ORIGINAL CODE: 0009261 |
|
STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: DK Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 Ref country code: AL Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 |
|
26N | No opposition filed |
Effective date: 20220902 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: SI Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: MC Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 |
|
P01 | Opt-out of the competence of the unified patent court (upc) registered |
Effective date: 20230502 |
|
REG | Reference to a national code |
Ref country code: BE Ref legal event code: MM Effective date: 20221031 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: LU Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20221022 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: BE Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20221031 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: IE Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES Effective date: 20221022 |
|
PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: GB Payment date: 20231024 Year of fee payment: 5 |
|
PGFP | Annual fee paid to national office [announced via postgrant information from national office to epo] |
Ref country code: IT Payment date: 20231024 Year of fee payment: 5 Ref country code: FR Payment date: 20231026 Year of fee payment: 5 Ref country code: DE Payment date: 20231027 Year of fee payment: 5 Ref country code: CH Payment date: 20231102 Year of fee payment: 5 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: HU Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT; INVALID AB INITIO Effective date: 20191022 |
|
PG25 | Lapsed in a contracting state [announced via postgrant information from national office to epo] |
Ref country code: CY Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT Effective date: 20211201 |