EP3038757B1 - Method and apparatus for treating a feed stream for a flotation device - Google Patents
Method and apparatus for treating a feed stream for a flotation device Download PDFInfo
- Publication number
- EP3038757B1 EP3038757B1 EP14790720.8A EP14790720A EP3038757B1 EP 3038757 B1 EP3038757 B1 EP 3038757B1 EP 14790720 A EP14790720 A EP 14790720A EP 3038757 B1 EP3038757 B1 EP 3038757B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- dilution water
- feed stream
- water stream
- stream
- microbubbles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000005188 flotation Methods 0.000 title claims description 100
- 238000000034 method Methods 0.000 title claims description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 114
- 238000010790 dilution Methods 0.000 claims description 106
- 239000012895 dilution Substances 0.000 claims description 106
- 239000002245 particle Substances 0.000 claims description 90
- 239000007787 solid Substances 0.000 claims description 57
- 239000003153 chemical reaction reagent Substances 0.000 claims description 54
- 239000007789 gas Substances 0.000 claims description 32
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 28
- 239000011261 inert gas Substances 0.000 claims description 27
- 239000012530 fluid Substances 0.000 claims description 20
- 229910052757 nitrogen Inorganic materials 0.000 claims description 14
- 230000005484 gravity Effects 0.000 claims description 8
- 239000001307 helium Substances 0.000 claims description 7
- 229910052734 helium Inorganic materials 0.000 claims description 7
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 claims description 7
- 238000011144 upstream manufacturing Methods 0.000 claims description 5
- 230000000712 assembly Effects 0.000 claims description 2
- 238000000429 assembly Methods 0.000 claims description 2
- 239000003570 air Substances 0.000 description 66
- 229910052500 inorganic mineral Inorganic materials 0.000 description 34
- 239000011707 mineral Substances 0.000 description 34
- 235000010755 mineral Nutrition 0.000 description 34
- 239000002002 slurry Substances 0.000 description 20
- 238000000227 grinding Methods 0.000 description 8
- 239000012141 concentrate Substances 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- 238000011084 recovery Methods 0.000 description 6
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 5
- 229910052737 gold Inorganic materials 0.000 description 5
- 239000010931 gold Substances 0.000 description 5
- 239000007788 liquid Substances 0.000 description 5
- 230000002209 hydrophobic effect Effects 0.000 description 4
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 description 4
- 229910052961 molybdenite Inorganic materials 0.000 description 3
- 230000003134 recirculating effect Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 238000005273 aeration Methods 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000011362 coarse particle Substances 0.000 description 2
- 239000011246 composite particle Substances 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 239000006260 foam Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229910052750 molybdenum Inorganic materials 0.000 description 2
- 239000011733 molybdenum Substances 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 238000009420 retrofitting Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000011143 downstream manufacturing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010423 industrial mineral Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000006194 liquid suspension Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000011555 saturated liquid Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D1/00—Flotation
- B03D1/02—Froth-flotation processes
- B03D1/025—Froth-flotation processes adapted for the flotation of fines
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/0084—Enhancing liquid-particle separation using the flotation principle
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D1/00—Flotation
- B03D1/02—Froth-flotation processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/28—Mechanical auxiliary equipment for acceleration of sedimentation, e.g. by vibrators or the like
- B01D21/286—Means for gentle agitation for enhancing flocculation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D1/00—Flotation
- B03D1/02—Froth-flotation processes
- B03D1/023—Carrier flotation; Flotation of a carrier material to which the target material attaches
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D1/00—Flotation
- B03D1/14—Flotation machines
- B03D1/16—Flotation machines with impellers; Subaeration machines
- B03D1/18—Flotation machines with impellers; Subaeration machines without air supply
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D1/00—Flotation
- B03D1/14—Flotation machines
- B03D1/24—Pneumatic
- B03D1/247—Mixing gas and slurry in a device separate from the flotation tank, i.e. reactor-separator type
Definitions
- WO 2012/061897 A1 discloses a method and apparatus for treating a feed stream in a flotation device comprising a tank and an impeller placed in the tank.
- the apparatus 1 also includes reagent inlets 15, 16 located at selected points of the dilution water pipe 5.
- the reagent inlet in the form of a Venturi pipe 15 delivers frother reagents into the dilution water stream 9 from a frother reagent line 17.
- the frother reagents in the dilution water facilitates microbubble formation and also reduces the surface tension of the microbubbles created by the air sparge 6, preventing the microbubbles 8 from merging or coalescing into larger bubbles once they enter the feed pipe 4.
- the frother Venturi pipe 15 delivers the frother reagents upstream of the air sparge 6 so as to prime the dilution water stream for microbubble generation.
- the skim air flotation cell 3 operates with a near zero froth depth, unlike flotation devices employing a mechanical agitator, so that the targeted solids particles 10 have a chance to be recovered directly into the launder 29 and not be potentially lost if there was a deep froth zone formed where coarse particles will readily detach.
- the froth surface is about 0 to 25 mm in depth, but should be very shallow and some slurry will overflow at times into the launder 29. Hence, the coarser solid particles do not drop back into the pulp zone as they are aided by the added buoyancy of the air bubbles plus the upward fluid velocity of the slurry provided by the auxiliary agitator 30c.
- any of the features in the preferred embodiments of the invention can be combined together and are not necessarily applied in isolation from each other.
- the feature of the microbubble generator being a cavitation tube and pump assembly and the feature of an angled feed pipe can be combined into a single apparatus. Similar combinations of two or more features from the above described embodiments or preferred forms of the invention can be readily made by one skilled in the art.
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Water Treatments (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FI20135868A FI20135868L (fi) | 2013-08-28 | 2013-08-28 | Menetelmä ja laite syöttövirtauksen käsittelemiseksi flotaatiolaitteeseen |
PCT/IB2014/064105 WO2015028958A1 (en) | 2013-08-28 | 2014-08-28 | Method and apparatus for treating a feed stream for a flotation device |
Publications (2)
Publication Number | Publication Date |
---|---|
EP3038757A1 EP3038757A1 (en) | 2016-07-06 |
EP3038757B1 true EP3038757B1 (en) | 2022-06-08 |
Family
ID=49150971
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP14790720.8A Active EP3038757B1 (en) | 2013-08-28 | 2014-08-28 | Method and apparatus for treating a feed stream for a flotation device |
Country Status (11)
Country | Link |
---|---|
US (1) | US10569196B2 (fi) |
EP (1) | EP3038757B1 (fi) |
AU (1) | AU2014313771B2 (fi) |
CA (1) | CA2922218C (fi) |
CL (1) | CL2016000418A1 (fi) |
EA (1) | EA029754B1 (fi) |
FI (1) | FI20135868L (fi) |
NZ (1) | NZ717343A (fi) |
PE (1) | PE20160233A1 (fi) |
WO (1) | WO2015028958A1 (fi) |
ZA (1) | ZA201601439B (fi) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA3033482C (en) * | 2016-08-15 | 2023-08-01 | Outotec (Finland) Oy | Flotation method |
EP3512971B1 (en) | 2016-09-14 | 2020-11-04 | Outotec (Finland) Oy | Method for recovering precious metal |
CA2992652C (en) | 2017-01-23 | 2021-03-23 | Jun Long | Nanobubble aided bitumen extraction from oil sand |
EP3743213A4 (en) * | 2018-01-23 | 2021-09-08 | Outotec (Finland) Oy | FLOTATION LINE |
RU2736287C1 (ru) * | 2019-11-01 | 2020-11-13 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Санкт-Петербургский государственный технологический институт (технический университет)" | Микрореактор с закрученными потоками растворов реагентов |
RU2748486C1 (ru) * | 2020-03-20 | 2021-05-26 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Санкт-Петербургский государственный технологический институт (технический университет)" | Микрореактор-смеситель многоступенчатый с закрученными потоками |
US20230348811A1 (en) * | 2022-04-29 | 2023-11-02 | Quaker Chemical Corporation | Systems and Methods for Removing Micro-Particles from a Metalworking Fluid |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3787316A (en) * | 1970-01-29 | 1974-01-22 | Fmc Corp | Foam flotation concentration of sewage |
WO2004082841A1 (en) * | 2003-03-17 | 2004-09-30 | Outokumpu Technology Oy | Auxiliary agitator for a flotation device |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB694918A (en) * | 1951-02-23 | 1953-07-29 | F S Gibbs Inc | Diffusion of gases in liquids |
DE3032887A1 (de) * | 1979-09-10 | 1981-04-02 | Shinryo Air Conditioning Co., Ltd., Tokyo | Verfahren und vorrichtung zum eindicken von schlamm |
US4417985A (en) * | 1981-11-06 | 1983-11-29 | James Keane | Treatment of waters with broad spectrum contaminants |
JPS6044085A (ja) * | 1983-08-22 | 1985-03-08 | Shinryo Air Conditioning Co Ltd | 汚泥の濃縮方法 |
US4738784A (en) * | 1986-07-03 | 1988-04-19 | Kazutoyo Sugihara | Flotation device |
AT410405B (de) | 2001-09-17 | 2003-04-25 | Andritz Ag Maschf | Verfahren und vorrichtung zur abtrennung von störstoffen aus suspensionen durch flotation |
FI20012538A (fi) | 2001-12-21 | 2003-06-22 | Outokumpu Oy | Menetelmä ja laitteisto vaahdotuksen tehostamiseksi |
DE10312670A1 (de) | 2003-03-21 | 2004-10-07 | Friz Biochem Gmbh | Substrat zur kontrollierten Benetzung vorbestimmter Benetzungsstellen mit kleinen Flüssigkeitsvolumina, Substratabdeckung und Flusskammer |
ITVI20070133A1 (it) | 2007-05-09 | 2008-11-10 | Comer Spa | Cella di flottazione perfezionata per la depurazione di sospensioni fibrose |
TWI580778B (zh) * | 2007-06-19 | 2017-05-01 | 再生海藻能源公司 | 微藻類調理及濃縮的方法 |
EP2450106B1 (de) | 2010-11-03 | 2016-06-01 | Primetals Technologies Germany GmbH | Flotationsapparat und Flotationsverfahren |
WO2012061897A1 (en) | 2010-11-11 | 2012-05-18 | Minetometal Pty Ltd | Separation and recovery of bubble particle aggregates |
AU2012100021B4 (en) * | 2012-01-10 | 2015-05-28 | Eriez Manufacturing Co. | Cavitation tube sparging system |
FI124687B (fi) | 2013-08-30 | 2014-12-15 | Outotec Finland Oy | Menetelmä ja hydraulinen alusta metallien elektrolyyttiseen rikastukseen eli elektroraffinointiin tarkoitettujen elektrolyysikennotankkien asentamiseksi säiliöhallissa sijaitsevalle tukirakenteelle ja hydraulisen alustan käyttö menetelmässä |
-
2013
- 2013-08-28 FI FI20135868A patent/FI20135868L/fi not_active Application Discontinuation
-
2014
- 2014-08-28 NZ NZ717343A patent/NZ717343A/en unknown
- 2014-08-28 WO PCT/IB2014/064105 patent/WO2015028958A1/en active Application Filing
- 2014-08-28 PE PE2016000297A patent/PE20160233A1/es active IP Right Grant
- 2014-08-28 AU AU2014313771A patent/AU2014313771B2/en active Active
- 2014-08-28 EA EA201690257A patent/EA029754B1/ru not_active IP Right Cessation
- 2014-08-28 US US14/914,537 patent/US10569196B2/en active Active
- 2014-08-28 CA CA2922218A patent/CA2922218C/en active Active
- 2014-08-28 EP EP14790720.8A patent/EP3038757B1/en active Active
-
2016
- 2016-02-24 CL CL2016000418A patent/CL2016000418A1/es unknown
- 2016-03-02 ZA ZA2016/01439A patent/ZA201601439B/en unknown
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3787316A (en) * | 1970-01-29 | 1974-01-22 | Fmc Corp | Foam flotation concentration of sewage |
WO2004082841A1 (en) * | 2003-03-17 | 2004-09-30 | Outokumpu Technology Oy | Auxiliary agitator for a flotation device |
Also Published As
Publication number | Publication date |
---|---|
EP3038757A1 (en) | 2016-07-06 |
CL2016000418A1 (es) | 2016-10-14 |
EA029754B1 (ru) | 2018-05-31 |
CA2922218C (en) | 2022-01-04 |
FI20135868L (fi) | 2015-03-01 |
ZA201601439B (en) | 2020-05-27 |
AU2014313771B2 (en) | 2016-10-27 |
US20160214036A1 (en) | 2016-07-28 |
NZ717343A (en) | 2020-03-27 |
US10569196B2 (en) | 2020-02-25 |
CA2922218A1 (en) | 2015-03-05 |
PE20160233A1 (es) | 2016-05-10 |
AU2014313771A1 (en) | 2016-03-24 |
EA201690257A1 (ru) | 2016-08-31 |
WO2015028958A1 (en) | 2015-03-05 |
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