EP2326595A1 - Optimized water treatment installation and process - Google Patents
Optimized water treatment installation and processInfo
- Publication number
- EP2326595A1 EP2326595A1 EP09804537A EP09804537A EP2326595A1 EP 2326595 A1 EP2326595 A1 EP 2326595A1 EP 09804537 A EP09804537 A EP 09804537A EP 09804537 A EP09804537 A EP 09804537A EP 2326595 A1 EP2326595 A1 EP 2326595A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- water
- filtration
- value
- units
- filtration units
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 176
- 238000000034 method Methods 0.000 title claims abstract description 57
- 238000009434 installation Methods 0.000 title claims abstract description 26
- 230000008569 process Effects 0.000 title claims abstract description 14
- 238000001914 filtration Methods 0.000 claims abstract description 143
- 238000005273 aeration Methods 0.000 claims description 21
- 230000008859 change Effects 0.000 claims description 10
- 230000003213 activating effect Effects 0.000 claims description 6
- 238000005374 membrane filtration Methods 0.000 claims description 6
- 238000004140 cleaning Methods 0.000 claims description 5
- 238000012423 maintenance Methods 0.000 claims description 5
- 238000012545 processing Methods 0.000 claims description 5
- 239000004793 Polystyrene Substances 0.000 claims description 4
- 229920002223 polystyrene Polymers 0.000 claims description 4
- 239000011324 bead Substances 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 238000009287 sand filtration Methods 0.000 claims description 2
- 238000012986 modification Methods 0.000 abstract description 7
- 230000004048 modification Effects 0.000 abstract description 7
- 239000012528 membrane Substances 0.000 description 75
- 238000004519 manufacturing process Methods 0.000 description 12
- 230000007774 longterm Effects 0.000 description 6
- 230000004907 flux Effects 0.000 description 5
- 238000011161 development Methods 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- 239000004576 sand Substances 0.000 description 4
- 239000010802 sludge Substances 0.000 description 4
- 238000011001 backwashing Methods 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 238000004364 calculation method Methods 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 230000002265 prevention Effects 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 238000005276 aerator Methods 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- 230000002427 irreversible effect Effects 0.000 description 2
- 230000000670 limiting effect Effects 0.000 description 2
- 238000001471 micro-filtration Methods 0.000 description 2
- 238000001728 nano-filtration Methods 0.000 description 2
- 230000035699 permeability Effects 0.000 description 2
- 230000000750 progressive effect Effects 0.000 description 2
- 238000001223 reverse osmosis Methods 0.000 description 2
- 238000000108 ultra-filtration Methods 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000010420 art technique Methods 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 238000009109 curative therapy Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 230000002542 deteriorative effect Effects 0.000 description 1
- 238000011981 development test Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000012510 hollow fiber Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
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- 238000000746 purification Methods 0.000 description 1
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- 230000002829 reductive effect Effects 0.000 description 1
- 230000004043 responsiveness Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D65/00—Accessories or auxiliary operations, in general, for separation processes or apparatus using semi-permeable membranes
- B01D65/10—Testing of membranes or membrane apparatus; Detecting or repairing leaks
- B01D65/109—Testing of membrane fouling or clogging, e.g. amount or affinity
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/008—Control or steering systems not provided for elsewhere in subclass C02F
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/14—Ultrafiltration; Microfiltration
- B01D61/22—Controlling or regulating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D65/00—Accessories or auxiliary operations, in general, for separation processes or apparatus using semi-permeable membranes
- B01D65/10—Testing of membranes or membrane apparatus; Detecting or repairing leaks
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2315/00—Details relating to the membrane module operation
- B01D2315/06—Submerged-type; Immersion type
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/441—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/442—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by nanofiltration
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
- C02F1/444—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by ultrafiltration or microfiltration
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2209/00—Controlling or monitoring parameters in water treatment
- C02F2209/10—Solids, e.g. total solids [TS], total suspended solids [TSS] or volatile solids [VS]
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2209/00—Controlling or monitoring parameters in water treatment
- C02F2209/40—Liquid flow rate
Definitions
- the field of the invention is that of the treatment of water. More specifically, the invention relates to the treatment of wastewater in view of their purification or treatment of water for the purpose of its potabilization, in filtration units.
- the invention relates in particular, but not exclusively, to membrane bioreactors, biological filters (such as Biostyr® marketed by the Applicant), sand filters or membrane filters (such as those that can be used to reverse osmosis, ultrafiltration, nanofiltration or micro filtration).
- biological filters such as Biostyr® marketed by the Applicant
- sand filters or membrane filters (such as those that can be used to reverse osmosis, ultrafiltration, nanofiltration or micro filtration).
- Most of the filtration units used for water treatment include an open or closed vessel that forms a reactor.
- the water to be treated is introduced into this reactor in order to reduce the pollution. For example, it may undergo biological treatment.
- These filtration units may be constituted by membranes or any other filtering material (sand, polystyrene beads, etc.).
- aerators In order to limit the clogging of filtration units, different technologies can be implemented, such as backwashing or the use of aerators in the context of membrane biological reactors. These aerators, generally positioned below the membrane modules, make it possible to inject a gas (mainly air), preferably intermittently into the reactor. This gas rises in the form of bubbles along the membranes and creates on their surface a phenomenon of agitation which tends to limit their clogging. 3.
- a gas mainly air
- the filtration phases can be alternated with: relaxation phases during which the flow through the membranes is stopped; backwashing phases during which water to be treated is injected countercurrently through the filtration material or membranes.
- phase are intended to remove the cake of particles that has deposited on the surface of the membranes.
- curative treatment phases for example maintenance cleaning or soaking phases with reagents.
- the maintenance of filtration units then imposes replacements of the filtration material, a relatively large workforce and consequently generates significant costs.
- the technique described in this document proposes to control various parameters of a water treatment process according to the value of the membrane resistance calculated during the treatment.
- the value of the resistance is compared with two resistance threshold values: an upper limit value which corresponds to the maximum resistance value tenable by the membrane; a lower limit value below which it is possible to change the controlled parameters in order to achieve energy savings.
- the aeration rate is increased so as to limit clogging.
- the resistance value is lower than the lower limit value, which means that the treatment of the water causes a weak clogging and therefore the need for aeration of the membranes is low, the aeration rate is reduced so as to allow to save energy.
- the value of the resistor is between the upper limit and the lower limit, which means that the system is working properly, the controlled parameters are not modified
- Parameters other than the aeration rate can also be controlled. These are organized hierarchically and are modified in a iterative, one after the other, until a satisfactory level of performance is achieved.
- the reference values at which the measured resistance value is compared are determined by experience in processing. a reference water in a typical installation.
- these values determined by experiment lead to optimally exploit the membranes used in this typical installation during the treatment of a water having the qualities of the treated water during the development of the system. .
- the performance of the membranes are not exploited optimally.
- the upper and lower limit values at which the measured resistance is compared are fixed.
- the controlled parameter (s) are modified in such a way that the clogging of the membranes is limited, which implies that the production capacity of the system is limited.
- the quality of the water to be treated is particularly bad, the prevention of clogging membranes will be favored at the expense of production capacity. This can lead to a situation in which the quantity of water produced is less than the needs and therefore insufficient.
- this technique operates iteratively, that is to say that each controlled parameter is modified only if the previous modification of the higher parameter in the hierarchy did not lead to improve the efficiency of the system. This implies that after modifying a first parameter, the impact this change is evaluated. If the desired performance level is not achieved by this change of the first parameter, a second parameter must be changed, this being reiterated until the expected performance level is reached.
- the modifications made to improve the performance of the system do not exert any real positive impact due to the lack of responsiveness of the system.
- an object of the invention is to provide a water treatment method that optimally utilizes the filtration units.
- an objective of the invention is to provide such a technique that makes it possible to limit the clogging of the filtration units.
- An object of the invention is also to implement such a technique which is particularly effective including during the quality variations of the water to be treated.
- the invention also aims to provide such a technique that allows under most operating conditions to produce a sufficient amount of treated water, that is to say corresponding to the wish.
- a water treatment process in an installation comprising a plurality of filtration units, said method comprising at least one filtration stage. of said water in said filtration units under initial filtration conditions, and a step of optionally changing the value of at least one controlled parameter within a tolerance range.
- such a method comprises: a step of determining the value of at least one information representative of the clogging power of the water to be filtered; a first step of comparing said value of at least one information representative of the clogging power with a predetermined threshold value; a step of determining the limits of said tolerance interval for said at least one controlled parameter according to said first comparison step, said step of determining the value of said at least one information representative of the clogging power of the water to be filtered being obtained by passing said water to be filtered, under conditions different from said initial filtration conditions, through at least one of said filtration units constituting a control filtration unit.
- the characteristic that the water to be filtered passes through the control unit under conditions different from the initial filtration conditions in which it passes through the other filtration units means that the conditions of pressure, flow, duration. .. water transit within the control unit are different from those within the filtration units.
- the invention is based on an original approach to the treatment of water within at least one reactor in which process parameters are controlled and the limits of the tolerance intervals of these parameters are modified as a function of the clogging power of the reactor. the water to be treated.
- this aspect of the invention is particularly interesting insofar as it optimizes the use of the membranes implemented according to operating constraints. Indeed, the fact of determining the clogging power of the water to be filtered and consequently modifying the tolerance interval of the controlled parameter (s) makes it possible to modify the controlled parameter (s) within ranges suitable for the treatment of this water. water through the membranes that are implemented.
- this implementation makes it possible in particular to pass the water to be treated in an accelerated manner through a filtration unit similar to that used to filter the water so as to anticipate the behavior of the filtration modules during treatment water coming into the installation.
- This study then makes it possible to define the limits of the tolerance intervals of the various controlled parameters so that they are adjusted in ranges of values which make it possible to use in an optimal way the resources of the filtration modules taking into account the nature of the water to treat.
- said step of determining the value of an information representative of the clogging power of the water to be filtered comprises the following sub-steps: performing successive filtering cycles of said water through said unit filter filtration; continuously measuring the evolution of the pressure or pressure drop across said control filter unit during each of said filter cycles; varying the value of the flow at which said water passes through said control filtration unit so that said water transits during each of said filtration cycles in a flow whose value is different from the value of the filtration flow of said water in at least one preceding filtration cycle; said information representative of the clogging power of the water to be filtered is the value of the circulation flow of said water recorded during one of said filtration cycles during which said pressure or said pressure drop increases beyond a predetermined threshold.
- the implementation of these steps makes it possible to define the critical flow, that is to say the flow of water passing through a filtration unit beyond which the clogging of this unit becomes irreversible.
- the critical flow is an indicator of the clogging power of the water to be filtered particularly representative and reliable. This technique of determination of the critical flow consequently makes it possible to obtain in a safe and precise manner an image of the clogging power of the water to be filtered.
- a method according to the invention comprises for each of said units: a step of measuring the value of at least one piece of information representative of the resistance of said filtration units; a step of calculating the value of the resistance of said filtration units
- the resistance of a filtration unit is equal to the inverse of its permeability.
- the permeability of a filtration unit is equal to the ratio of the flow of water passing through it to the pressure, the flow being itself equal to the ratio of the filtration rate to the filtration surface.
- the invention is therefore based on the modification of controlled parameters as a function of the value of the resistance of the filtration units. Resistance is indeed an indicator that can effectively monitor the evolution over time clogging of filtration units. According to a preferred aspect of the invention, at least two of said parameters are modified simultaneously.
- This feature ensures that a method according to the invention can effectively manage water quality variations.
- a treatment method according to the invention comprises a step of modifying said resistance value. threshold within a tolerance range.
- a method according to the invention comprises a step of choosing the value of the volume of water to be treated over a given period.
- the process advantageously comprises: a step of measuring the volume of treated water; a third step of comparing the value of said volume of treated water with said selected water volume setpoint value to be processed over a given period; a step of possible correction of said threshold resistance value as a function of said third comparison step.
- the resistance threshold value may be modified upwards so as to allow greater clogging of the membranes. It will then be possible to give priority to the production of water and to produce it so as to satisfy the needs to the detriment of the damage of the filtration units.
- said at least one controlled parameter is a parameter related to the clogging of said filtration units.
- the implementation of the invention thus leads to control, at least to a better extent compared to the techniques of the prior art, the clogging of the filtration units.
- said at least one controlled parameter belongs to the group comprising: the filtration time in each of said filtration units; the filtration flux in each of said filtration units; the relaxation time of said filtration units; the aeration rate of said filtration units; the duration of aeration of said filtration units; the amount of filtration units implemented; activating a backwash cycle; the backwash flow rate, the backwash time, the backwash frequency, the volume of backwash water in each of said filtration units. ; the conversion rate; the opening or closing of a recirculation loop; activating a maintenance cleaning of said filtration units; activating a curative cleaning of said filtration units. Acting on at least one of these parameters makes it possible to control the impact of water treatment on the clogging of the filtration units.
- the present application also relates to an installation for the implementation of such a method.
- An installation of this type comprises: a battery of filtration units and aeration means of said filtration units; first means for withdrawing said water through said battery; means for measuring the resistance of said filtration units; means for measuring the value of information representative of the clogging power of said water to be filtered; means for controlling at least one processing parameter.
- said means for measuring the value of an information representative of the clogging power comprise at least one filtration unit constituting a control filtration unit able to operate under different conditions of said battery and having the same characteristics. said filter units forming said battery, and second means for withdrawing said water through said control unit.
- said filtration units belong to the group comprising: - sand filtration units; membrane filtration units; biological filtration units; filtration units on polystyrene beads.
- the present technique can therefore be implemented for any type of filtration.
- FIG. 1 presents a diagram of an installation according to the invention
- Figure 2 shows a variant of an installation according to the invention
- FIG. 3 illustrates a diagram of the control system of a method according to the invention. 7. Description of an embodiment of the invention
- the invention relates to a method for treating water within a reactor, such as for example a membrane-based biological reactor and in which at least one parameter such as, for example, the aeration rate of the membranes, the flow passing through the membranes ... is controlled in such a way that its value can evolve within a tolerance range. It is noted that this parameter can for example be modified according to the value of the membrane resistance measured in real time.
- the invention is based on the implementation of a step of measuring an information representative of the clogging power and a comparison step of this value with a predetermined threshold value so as to change the limits of the tolerance interval of the controlled parameter (s).
- This step of determining the value of information representative of the clogging power of the water to be filtered is obtained by passing the water to be treated under particular conditions through a control filtration unit.
- This implementation makes it possible in particular to pass the water to be treated in an accelerated manner through a filtration unit similar to that used to filter the water so as to be able to anticipate the behavior of the filtration modules during the treatment of the water. water coming into the facility.
- This study then makes it possible to define the limits of the tolerance intervals of the various controlled parameters so that they are adjusted in ranges of values which make it possible to make optimum use of the resources of the filtration modules taking into account the nature of the water to treat.
- the controlled parameters when the clogging power is lower than a reference value, which means that the quality of the water to be treated is relatively good, the controlled parameters will be likely to evolve within a certain value range. If it is detected that the clogging power of the water to be filtered is greater than a reference value, which means that the quality of the water is deteriorating, the range in which the controlled parameters are likely to evolve will be modified. .
- This aspect of the invention is particularly interesting insofar as it makes it possible to optimize the use of the membranes used as a function of the operating constraints. Indeed, the fact of determining the clogging power of the water to be filtered and consequently modifying the tolerance interval of the controlled parameter (s) makes it possible to modify the controlled parameter (s) within ranges suitable for the treatment of this water. water through the membranes that are implemented.
- the resistance threshold value at which the real-time calculated resistance is compared may be varied. In particular, this value can be chosen, in a tolerance range whose limits will be predetermined, by comparing the flow to be treated over a given period with the flow already treated before the expiry of this period.
- the threshold value of resistance will be raised so as to allow to produce water in the desired quantities, that is to say by exploiting more the capabilities of the membranes. In this case, we favor production over the membranes.
- the setpoints of several controlled parameters may vary simultaneously depending on the value of the resistance of the membranes. This is contrary to the prior art technique in which the controlled parameters are modified one by one in an order of priority and evaluating the impact of each of the modifications until a suitable level of performance is achieved.
- This characteristic of the invention makes it possible to significantly improve the reactivity of the process in the event of variation in the quality of the water to be treated.
- FIG. 1 illustrates a schematic representation of an installation intended for the implementation of a water treatment method according to the invention.
- Such an installation comprises a biological reactor 10 containing water to be treated mixed with activated sludge.
- This biological reactor 10 houses a membrane filtration unit 11.
- This membrane filtration unit 11 can integrate a plurality of membrane modules, for example of the microfiltration, ultrafiltration, nanofiltration or reverse osmosis type. These membrane modules may for example comprise hollow fibers. , flat membranes, tubular membranes or membranes of any other type.
- the biological reactor 10 also houses a control membrane module 12.
- This control membrane module 12 is identical and has the same characteristics as the modules that make up the membrane filtration unit 11.
- Aeration means are provided in a lower portion of the biological reactor 10. These aeration means may take the form of gas injection nozzles 13, preferably air. These nozzles 13 are connected to a booster 14.
- the air injected into the biological reactor 10 provides a function of unclogging and / or preventing clogging of the filtration membranes. In fact, the air injected into the biological reactor 10 rises in the form of bubbles along the membranes so that it causes a stirring phenomenon on their surface. This agitation phenomenon makes it possible to limit the agglomeration of the activated sludge on the membranes and also makes it possible to remove a part of the accumulated deposit on the surface of the membranes, called cake.
- Another aeration device (not shown) provides aeration of activated sludge for biological treatment.
- the membrane filtration unit 11 is connected to a first variable rate filler pump 16.
- the indicator membrane module 12 is connected to a second variable rate filler pump 17.
- This installation further comprises a battery of sensors (not shown) which make it possible to measure various information relating to the state of the system. It comprises in particular sensors which make it possible to measure, for each of the membrane modules of the filtration unit 11, the value of the information needed to calculate their resistance, including transmembrane pressure, flow, temperature. It also includes sensors for measuring all the information needed to calculate the flow through the control module 12, including flow, transmembrane pressure and temperature.
- FIG. 2 illustrates a variant of an installation according to the invention in which a first 20 and a second 21 reactors are implemented.
- the first reactor 20 constitutes an activated sludge basin while the second reactor 21 houses the membrane modules.
- the filtration modules are membrane modules. In variants, it may of course be other type of filtration unit such as sand filters ...
- This installation also comprises means making it possible to control different parameters of the treatment method according to the different measurements made.
- FIG. 3 represents a diagram which illustrates the control and control means of an installation according to the invention, as well as the way in which they interact.
- the method according to the invention allows the control of four parameters: the filtration time; the filtration flow; the relaxation time; the aeration rate of the membranes.
- other parameters can be used like the time and the flow of retro washing ...
- the control means here comprise six regulators (21 to 26). Four of these regulators make it possible to deliver a setpoint for controlling a controlled parameter by comparing the calculated value of the resistance of each of the modules with a predetermined threshold value: the regulator 22 makes it possible to deliver a filtration time setpoint; the regulator 23 makes it possible to deliver a flow setpoint or filtration flow (the flow being the flow rate relative to the filtration surface); the regulator 24 makes it possible to deliver a set of relaxation times; the regulator 25 makes it possible to deliver an aeration flow setpoint.
- the regulator 21 makes it possible to correct the tolerance interval in which the setpoint of each of the controlled parameters delivered by the regulators 22 to 25 must be situated, by comparing information representative of the clogging power of the water to be treated with a predetermined threshold value. .
- the regulator 26 makes it possible to correct the resistance threshold value within an interval whose limits are predetermined, by comparing the volume of water treated over a given period with the volume of water that has actually been treated from the beginning. treatment.
- the calibration of an installation according to the invention comprises the determination of tolerance intervals for each controlled parameter according to the quality of the water to be treated.
- tolerance intervals are determined by experiment taking into account the clogging power of the water to be filtered, which is a parameter representative of the quality of the water to be treated.
- the determination of the clogging power of the water to be filtered is obtained by determining, with the control module, the critical flow, that is to say the flow from which the clogging of the membrane becomes irreversible.
- the determination of the critical flux is obtained by subjecting the control module to a succession of filtration cycles, the value of the flux being increased between each cycle, for example by the implementation of a variable flow rate pump.
- the transmembrane pressure is measured continuously during each filtration cycle. This can for example be achieved by means of a manometer. When it is detected that the transmembrane pressure increases beyond a predetermined threshold, initially set empirically and adjusted case by case, during a filtration cycle, the value of the flow according to which the water to be processed is filtered during this cycle is the critical flow.
- This critical flow determination protocol is just one example.
- it may be planned to carry out, between each filtration cycle, a relaxation phase, or backwashing so as to restore the membrane. It can also be expected that the flow is not systematically increased between two consecutive filter cycles.
- each controlled parameter can be modified by comparing the calculated resistance for each of the membranes to a threshold value.
- the threshold resistance value can vary within a tolerance range whose terminals are predefined.
- the regulator 26 makes it possible to correct the resistance threshold value by comparing the volume of water to be treated over a given period of time.
- the regulator 26 makes it possible to modify the resistance threshold value so as to allow sufficient production of treated water.
- the controller 26 may for example automatically switch between three treatment modes: cautious mode, optimal mode or maximum mode. Each treatment mode has a resistance value. If the quantity of water produced meets the requirements, the regulator 26 will choose to operate in optimal mode.
- the regulator 26 switches to a cautious mode so as to favor the prevention of clogging to the production of the treated water. If, on the contrary, the water is not produced in sufficient quantity, the regulator
- the regulators 22 to 25 then establish a relationship between the calculated resistance and the resistance setpoint delivered by the regulator 26, and issue instructions for each controlled parameter. 7.2.3. Implementation of the process
- the critical flow that represents the clogging power of the water is determined as previously described by the implementation of a succession of filtration phases through the control module.
- the regulator 21 compares the value of the determined critical flux with one or more threshold values so as to modify the limits of the tolerance intervals of each controlled parameter.
- the regulators 22, 23, 24, 25 determine respectively as a function of the resistance of each membrane and the resistance reference which is related to the operating mode engaged by the regulator 26: a filtration time setpoint; a filtration flow set point; a set of relaxation time; an aeration flow instruction.
- the values of these setpoints are included in the tolerance intervals defined by the controller 21.
- the controller 21 changes the limits of the tolerance intervals of each controlled parameter. If the setpoint of one of these parameters is outside its new range, it is modified accordingly. Otherwise, the deposit does not change.
- the regulators 22, 23, 24, 25 will deliver new setpoints located in the new intervals defined by the regulator 21.
- the operator fixes for the day a set of water volume to be treated. The volume of water treated since the morning is calculated during the implementation of the process. If, as the day goes by, a comparison by the regulator 26 of the volume to be treated on the day and the volume actually passed since the beginning of the day makes it possible to detect that the system does not make it possible to produce water in sufficient quantities, the regulator 26 will change the resistance setpoint.
- membrane capacities can be further exploited to increase productivity at the expense of their service life. According to a variant, it can be provided the implementation of two control horizons.
- a control horizon can be implemented to monitor the evolution of clogging.
- a control horizon called “long horizon” can be implemented to monitor the evolution of the volume of water produced. It is noted that the short and long horizons can be linked for example by a multiplier factor relationship.
- Table 1 gathers the data relating to a starting situation called initial situation.
- the standard set of water to be filtered which corresponds to the reference value of the critical flow through the control module, is set at 40 L / h / m 2 .
- the daily volume of water to be treated is set at 100 m 3 / d.
- the long-term sealing setpoint that is to say the resistance for each of the membranes is set at 4 m ' Vj.
- the measurement of the daily volume of treated water makes it possible to determine that it is equal to 110 m Zj, that is to say that it is greater than the set point.
- the starting situation is therefore a situation in which the treatment plant produces more water than necessary without clogging the membranes.
- the cautious mode is then engaged by the regulator 26 and the regulator 21 does not modify the thresholds of the different controlled parameters.
- the critical flux representing the clogging power of the water is now 30 L / h / m 2 . It is therefore lower than the set point which means that the water is more clogging.
- the regulator 21 consequently modifies the tolerance ranges of the various parameters controlled so that their ranges of evolution are restricted to a treatment area more in adequacy with the water to be treated.
- the regulators operate in a conventional manner. It can for example be PID controllers.
- the regulators 22 and 23 do not modify the value of the setpoint they deliver, insofar as it is in the modified range.
- the regulators 24 and 25 respectively modify the value of the setpoint they deliver so that it is in the new interval defined by the regulator 21.
- the regulator 26 compares the volume of treated water with the volume of water to be treated daily.
- the daily volume whose value is now 90 m 3 / d, is below the set point, ie the quantity of water produced is less than necessary.
- the regulator 26 switches on the maximum mode so as to allow sufficient water to be produced by making greater use of the capacity of the installation.
- the regulator 26 then delivers a so-called maximum long-term sealing setpoint within the tolerance range so as to allow greater clogging of the membranes, that is to say to further exploit the capabilities of the membranes in order to produce enough water.
- the regulators 22 to 25 respectively deliver, by comparing the measured value of the long-term clogging with the long-term sealing setpoint delivered by the regulator 26, setpoints included in the intervals defined by the regulator 21 so as to increase the production of treated water.
- the filtration time and the aeration of the membranes are increased by the regulators 22 and 25 within their intervals so as to increase the volume of treated water.
- the controller 21 Since the measurement of the critical flow makes it possible to detect that the pollution has passed, that is to say that the water is filtered better, which occurs when its clogging power (critical flow) becomes equal to the setpoint of type of water to be filtered, the controller 21 changes again the limits of the tolerance intervals of the various controlled parameters.
- Table 3 values after pollution peak treatment
- the treated water is now produced in sufficient quantities.
- the regulator 26 then actuates the optimal mode.
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Water Supply & Treatment (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Organic Chemistry (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
Description
Claims
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0855445A FR2934853B1 (en) | 2008-08-06 | 2008-08-06 | OPTIMIZED WATER TREATMENT PROCESS |
PCT/EP2009/059683 WO2010015543A1 (en) | 2008-08-06 | 2009-07-27 | Optimized water treatment installation and process |
Publications (1)
Publication Number | Publication Date |
---|---|
EP2326595A1 true EP2326595A1 (en) | 2011-06-01 |
Family
ID=40409852
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP09804537A Withdrawn EP2326595A1 (en) | 2008-08-06 | 2009-07-27 | Optimized water treatment installation and process |
Country Status (5)
Country | Link |
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EP (1) | EP2326595A1 (en) |
AU (1) | AU2009278073A1 (en) |
CA (1) | CA2732770A1 (en) |
FR (1) | FR2934853B1 (en) |
WO (1) | WO2010015543A1 (en) |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4482461A (en) * | 1982-12-20 | 1984-11-13 | French Systems, Inc. | Backwash control for constant volume-pressure filtration system |
US6077435A (en) * | 1996-03-15 | 2000-06-20 | Usf Filtration And Separations Group Inc. | Filtration monitoring and control system |
FR2817768B1 (en) * | 2000-12-13 | 2003-08-29 | Lyonnaise Eaux Eclairage | METHOD FOR REGULATING A MEMBRANE FILTRATION SYSTEM |
ES2599640T3 (en) * | 2005-07-12 | 2017-02-02 | Zenon Technology Partnership | Procedure control for a submerged membrane system |
US8007568B2 (en) * | 2006-04-12 | 2011-08-30 | Millipore Corporation | Filter with memory, communication and pressure sensor |
FR2909903B1 (en) * | 2006-12-19 | 2009-02-27 | Degremont Sa | METHOD FOR OPTIMIZED MANAGEMENT OF A FILTRATION UNIT ON MEMBRANE, AND INSTALLATION FOR ITS IMPLEMENTATION |
NL2000586C2 (en) * | 2007-03-30 | 2008-10-02 | Norit Procestechnologie B V | Method for filtering a fluid. |
WO2008132186A1 (en) * | 2007-04-27 | 2008-11-06 | Vlaamse Instelling Voor Technologisch Onderzoek (Vito) | Supervisory control system and method for membrane cleaning |
-
2008
- 2008-08-06 FR FR0855445A patent/FR2934853B1/en not_active Expired - Fee Related
-
2009
- 2009-07-27 AU AU2009278073A patent/AU2009278073A1/en not_active Abandoned
- 2009-07-27 CA CA2732770A patent/CA2732770A1/en not_active Abandoned
- 2009-07-27 WO PCT/EP2009/059683 patent/WO2010015543A1/en active Application Filing
- 2009-07-27 EP EP09804537A patent/EP2326595A1/en not_active Withdrawn
Non-Patent Citations (1)
Title |
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See references of WO2010015543A1 * |
Also Published As
Publication number | Publication date |
---|---|
AU2009278073A1 (en) | 2010-02-11 |
FR2934853B1 (en) | 2012-07-27 |
CA2732770A1 (en) | 2010-02-11 |
WO2010015543A1 (en) | 2010-02-11 |
FR2934853A1 (en) | 2010-02-12 |
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