EP2222826B1 - Method of producing edible oil from rapeseed - Google Patents

Method of producing edible oil from rapeseed Download PDF

Info

Publication number
EP2222826B1
EP2222826B1 EP08827060.8A EP08827060A EP2222826B1 EP 2222826 B1 EP2222826 B1 EP 2222826B1 EP 08827060 A EP08827060 A EP 08827060A EP 2222826 B1 EP2222826 B1 EP 2222826B1
Authority
EP
European Patent Office
Prior art keywords
seeds
oil
seed
rapeseed
exceeding
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
EP08827060.8A
Other languages
German (de)
English (en)
French (fr)
Other versions
EP2222826A2 (en
Inventor
Jerzy Tys
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Instytut Agrofizyki Im Bohdana Dobrzanskiego Polskiej Akademii Nauk
Original Assignee
Instytut Agrofizyki Im Bohdana Dobrzanskiego Polskiej Akademii Nauk
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Instytut Agrofizyki Im Bohdana Dobrzanskiego Polskiej Akademii Nauk filed Critical Instytut Agrofizyki Im Bohdana Dobrzanskiego Polskiej Akademii Nauk
Publication of EP2222826A2 publication Critical patent/EP2222826A2/en
Application granted granted Critical
Publication of EP2222826B1 publication Critical patent/EP2222826B1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/06—Production of fats or fatty oils from raw materials by pressing
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials

Definitions

  • the subject of the invention is a method of producing edible oil from rapeseed.
  • Patent No. PL 186045 gives a method for the isolation of oil from the seeds of oil-bearing plants through expression and extraction of oil from the oil cake, in which the seeds are subjected to expression at temperatures not exceeding 313 K, and the oil cake is subjected to extraction with carbon dioxide, used in amounts up to 50 kg per 1 kg of oil cake under pressure in the range of 5 to 40 MPa, at temperatures up to 363 K, and then from the gas phase, through heating and/or decompression, a mixture of water, oil and wax is obtained, from which oil is isolated through separation of water and wax.
  • Polish parent according to patent application P. 341836 gives a method and an apparatus for the production of edible oil from rapeseed or other oil-bearing plants, in which seeds of oil-bearing plants, after sorting, are dried, fragmented, sifted and, after preparation, fed into an oil expression press. After sorting by means of a sifter, fractions are obtained that differ from one another in grain sizes, and in particular a fraction composed of contaminations, a fraction composed of cleaned seeds, and a fine fraction. Cleaned and sorted rapeseed is dried at a temperature up to 40° C until moisture content between 4.5% and 5.5% is obtained, while the contaminations and fine fraction are diverted to a container.
  • the dried rapeseed is fragmented in a system of rollers, and the fragmented seed is sorted into three fractions with various particle sizes.
  • the usable fraction, containing parenchyma with seed coat is subjected to further diminution in a system of rollers and, ground and containing seed coat, is expressed at ambient temperature using an expression press. Edible oil is obtained after removing solid intrusions from the non-purified oil expressed on the press.
  • the essence of the invention is a method for the production of edible oil from rapeseed, in which for processing well-formed seeds of large- and/or small-seeded cultivars are selected, with "salad" profile of fatty acids, acquired at the late ripeness phase from an ecological cultivation.
  • Well-formed seeds are determined on the basis of the share - up to 3% - of seeds with weight 10% lower from the mean weight of 1000 seeds. Meeting this condition requires, for coarse-seeded cultivars, sifting through a screen with mesh size dia. 1.8 mm, and for small-seeded cultivars - through a screen with mesh size dia. 1.7 mm.
  • Cultivars with "salad” type of fatty acid composition contain not less than 65% of oleic acid, up to 2% of erucic acid, and up to 3.5% of saturated fatty acids.
  • a cultivation has ecological character when after the period of blooming no application of any chemical agents is permitted - weed control agents, preparations against pests and plant diseases, as well as desiccants and ripening regulators.
  • seeds are selected such that their natural moisture content is lower than 7.5%, while the chlorophyll content measured with absorbance at wavelength of 666 nm does not exceed the value of 25.
  • the share of immature seeds in seed material to be processed, defined on the basis of the amount of seeds with brown colouring, cannot be higher than 1%.
  • Seed purity at the moment of harvest i.e. the amount of usable contaminations that include micro- and macro-damage to seeds, cannot be higher than 3%, and the content of organic contaminants - resides of stems and pods - cannot exceed 5% and there are no germinated seeds nor weed seeds present.
  • the method according to the invention is characterised by the fact that seeds selected as above are stored in silos, under pressure not exceeding 80 kPa, in an inert gas atmosphere, preferably nitrogen, at temperature not exceeding 25° C and for periods not longer than 8 months, and from seed prepared in this way portions are taken, with weight not greater than 500 kgs, and placed in an air-tight hopper filled with an inert gas, preferably nitrogen, at temperature not higher than 40° C and with no light.
  • the obtained oil is subjected to purification and then to microbiological evaluation of quality, and when the total content of fungi in 1 g of the oil does not exceed 5 x 10 4 , that total including not more than 10 3 of fusarium, not more than 10 3 of gliocladium, and aspergillus at no more than 5 x 10 3 , including aspergillus flavus, aspergillus parasiticus, aspergillus nomius (alphatysines), aspergillus alutaceus (ochratoxin A), aspergillus clavatus (patuline) at not more than 10 x 10 2 , the oil is poured into darkened containers with walls opaque to light rays, with an atmosphere of an inert gas, preferably nitrogen, filling the empty space after closing the container, with the containers being of such volume that is adapted to complete one-time use.
  • an inert gas preferably nitrogen
  • the seed is dried until the moment when the moisture gets down to maximum 7.5%, using seed deposit ventilation with a drying agent, preferably air warmed to a temperature not exceeding 35° C.
  • Rapeseed oil produced with the method according to the invention based on raw material with specific properties - ecological production, special methods of harvest, drying and storage, expression without access of light and oxygen, permits the retention of a number of substances in the oil that have a strong pro-health effect.
  • the particular stages of acquisition of rapeseed plants, and especially harvest, delayed to achieve full ripeness, ensure a high content of carotenoid pigments and at the same time a minimum amount of undesirable chlorophylls.
  • rapeseed oil rapeseeds were used obtained from a plantation where the sowing material was seed of cv. Contact with the following fatty acid profile:
  • the seeds were subjected to cleaning to eliminate small seeds. Seeds of coarse-seed cultivars were sifted through a screen with mesh size dia 1.8 mm, and those of small-seeded cultivars through a screen with mesh size dia, 1.7 mm.
  • a silo was used, 12 m high and with a diameter of 3 m, which ensured that pressure exerted by the seed deposit on the silo bottom did not exceed 80 kPa at full charge.
  • the silo Prior to filling with seeds, the silo was filled with nitrogen whose amount was topped up during the whole cycle of rapeseed storage. The duration of the full storage cycle, i.e.
  • the total content of fungi in 1 g of oil was less than the limit values of 5 x 10 4 , that total including fusarium up to 10 3 , gliocladium up to 10 3 , and aspergillus at up to 5 x 10 3 , including aspergillus flavus, aspergillus parasiticus, aspergillus nomius (alphatysines), aspergillus alutaceus (ochratoxin A), aspergillus clavatus (patuline) in amount up to 10 x 10 2 .
  • the obtained oil was poured into containers with dark, opaque to light rays walls, with volume of 150 ml. The filling of the containers was performed in an atmosphere of nitrogen that, after the containers were closed, filled the space above the oil surface.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Pretreatment Of Seeds And Plants (AREA)
  • Edible Oils And Fats (AREA)
EP08827060.8A 2007-08-09 2008-07-30 Method of producing edible oil from rapeseed Active EP2222826B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
PL383110A PL208504B1 (pl) 2007-08-09 2007-08-09 Sposób wytwarzania oleju jadalnego z rzepaku
PCT/PL2008/050010 WO2009020409A2 (en) 2007-08-09 2008-07-30 Method of producing edible oil from rapeseed

Publications (2)

Publication Number Publication Date
EP2222826A2 EP2222826A2 (en) 2010-09-01
EP2222826B1 true EP2222826B1 (en) 2014-06-25

Family

ID=40220221

Family Applications (1)

Application Number Title Priority Date Filing Date
EP08827060.8A Active EP2222826B1 (en) 2007-08-09 2008-07-30 Method of producing edible oil from rapeseed

Country Status (3)

Country Link
EP (1) EP2222826B1 (pl)
PL (1) PL208504B1 (pl)
WO (1) WO2009020409A2 (pl)

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4411499C1 (de) * 1994-04-05 1995-10-26 Allkraft Futtermittel Gmbh Verwendung eines Leinöls als Ergänzungsfuttermittel zur Förderung des Muskulaturaufbaus bei Pferden
PL186045B1 (pl) 1998-06-02 2003-09-30 Inst Chemii Przemyslowej Im Pr Sposób wydzielania oleju z nasion roślin
DE19937081C2 (de) 1999-08-06 2002-05-02 Felix Horst Schneider Verfahren und Einrichtung zur Herstellung von Speiseöl aus Rapssaat
FR2858982B1 (fr) * 2003-08-18 2008-04-11 Claude Boucher Procedes d'obtention d'huiles a partir de presses ou extrudeuses mises sous vide, avec ou sans temperature regulee et utilisation des composants obtenus par fractionnements de ces huiles
EP1827123B1 (en) * 2004-11-04 2015-07-22 Monsanto Technology, LLC High pufa oil compositions

Also Published As

Publication number Publication date
WO2009020409A3 (en) 2009-03-26
EP2222826A2 (en) 2010-09-01
WO2009020409A2 (en) 2009-02-12
PL208504B1 (pl) 2011-05-31
PL383110A1 (pl) 2009-02-16

Similar Documents

Publication Publication Date Title
Minifie Chocolate, cocoa and confectionery: science and technology
Bee et al. The raw bean
Nugroho et al. Physical bean quality of Arabica coffee (Coffea arabica) cultivated at high and medium altitude
EP2222826B1 (en) Method of producing edible oil from rapeseed
AU2012295146B2 (en) Micro-fermentation of cocoa
Santos et al. Physico-chemical characterization and kinetics of drying of organic yellow bell pepper (Capsicum annuum L.)
RU2226059C2 (ru) Способ производства чая из кипрея узколистного
Rodrigues et al. Growth and maturation of pequi fruit of the Brazilian cerrado
Marwati et al. Packaging and storage of cocoa beans fermented with Lactobacillus plantarum HL-15 in Agricultural Technology Park Nglanggeran, Yogyakarta
Gamuchirai et al. Effect of drying techniques and storage conditions on quality and incidence of aflatoxins in dried chillies (Capsicum frutescens) in Zimbabwe
White et al. Factors affecting the deterioration of stored flaxseed including the potential of insect infestation
Paull Postharvest handling of Smooth Cayenne pineapple in Hawaii for the fresh fruit market
Shakerardekani et al. Types of dryers and their effect on the pistachio nuts quality-a Review
Chiou et al. Comparison of fatty acid composition and oxidative stability of peanut oils prepared from spring and fall crops of peanuts
WO2006043117A1 (en) Processing of olive marc into alimentary meal
Fielke et al. The potential for infield hulling of early harvest almonds
Chalfoun et al. Brazilian coffee quality: Cultural, microbiological and bioactivity aspects
Gomaa et al. Post-harvest studies on reducing losses and maintaining quality of packaging Roselle calyxes
CN115530235B (zh) 一种鲜榛仁的贮藏保鲜方法
Jayashree Spice Processing and Value Addition Opportunities for Start-up Entrepreneurs
Venskutonis Harvesting and post-harvest handling in the genus Thymus
Borém et al. Processing and drying of coffee
Minifie et al. History and Development
Robert et al. Effect of reconditioning of discrepant cocoa on the quality of cocoa beans
Kreibich et al. Cocoa (Theobroma cacao L.) bean processing and storage conditions control for safe chocolate products

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 20100319

AK Designated contracting states

Kind code of ref document: A2

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MT NL NO PL PT RO SE SI SK TR

AX Request for extension of the european patent

Extension state: AL BA MK RS

DAX Request for extension of the european patent (deleted)
17Q First examination report despatched

Effective date: 20130510

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

INTG Intention to grant announced

Effective date: 20140122

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MT NL NO PL PT RO SE SI SK TR

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

REG Reference to a national code

Ref country code: CH

Ref legal event code: EP

REG Reference to a national code

Ref country code: AT

Ref legal event code: REF

Ref document number: 674737

Country of ref document: AT

Kind code of ref document: T

Effective date: 20140715

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

REG Reference to a national code

Ref country code: DE

Ref legal event code: R096

Ref document number: 602008033017

Country of ref document: DE

Effective date: 20140807

REG Reference to a national code

Ref country code: SE

Ref legal event code: TRGR

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: CY

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140926

Ref country code: FI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

REG Reference to a national code

Ref country code: NO

Ref legal event code: T2

Effective date: 20140625

REG Reference to a national code

Ref country code: AT

Ref legal event code: MK05

Ref document number: 674737

Country of ref document: AT

Kind code of ref document: T

Effective date: 20140625

REG Reference to a national code

Ref country code: NL

Ref legal event code: VDEP

Effective date: 20140625

REG Reference to a national code

Ref country code: LT

Ref legal event code: MG4D

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LV

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: HR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: CZ

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: SK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: ES

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: RO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: PT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20141027

Ref country code: EE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: PL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: NL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: AT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: IS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20141025

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

REG Reference to a national code

Ref country code: DE

Ref legal event code: R097

Ref document number: 602008033017

Country of ref document: DE

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MC

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

REG Reference to a national code

Ref country code: IE

Ref legal event code: MM4A

REG Reference to a national code

Ref country code: FR

Ref legal event code: ST

Effective date: 20150331

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20140731

Ref country code: IT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: DK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20140731

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20140925

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20140825

26N No opposition filed

Effective date: 20150326

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: BE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20140925

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20140730

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: NO

Payment date: 20150707

Year of fee payment: 8

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: SE

Payment date: 20150707

Year of fee payment: 8

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: BG

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: TR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20140625

Ref country code: HU

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT; INVALID AB INITIO

Effective date: 20080730

Ref country code: LU

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20140730

REG Reference to a national code

Ref country code: NO

Ref legal event code: MMEP

REG Reference to a national code

Ref country code: SE

Ref legal event code: EUG

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20160731

Ref country code: NO

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20160731

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20240102

Year of fee payment: 16