EP1848009B1 - Langkörper und ihre Verwendung - Google Patents

Langkörper und ihre Verwendung Download PDF

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Publication number
EP1848009B1
EP1848009B1 EP06112828.6A EP06112828A EP1848009B1 EP 1848009 B1 EP1848009 B1 EP 1848009B1 EP 06112828 A EP06112828 A EP 06112828A EP 1848009 B1 EP1848009 B1 EP 1848009B1
Authority
EP
European Patent Office
Prior art keywords
member according
bushing
conductor
high voltage
shell
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
EP06112828.6A
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English (en)
French (fr)
Other versions
EP1848009A1 (de
Inventor
Peter SJÖBERG
Gerd Chalikiá
Roger Hedlund
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ABB Technology AG
Original Assignee
ABB Technology AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to EP06112828.6A priority Critical patent/EP1848009B1/de
Application filed by ABB Technology AG filed Critical ABB Technology AG
Priority to CN2007800138611A priority patent/CN101427325B/zh
Priority to KR1020087025230A priority patent/KR101321222B1/ko
Priority to PCT/EP2007/053442 priority patent/WO2007122099A1/en
Priority to CA2649223A priority patent/CA2649223C/en
Priority to BRPI0710518A priority patent/BRPI0710518B8/pt
Priority to RU2008144777/07A priority patent/RU2428760C2/ru
Priority to US12/297,765 priority patent/US7939752B2/en
Priority to JP2009505845A priority patent/JP2009534787A/ja
Publication of EP1848009A1 publication Critical patent/EP1848009A1/de
Application granted granted Critical
Publication of EP1848009B1 publication Critical patent/EP1848009B1/de
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Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B17/00—Insulators or insulating bodies characterised by their form
    • H01B17/32—Single insulators consisting of two or more dissimilar insulating bodies
    • H—ELECTRICITY
    • H02—GENERATION; CONVERSION OR DISTRIBUTION OF ELECTRIC POWER
    • H02G—INSTALLATION OF ELECTRIC CABLES OR LINES, OR OF COMBINED OPTICAL AND ELECTRIC CABLES OR LINES
    • H02G15/00—Cable fittings
    • H02G15/02—Cable terminations
    • H02G15/06—Cable terminating boxes, frames or other structures
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B17/00—Insulators or insulating bodies characterised by their form
    • H01B17/34—Insulators containing liquid, e.g. oil
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B17/00—Insulators or insulating bodies characterised by their form
    • H01B17/36—Insulators having evacuated or gas-filled spaces

Definitions

  • the present invention relates to an elongated member according to the preamble of appended claim 1.
  • the invention is directed to any such member where a high voltage is to be shielded with respect to the environment for preventing flash-overs from occurring to equipment, casings or other objects normally being connected to earth.
  • An example of such a member is a bushing connecting a transformer to a high voltage network, in which it is essential to shield the high voltage of the conductor to be connected to the high voltage network to a location at a considerable distance, such as for example 4 meters, from the transformer.
  • Cable terminations and High voltage apparatuses are other examples of such members.
  • a member of this type has to withstand large temperature changes over time. These temperature changes may be due to the fact that it is totally or at least partially located outdoors, where the temperature depending upon the time of the year may change between -40°C and +40°C. Furthermore, the load of said high voltage conductor may vary, i.e. the current flowing therethrough may vary so much that the temperature of this conductor and by that of the parts of said elongated member inside said shell may vary considerably. In fact, the temperature of the shell will be mainly determined by the temperature of the environment of said member, whereas the temperature of the internal parts thereof, such as of said medium, will also depend on the intensity of the current flowing through the conductor.
  • the medium of a material with certain electrically insulating properties, which has to fill said gap, will tend to change in volume with the temperature, which means that a pressure will be built up inside the shell upon a temperature rise if the medium is totally enclosed in said shell. This pressure may cause the outer insulator shell to be damaged.
  • the first is to construct the member with the outer insulator shell so that it is able to withstand the pressure built up, which is difficult and costly to obtain.
  • the other solution is to construct the member so that the pressure built-up is taken care of, for instance by connecting said gap filled with a fluid to an expansion vessel, which is both complicated and expensive. Furthermore, this involves a risk of leakage of said medium, which may constitute a fire risk.
  • EP-A-0971372 discloses all features of the preamble of appended claim 1 except for the feature that a high voltage conductor extends in the longitudinal direction of the shell of the elongated member.
  • the problems of the filling degree of said medium of a material with certain electrically insulating properties of said gap due to temperature changes are in EP-A-0971372 solved by forming said medium by an electrically insulating material containing hollow spaces in the form of microspheres filled with gas, so that this material is adapted to expand upon a temperature rise thereof by reversibly compressing the hollow spaces and reducing the volume thereof.
  • This object is according to the present invention obtained by providing an elongated member according to appended claim 1, i.e. by arranging microspheres filled with a mixture of liquid and gas in the gap inside the shell, in which the gas content is adapted to increase with the temperature of said material and thereby of the microspheres. Thanks to the increase of gas content with the temperature increase the volume reduction of said microspheres is facilitated with increasing temperatures making it possible to obtain a pressure of said medium inside the shell being less temperature dependent than in such elongated members already known, such as the one disclosed in EP-A-0971372 .
  • said microspheres have a diameter of 10 ⁇ m - 100 ⁇ m when not deformed. It has turned out that these are suitable dimensions of such hollow spaces for ensuring the maintenance of excellent electrically insulating properties of said medium aimed at.
  • microspheres are expanded microspheres.
  • the total volume of said hollow spaces is at room temperature 10-50%, preferably 20-40%, of the total volume of said medium and accordingly of said gap. This means an ability of said material to expand considerably while reducing the volume of said hollow spaces without substantially increasing the pressure upon parts of the member defining said gap.
  • said medium is filled into said gap to have an overpressure therein, i.e. influencing the internal walls of said shell, with a pressure P of 0 ⁇ P ⁇ 2 bar at room temperature.
  • an overpressure at room temperature has turned out to be sufficient for ensuring that the entire gap is totally filled with said medium also at lower temperatures of said member.
  • said conductor is a conductor tube extending through substantially the entire shell.
  • said gap separates the internal walls of the shell from an active core of the member comprising said conductor.
  • said gap has not to fill the entire volume between said conductor and the outer shell, and according to an embodiment of the invention said member is a bushing designed for leading a high voltage conductor through a wall and said active core then comprises electrical field distributing capacitor surrounding said conductor, so that the electrical field will be nearly constant from said conductor and outwards towards the insulator shell.
  • "Wall” is here to be given a wide meaning and may just as well be a wall of a casing, such as a transformer casing, as a wall of a building.
  • said shell is a ceramic sleeve, preferably with outer flanges.
  • This ceramic sleeve may at the ends thereof be secured to metal flanges, for instance of aluminium.
  • the member is designed to have said conductor on a system voltage of at least 12 kV, such as 12 kV-800 kV, especially 50 kV-800 kV. These are conceivable ranges for the voltage of the conductor in a member to which the present invention is directed.
  • said member is designed to have a current of at least 1A, such as 1 A-100 kA, especially 500 A-25 kA, to flow through the conductor thereof.
  • a current of at least 1A such as 1 A-100 kA, especially 500 A-25 kA
  • Such current intensities may typically occur in applications where a member of this type is useful, and changes of these currents may cause considerable temperature changes of said medium in said gap.
  • the member is a bushing to be arranged at a high voltage converter station for leading a high voltage conductor through a wall of a current valve hall and outdoors or from one such hall to another such hall.
  • the member may also be a bushing adapted to be connected to the outer casing of any high voltage apparatus, such as a bushing adapted to be connected to a high voltage disconnector, where there is a need to insulate a conductor with respect to an earthed plane it has to pass.
  • the member may be a transformer bushing or a generator bushing, or it may be a wall bushing.
  • said member is designed to be arranged on the circumference of a bushing for leading a high voltage conductor through a wall for tapping a voltage from this bushing. Temperature changes of the said electrically insulating medium of such a member may also constitute a severe problem with respect to pressure built-up wouldn't said material be able to expand by reducing the volume of said hollow spaces.
  • said member is designed as a cable termination adapted to have a high voltage cable connected to one end thereof.
  • Such cable terminations may be used for connecting an electrical cable, such as a PEX-cable to a power line of a high voltage network, a transformer or a gas-insulated switchgear in which said member may be arranged to stand on the ground at the cable end thereof.
  • the invention also relates to a use of a member according to the invention as a wall bushing, a transformer or a generator bushing or as a cable termination or as a high voltage apparatus.
  • Fig 1 illustrates an elongated member according to an embodiment of the invention in the form of a transformer bushing having an outer sleeve-like rigid ceramic or polymer insulator shell 1 with outer flanges 2, which shell may have a length in the order of 1 dm - 10 m and is secured at the ends to metal flanges 3, 4, which may be of aluminium.
  • the conductor 5 is surrounded by electrical field distributing capacitors in the form of a number of layers 9 of for instance alternatingly paper and metal wound therearound. These number of layers and accordingly the number of capacitors are reduced at the end 7 distant to the connection of the bushing to the transformer casing 8 as well as at the end thereof immerged into an oil bath 25 inside the transformer casing. This means that the electric field will be substantially constant gradually from the conductor 5 and outwards towards the shell 1. Furthermore, the cone-like shape of the capacitor layer 9 results in a smooth electrical field in the axial direction inside the bushing.
  • a gap 10 is formed inside the shell 1 next to the internal wall of the shell, and this gap is filled with a medium 11 of a material with electrically insulating properties.
  • This material contains expanded hollow microspheres, filled with a liquid/gas-mixture mixed into a silicone gel, or another type of gel. After this mixing the silicone gel cross-links, which results in a compressible gel, the function of which will be explained below with reference to fig 2 .
  • the total volume of the hollow spaces of the microspheres is at room temperature 10-50% of the total volume of said medium and accordingly of said gap.
  • the silicone gel with the microspheres contained therein is filled into the gap to have an overpressure therein, i.e. influencing the internal walls 12 of said shell, with a pressure P of 0 ⁇ P ⁇ 2 bar at room temperature.
  • the function of the medium 11 in said gap 10 will be as follows.
  • the temperature of this medium may change as a consequence of changes of the outdoor temperature when said shell is located outdoors and as a consequence of changes of the intensity of a current flowing through the conductor 5. It is shown in fig 2 what happens when the temperature of said medium increases resulting in a change of the condition of said medium from A to B. Accordingly, the gel 13 will expand while compressing the microspheres 14 and by that reducing the volume thereof keeping any pressure built up inside the shell at an acceptable low level. The microspheres are in this way reversibly compressed, which means that they will expand and increase in volume when the temperature of said medium sinks again.
  • Fig 3 illustrates a member 15 according to another embodiment of the invention which is also present in fig 1 , designed to be arranged on the circumference of the bushing for tapping a voltage from this bushing.
  • This is obtained by a wire 16 extending into the layer 9 of capacitors and connecting to a capacitor on a potential differing considerably from earth, which will be the potential of the outermost capacitor layer bearing against the metallic flange 17.
  • this wire 16 has to be electrically insulated with respect to the flange 17, and a gap 10 surrounding this wire 16 is filled with a medium 11 of the type described above.
  • this medium 11 will act according to above when the temperature thereof is changing protecting an insulator body 18 surrounding the wire against damage as a consequence of pressure built up inside the gap 10 filled with said medium.
  • Fig 4 illustrates a member according to a third embodiment of the invention in the form of a cable termination. Parts thereof corresponding to part of the bushing in fig 1 have been provided with the same reference numerals.
  • This cable termination has a cable clamp 20 at one end thereof, to which a high voltage cable 21, such as a PEX-cable, is connected.
  • This clamp 20 is connected to a conductor tube 5, extending inside the ceramic shell 1 to the other end thereof for connection to an overhead line 22 of a high voltage network.
  • the bottom end of the cable termination is preferably secured to a ground plate 23 by an aluminium flange 24.
  • the gap 10 between the conductor 5 and the shell 1 is filled with a medium 11 of the type described above in connection with fig 1 and 2 resulting in the same behaviour and advantages as mentioned above.

Landscapes

  • Insulators (AREA)
  • Installation Of Bus-Bars (AREA)
  • Housings And Mounting Of Transformers (AREA)
  • Gas-Insulated Switchgears (AREA)

Claims (25)

  1. Langkörper mit einer äußeren hüllenartigen starren Isolatorschale (1), die einen Hochspannungsleiter (5, 16) umgibt, welcher in der Längsrichtung der Schale verläuft, und einem Spalt (10) innerhalb der Schale neben der Innenwand der Schale, der den Leiter mindestens teilweise umgibt und mit einem Medium (11) aus einem Material mit elektrisch isolierenden Eigenschaften gefüllt ist, wobei das Medium durch ein elektrisch isolierendes Material (13) ausgebildet ist, das Hohlräume (14) enthält, welche mindestens teilweise mit Gas gefüllt sind, und wobei das Material dazu geeignet ist, sich auf einen Temperaturanstieg durch umkehrbares Zusammendrücken der Hohlräume und Reduzieren ihres Volumens auszudehnen, wobei die Hohlräume durch verformbare Kugeln (14) ausgebildet sind, die dazu geeignet sind, nach Verformung ihre Form wieder anzunehmen, wenn externe Kompressionskräfte von dem Material (13) infolge eines Temperaturabfalls reduziert werden, wobei das Material ein vernetztes Gel (13) mit darin eingebetteten Mikrokugeln (14) ist, dadurch gekennzeichnet, dass die Mikrokugeln (14) mit einer Mischung aus Flüssigkeit und Gas gefüllt sind, in der der Gasinhalt dazu geeignet ist, mit der Temperatur des Materials und damit der Mikrokugeln zuzunehmen.
  2. Körper nach Anspruch 1, dadurch gekennzeichnet, dass die Mikrokugeln (14) einen Durchmesser von 10 µm bis 100 µm aufweisen, wenn sie nicht verformt sind.
  3. Körper nach einem der Ansprüche 1 oder 2, dadurch gekennzeichnet, dass das Gel (13) ein Silikongel ist.
  4. Körper nach einem der Ansprüche 1 bis 3, dadurch gekennzeichnet, dass die Mikrokugeln (14) ausgedehnte Mikrokugeln sind.
  5. Körper nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass das Gesamtvolumen der Hohlräume (14) auf Raumtemperatur 10 bis 50%, vorzugsweise 20 bis 40% des Gesamtvolumens des Mediums (11) und dementsprechend des Spalts (10) beträgt.
  6. Körper nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass das Medium in den Spalt zum Aufweisen eines Überdrucks darin gefüllt ist, d.h. die Innenwände der Schale beeinflusst, mit einem Druck P von 0<P<2 Bar auf Raumtemperatur.
  7. Körper nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass der Leiter ein Leiterrohr (5) ist, der im Wesentlichen durch die gesamte Schale (1) verläuft.
  8. Körper nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass der Spalt (10) die Innenwände der Schale (1) von einem aktiven Kern des Körpers trennt, der den Leiter (5) umfasst.
  9. Körper nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass die Schale (1) eine Keramik- oder Polymerhülle, vorzugsweise mit Außenflanschen (2), ist.
  10. Körper nach Anspruch 9, dadurch gekennzeichnet, dass die Keramik- oder Polymerhülle (1) an ihren Enden an Metallflanschen (3, 4) befestigt ist.
  11. Körper nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass er derart gestaltet ist, dass an den Leiter eine Systemspannung von mindestens 12 kV, wie etwa 12 kV bis 800 kV, insbesondere 50 kV bis 800 kV anliegt.
  12. Körper nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass er derart gestaltet ist, dass ein Strom von mindestens 1 A, wie etwa 1 A bis 100 kA, insbesondere 500 A bis 25 kA, durch den Leiter davon fließt.
  13. Körper nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass er eine Buchse ist, die zum Führen eines Hochspannungsleiters durch eine Wand gestaltet ist.
  14. Körper nach einem der Ansprüche 8 und 13, dadurch gekennzeichnet, dass der aktive Kern elektrische Feldverteilungskondensatoren (9) aufweist, die den Leiter (5) umgeben.
  15. Körper nach Anspruch 13, dadurch gekennzeichnet, dass er eine Buchse ist, die an einer Hochspannungsumrichterstation zum Führen eines Hochspannungsleiters durch eine Wand einer Stromventilhalle und ins Freie oder von einer derartigen Halle zu einer anderen derartigen Halle angeordnet ist.
  16. Körper nach Anspruch 13, dadurch gekennzeichnet, dass er eine Buchse ist, die dazu geeignet ist, mit dem Außengehäuse von jeglicher Hochspannungsvorrichtung verbunden zu sein.
  17. Körper nach Anspruch 16, dadurch gekennzeichnet, dass er eine Buchse ist, die dazu geeignet ist, mit einem Hochspannungstrenner verbunden zu sein.
  18. Körper nach Anspruch 13, dadurch gekennzeichnet, dass er eine Transformatorbuchse oder eine Generatorbuchse ist.
  19. Körper nach Anspruch 13, dadurch gekennzeichnet, dass er eine Wandbuchse ist.
  20. Körper nach einem der vorhergehenden Ansprüche, dadurch gekennzeichnet, dass er dazu gestaltet ist, am Umfang einer Buchse zum Führen eines Hochspannungsleiters durch eine Wand zum Anzapfen einer Spannung aus dieser Buchse angeordnet zu sein.
  21. Körper nach einem der Ansprüche 1 bis 11, dadurch gekennzeichnet, dass er als Kabelende gestaltet ist, das dazu geeignet ist, ein Hochspannungskabel an einem Ende davon verbunden aufzuweisen.
  22. Verwendung eines Körpers nach einem der Ansprüche 1 bis 11 als Wandbuchse.
  23. Verwendung eines Körpers nach einem der Ansprüche 1 bis 11 als Transformator- oder Generatorbuchse.
  24. Verwendung eines Körpers nach einem der Ansprüche 1 bis 11 als Kabelende.
  25. Verwendung eines Körpers nach einem der Ansprüche 1 bis 11 als Hochspannungsvorrichtung.
EP06112828.6A 2006-04-20 2006-04-20 Langkörper und ihre Verwendung Active EP1848009B1 (de)

Priority Applications (9)

Application Number Priority Date Filing Date Title
EP06112828.6A EP1848009B1 (de) 2006-04-20 2006-04-20 Langkörper und ihre Verwendung
KR1020087025230A KR101321222B1 (ko) 2006-04-20 2007-04-10 기다란 부재 및 그의 용도
PCT/EP2007/053442 WO2007122099A1 (en) 2006-04-20 2007-04-10 An elongated member and use thereof
CA2649223A CA2649223C (en) 2006-04-20 2007-04-10 An elongated member and use thereof
CN2007800138611A CN101427325B (zh) 2006-04-20 2007-04-10 伸长部件及其用途
BRPI0710518A BRPI0710518B8 (pt) 2006-04-20 2007-04-10 “elemento alongado possuindo um envoltório isolante rígido tipo manga externa cercando um condutor de alta voltagem”
RU2008144777/07A RU2428760C2 (ru) 2006-04-20 2007-04-10 Удлиненный элемент и его применение
US12/297,765 US7939752B2 (en) 2006-04-20 2007-04-10 Elongated member and use thereof
JP2009505845A JP2009534787A (ja) 2006-04-20 2007-04-10 細長部材及びその使用

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP06112828.6A EP1848009B1 (de) 2006-04-20 2006-04-20 Langkörper und ihre Verwendung

Publications (2)

Publication Number Publication Date
EP1848009A1 EP1848009A1 (de) 2007-10-24
EP1848009B1 true EP1848009B1 (de) 2014-03-26

Family

ID=36950193

Family Applications (1)

Application Number Title Priority Date Filing Date
EP06112828.6A Active EP1848009B1 (de) 2006-04-20 2006-04-20 Langkörper und ihre Verwendung

Country Status (9)

Country Link
US (1) US7939752B2 (de)
EP (1) EP1848009B1 (de)
JP (1) JP2009534787A (de)
KR (1) KR101321222B1 (de)
CN (1) CN101427325B (de)
BR (1) BRPI0710518B8 (de)
CA (1) CA2649223C (de)
RU (1) RU2428760C2 (de)
WO (1) WO2007122099A1 (de)

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EP2039496A1 (de) * 2007-09-20 2009-03-25 ABB Research Ltd. Verfahren zur Herstellung eines Gummiprodukts
CH698970A1 (de) * 2008-06-04 2009-12-15 Trench Switzerland Ag Hochspannungs-Messwandler mit flexibler Isolierung.
CN102498529B (zh) 2009-04-14 2014-08-20 阿尔斯通电网简易股份有限公司 折叠式高压绝缘柱
DE102010015729B4 (de) * 2010-04-21 2015-01-22 Maschinenfabrik Reinhausen Gmbh Hochspannungsisolator
US8963015B2 (en) * 2011-01-18 2015-02-24 Fisher Controls International Llc Capacitor coupled cable shield feedthrough
JP5740687B2 (ja) * 2011-01-18 2015-06-24 株式会社ダイヘン 地上設置型変圧器装置
US9078346B2 (en) * 2013-03-11 2015-07-07 Varian Semiconductor Equipment Associates, Inc. Insulator protection
EP2924698B1 (de) * 2014-03-27 2018-11-21 ABB Schweiz AG Öl-Öl-Durchführung und Öltransformator
CN108257741B (zh) * 2018-03-27 2021-04-23 江苏神马电力股份有限公司 一种支柱绝缘子及绝缘支柱
DE102019125962A1 (de) 2019-09-26 2021-04-01 Maschinenfabrik Reinhausen Gmbh Trockener, syntaktischer Schaum als elektrisch isolierendes Material
CN111734950A (zh) * 2020-07-01 2020-10-02 西安维国电子科技有限公司 密闭空间电绝缘气体填充与回收的方法及填充装置
FR3140201A1 (fr) * 2022-09-22 2024-03-29 Arkema France Appareil électrique comprenant au moins un matériau gélifié

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JPS61161830U (de) * 1985-03-27 1986-10-07
US5466890A (en) * 1994-03-22 1995-11-14 Cooper Industries, Inc. Expansion joint for an electrical conduit which is electrically grounded through the expansion joint
US5466891A (en) * 1994-04-08 1995-11-14 Abb Power T&D Company Inc. Conical composite SF6 high voltage bushing with floating shield
JPH0963381A (ja) * 1995-08-25 1997-03-07 Ngk Insulators Ltd 懸垂がいし
US6140573A (en) * 1998-05-29 2000-10-31 Siemens Aktiengesellschaft Hollow core composite bushings
EP0971372A1 (de) 1998-07-10 2000-01-12 ABB Research Ltd. Elektrische Vorrichtung mit isolierendem Siliconenfüllung
CN2453521Y (zh) * 2000-12-07 2001-10-10 南京供电局 配电变压器上使用的带有电流互感器的套管绝缘子
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Also Published As

Publication number Publication date
KR20080110821A (ko) 2008-12-19
EP1848009A1 (de) 2007-10-24
CN101427325A (zh) 2009-05-06
BRPI0710518B8 (pt) 2022-12-13
CA2649223C (en) 2014-12-09
BRPI0710518A2 (pt) 2011-08-16
US20090173515A1 (en) 2009-07-09
US7939752B2 (en) 2011-05-10
CA2649223A1 (en) 2007-11-01
KR101321222B1 (ko) 2013-10-23
CN101427325B (zh) 2012-08-22
WO2007122099A1 (en) 2007-11-01
RU2428760C2 (ru) 2011-09-10
JP2009534787A (ja) 2009-09-24
RU2008144777A (ru) 2010-05-27
BRPI0710518B1 (pt) 2018-03-06

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