EP1605198A3 - Procédé de production de dioxyde de carbone liquide et application à la production de dioxyde de carbone supercritique - Google Patents

Procédé de production de dioxyde de carbone liquide et application à la production de dioxyde de carbone supercritique Download PDF

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Publication number
EP1605198A3
EP1605198A3 EP05300449A EP05300449A EP1605198A3 EP 1605198 A3 EP1605198 A3 EP 1605198A3 EP 05300449 A EP05300449 A EP 05300449A EP 05300449 A EP05300449 A EP 05300449A EP 1605198 A3 EP1605198 A3 EP 1605198A3
Authority
EP
European Patent Office
Prior art keywords
carbon dioxide
application
production
pressure
container
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP05300449A
Other languages
German (de)
English (en)
Other versions
EP1605198A2 (fr
Inventor
Vincent Boisdon
Harald Winter
Christophe Magneney
Olivier Deretz
Dominique Bras
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Publication of EP1605198A2 publication Critical patent/EP1605198A2/fr
Publication of EP1605198A3 publication Critical patent/EP1605198A3/fr
Withdrawn legal-status Critical Current

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C7/00—Methods or apparatus for discharging liquefied, solidified, or compressed gases from pressure vessels, not covered by another subclass
    • F17C7/02—Discharging liquefied gases
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C13/00—Details of vessels or of the filling or discharging of vessels
    • F17C13/02—Special adaptations of indicating, measuring, or monitoring equipment
    • F17C13/025—Special adaptations of indicating, measuring, or monitoring equipment having the pressure as the parameter
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C9/00—Methods or apparatus for discharging liquefied or solidified gases from vessels not under pressure
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2221/00—Handled fluid, in particular type of fluid
    • F17C2221/01—Pure fluids
    • F17C2221/013—Carbone dioxide
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/01—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the phase
    • F17C2223/0146—Two-phase
    • F17C2223/0153—Liquefied gas, e.g. LPG, GPL
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/03—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the pressure level
    • F17C2223/036—Very high pressure (>80 bar)
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2225/00—Handled fluid after transfer, i.e. state of fluid after transfer from the vessel
    • F17C2225/01—Handled fluid after transfer, i.e. state of fluid after transfer from the vessel characterised by the phase
    • F17C2225/0107—Single phase
    • F17C2225/0115—Single phase dense or supercritical, i.e. at high pressure and high density
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2225/00—Handled fluid after transfer, i.e. state of fluid after transfer from the vessel
    • F17C2225/04—Handled fluid after transfer, i.e. state of fluid after transfer from the vessel characterised by other properties of handled fluid after transfer
    • F17C2225/042—Localisation of the filling point
    • F17C2225/046—Localisation of the filling point in the liquid
    • F17C2225/047—Localisation of the filling point in the liquid with a dip tube
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2227/00—Transfer of fluids, i.e. method or means for transferring the fluid; Heat exchange with the fluid
    • F17C2227/03—Heat exchange with the fluid
    • F17C2227/0337—Heat exchange with the fluid by cooling
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2250/00—Accessories; Control means; Indicating, measuring or monitoring of parameters
    • F17C2250/06—Controlling or regulating of parameters as output values
    • F17C2250/0605—Parameters
    • F17C2250/0626—Pressure
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2250/00—Accessories; Control means; Indicating, measuring or monitoring of parameters
    • F17C2250/06—Controlling or regulating of parameters as output values
    • F17C2250/0605—Parameters
    • F17C2250/0631—Temperature

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

Procédé de production de dioxyde de carbone liquide franc, sous pression stabilisée, en un point d'application (21) à une extrémité d'une ligne (20) d'alimentation.
Selon l'invention, ledit procédé comprend les étapes consistant à :
- fournir un conteneur (10) de dioxyde de carbone liquide à la pression désirée au point (21) d'application,
- contrôler et stabiliser ladite pression en contrôlant la température du dioxyde de carbone au sein du conteneur (10),
- prélever le dioxyde de carbone dans la phase liquide du conteneur (10) et l'introduire dans la ligne (20) d'alimentation,
- refroidir sur la ligne (20) d'alimentation le dioxyde de carbone sous pression stabilisée jusqu'à une température telle qu'au point (21) d'application la température du dioxyde de carbone est inférieure à la température d'ébullition du dioxyde de carbone à ladite pression stabilisée.
Application à la chromatographie préparative par extraction supercritique de principes actifs en chimie fine et en pharmacie.
EP05300449A 2004-06-11 2005-06-03 Procédé de production de dioxyde de carbone liquide et application à la production de dioxyde de carbone supercritique Withdrawn EP1605198A3 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0406335 2004-06-11
FR0406335A FR2871549B1 (fr) 2004-06-11 2004-06-11 Procede de production de gaz carbonique liquide et application a la production de gaz carbonique supercritique

Publications (2)

Publication Number Publication Date
EP1605198A2 EP1605198A2 (fr) 2005-12-14
EP1605198A3 true EP1605198A3 (fr) 2008-01-23

Family

ID=34942640

Family Applications (1)

Application Number Title Priority Date Filing Date
EP05300449A Withdrawn EP1605198A3 (fr) 2004-06-11 2005-06-03 Procédé de production de dioxyde de carbone liquide et application à la production de dioxyde de carbone supercritique

Country Status (2)

Country Link
EP (1) EP1605198A3 (fr)
FR (1) FR2871549B1 (fr)

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE495795C (de) * 1928-05-05 1930-04-12 Pierre Polard Verfahren zum Foerdern fluessiger Gase durch einen Pumpvorgang
US3282305A (en) * 1964-02-20 1966-11-01 Gen Dynamics Corp Cylinder filling apparatus
US4554791A (en) * 1983-01-07 1985-11-26 Danfoss A/S Apparatus for conveying liquids
US4751822A (en) * 1986-02-07 1988-06-21 Carboxyque Francaise Process and plant for supplying carbon dioxide under high pressure
EP0501806A1 (fr) * 1991-03-01 1992-09-02 Suprex Corporation Pompe pour dioxyde de carbone liquéfié
US5761911A (en) * 1996-11-25 1998-06-09 American Air Liquide Inc. System and method for controlled delivery of liquified gases
US5850876A (en) * 1990-01-08 1998-12-22 Pyrozone Pty. Ltd. Apparatus and system for the storage and supply of liquid CO2 at low pressure for extinguishing of fires
FR2781037A1 (fr) * 1998-07-10 2000-01-14 Messer France Installation de regulation fonctionnelle d'une unite de stockage-distribution de dioxyde de carbone
WO2003067144A2 (fr) * 2002-02-07 2003-08-14 L'air Liquide, Societe Anonyme A Directoire Et Conseil De Surveillance Pour L'etude Et L'exploitation Des Procedes Georges Claude Procede d'alimentation ininterrompue de dioxyde de carbone en surfusion fluide a pression constante superieure a 40 bars et systeme de mise en oeuvre de ce procede

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE495795C (de) * 1928-05-05 1930-04-12 Pierre Polard Verfahren zum Foerdern fluessiger Gase durch einen Pumpvorgang
US3282305A (en) * 1964-02-20 1966-11-01 Gen Dynamics Corp Cylinder filling apparatus
US4554791A (en) * 1983-01-07 1985-11-26 Danfoss A/S Apparatus for conveying liquids
US4751822A (en) * 1986-02-07 1988-06-21 Carboxyque Francaise Process and plant for supplying carbon dioxide under high pressure
US5850876A (en) * 1990-01-08 1998-12-22 Pyrozone Pty. Ltd. Apparatus and system for the storage and supply of liquid CO2 at low pressure for extinguishing of fires
EP0501806A1 (fr) * 1991-03-01 1992-09-02 Suprex Corporation Pompe pour dioxyde de carbone liquéfié
US5761911A (en) * 1996-11-25 1998-06-09 American Air Liquide Inc. System and method for controlled delivery of liquified gases
FR2781037A1 (fr) * 1998-07-10 2000-01-14 Messer France Installation de regulation fonctionnelle d'une unite de stockage-distribution de dioxyde de carbone
WO2003067144A2 (fr) * 2002-02-07 2003-08-14 L'air Liquide, Societe Anonyme A Directoire Et Conseil De Surveillance Pour L'etude Et L'exploitation Des Procedes Georges Claude Procede d'alimentation ininterrompue de dioxyde de carbone en surfusion fluide a pression constante superieure a 40 bars et systeme de mise en oeuvre de ce procede

Also Published As

Publication number Publication date
FR2871549B1 (fr) 2006-08-04
FR2871549A1 (fr) 2005-12-16
EP1605198A2 (fr) 2005-12-14

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