EP1347682A1 - Termite bait composition and method - Google Patents
Termite bait composition and methodInfo
- Publication number
- EP1347682A1 EP1347682A1 EP01990083A EP01990083A EP1347682A1 EP 1347682 A1 EP1347682 A1 EP 1347682A1 EP 01990083 A EP01990083 A EP 01990083A EP 01990083 A EP01990083 A EP 01990083A EP 1347682 A1 EP1347682 A1 EP 1347682A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- termite
- set forth
- bait composition
- group
- attractant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/002—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing a foodstuff as carrier or diluent, i.e. baits
- A01N25/006—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing a foodstuff as carrier or diluent, i.e. baits insecticidal
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/34—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the groups, e.g. biuret; Thio analogues thereof; Urea-aldehyde condensation products
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N51/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds having the sequences of atoms O—N—S, X—O—S, N—N—S, O—N—N or O-halogen, regardless of the number of bonds each atom has and with no atom of these sequences forming part of a heterocyclic ring
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S424/00—Drug, bio-affecting and body treating compositions
- Y10S424/11—Termite treating
Definitions
- This invention relates to termite bait compositions and methods for controlling termites and, more particularly, to such compositions and methods which employ a powdered cellulosic attractant having a particle size in the range of approximately 1 to 100 micrometers.
- a termite bait composition and method for controlling termites in which a powdered cellulosic dust having a particle size in the range of 1 to 100 micrometers is employed as an attractant; the provision of such a termite bait composition and method in which the use of such a cellulosic attractant promotes increased ingestion and consequent exposure of termites to termite controlling or killing agents; the provision of such a termite bait composition and method in which such a cellulosic attractant permits better adherence of the composition to termites thereby increasing the prospects for introduction of the termite controlling or killing agent back to the termite colony by contact and grooming; and the provision of such a termite bait composition and method which may be readily and economically practiced for improved control of termites.
- Other objects will be in part apparent and in part pointed out hereinafter.
- the present invention is directed to a termite bait composition
- a termite bait composition comprising a powdered cellulosic attractant having a particle size in the range of approximately 1 to 100 micrometers and a termite killing agent carried by or within the attractant.
- the invention is also directed to a method for controlling termites which comprises applying to a termite infested area the above-noted termite bait composition.
- the invention is further directed to a termite bait composition package for use in a termite bait station comprising the above-noted termite bait composition contained within a closed cellulosic package.
- an improved termite bait composition is provided by utilizing as an attractant a powdered cellulosic material having a particle size in the range of approximately 1 to 100 micrometers with a termite killing or controlling agent being carried by or within the attractant.
- a powdered cellulosic material having a particle size in the range of approximately 1 to 100 micrometers with a termite killing or controlling agent being carried by or within the attractant.
- powdered cellulosic material of this small particle size as an attractant, it has been found that the resulting termite bait composition leads to increased ingestion since the termites may more easily ingest material of this small particle size.
- the fine particle size of the termite bait composition of the invention also improves physical exposure by better adhering to termite bodies through static electrical charge.
- the fine powdered bait composition containing the termiticide or killing agent more readily adheres to the termites and is carried back to the nest where it becomes distributed throughout the colony by contact and grooming.
- the bait composition and method of the present invention thereby lead to improved control of termite colonies through the increased ingestion by termites and better adherence to termites of the bait composition by reason of the employment of powdered cellulosic material of small particle size as an attractant.
- any cellulosic material having a particle size within the range of approximately 1 to 100 micrometers may be employed.
- the dust or powdered attractant of this particle size may be cellulose, microcrystalline cellulose, paper or mixtures thereof.
- the preferred cellulosic material for use as the attractant in the present invention is microcrystalline cellulose such as that marketed under the trade designation "Lattice NT-020 Microcrystalline cellulose" having an average particle size of 20 micrometers (FMC Corporation). It will be understood that other cellulosic materials having a particle size within the range of approximately 1 to 100 micrometers, preferably 20 to 100 micrometers and more preferably 20 to 50 micrometers, may also be used in the practice of the invention.
- any known termite killing or controlling agent or termiticide can also be used in the practice of the invention.
- chitin synthesis inhibitors such as hexaflumuron, flufenoxuron, lufenuron and dimilin
- juvenile hormone mimics such as methoprene and pyriproxyfen
- stomach toxicants such as sulfuramide, abamectin, cryolite, boric acid and alkali and alkaline earth salts of boric acid
- contact insecticides such as thiamethoxam, imidicloprid and fipronil, or mixtures or combinations of these agents.
- the particle size of the termite killing agent employed may vary over a wide range, but is preferably of the same order as the particle size of the cellulosic attractant discussed above.
- the use of dimilin as the termite killing agent is preferred and the highly preferred particle size range for dimilin is approximately 2 to 5 micrometers.
- the termite killing or controlling agent may be present in the bait composition in various concentrations such as 0.1 to 1% by weight.
- the termite killing agent or termiticide utilized is generally incorporated into the particular cellulosic attractant employed by absorption, blending or other conventional formulating means. As thus prepared, the termite killing agent is carried by or within the cellulosic attractant.
- the termite bait composition may be compressed into tablets or granular form for placement in a termite bait station.
- the termite bait composition of the invention prepared as described above is packaged in a termite attractive package such as a paper bag, cardboard tube or other cellulosic container which may then be dropped into or placed in a termite bait station without being opened.
- termites eat through the cellulosic package material and thereby gain access to the bait composition contained therein.
- the use of the package for the bait composition enables the powdered bait composition to be maintained in a fresh condition until it is used and also renders handling of the packaged bait composition safer since the user is not required to come into direct contact with the killing agent or toxicant in the packaged bait composition.
- the microcrystalline cellulose used had an average particle size of 20 micrometers and the Solka Flock used had an average particle size in the range of 20 to 100 micrometers.
- the tests were conducted using a choice test arena arrangement in which eight feeding chambers surround a central termite chamber in a wheel configuration with tubes extending from the central chamber to each of the feeding chambers or bait stations. One feeding chamber was left empty for these 7-way tests. There were three combinations of the 11 termite bait attractants presented simultaneously to a group of termites (Reticulitermes flavipes (Kollar)). Each combination included pine wood as one choice (the control or standard food) and only one bait (054) was presented in each of the three combinations. There were four replicates of each combination of bait attractants. The following table summarizes the results of the tests in terms of termite feeding rates (mg of bait removed/g of termite/day).
- the following table shows the average of the mean feeding rates (mg of bait/g of termite/day) for the above-noted tests.
- microcrystalline cellulose (formulation 025) is an effective termite bait attractant.
- Example 2 is an effective termite bait attractant.
- the termite bait active ingredients or killing agents diflubenzuron, emamectin benzoate and thiamethoxam were tested for their efficacy.
- the termite species tested was Reticulitermes virginicus.
- the methodology employed was the standard "choice box" test used in Example 1 in which termites were released into a central chamber with untreated wood.
- the central chamber was connected, using Tygon tubing (2 mm 1 D), with peripheral feeding chambers containing a termite bait composition of the invention (microcrystalline cellulose powder having an average particle size of 20 micrometers and a termite killing agent) or untreated pine wood.
- a termite bait composition of the invention microcrystalline cellulose powder having an average particle size of 20 micrometers and a termite killing agent
- untreated pine wood Each replicate was given the choice of one gram of the treated cellulose powder or three blocks (1 cm) of untreated pine wood.
- the number of live termites was counted.
- the bait compositions containing thiamethoxam and emamectin benzoate killed termites by contact whereas dimilin killed termites by ingestion.
- the results show that dimilin gave almost complete control after 37 days exposure and thiamethoxam and emamectin benzoate both killed 100% of the termites after 25 days. Relatively little cellulose powder was consumed but more treated powder was removed than was untreated wood.
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- General Health & Medical Sciences (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Environmental Sciences (AREA)
- Food Science & Technology (AREA)
- Toxicology (AREA)
- Insects & Arthropods (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Catching Or Destruction (AREA)
Abstract
Description
Claims
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US754722 | 2001-01-04 | ||
US09/754,722 US6416752B1 (en) | 2001-01-04 | 2001-01-04 | Termite bait composition and method |
PCT/US2001/047636 WO2002052940A1 (en) | 2001-01-04 | 2001-12-11 | Termite bait composition and method |
Publications (3)
Publication Number | Publication Date |
---|---|
EP1347682A1 true EP1347682A1 (en) | 2003-10-01 |
EP1347682A4 EP1347682A4 (en) | 2004-07-14 |
EP1347682B1 EP1347682B1 (en) | 2007-10-10 |
Family
ID=25036027
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP01990083A Expired - Lifetime EP1347682B1 (en) | 2001-01-04 | 2001-12-11 | Termite bait composition and method |
Country Status (10)
Country | Link |
---|---|
US (1) | US6416752B1 (en) |
EP (1) | EP1347682B1 (en) |
JP (1) | JP4317364B2 (en) |
AT (1) | ATE375083T1 (en) |
AU (1) | AU2002228956B2 (en) |
DE (1) | DE60130921T2 (en) |
ES (1) | ES2295231T3 (en) |
MX (1) | MXPA03006005A (en) |
PT (1) | PT1347682E (en) |
WO (1) | WO2002052940A1 (en) |
Families Citing this family (32)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6978572B1 (en) | 1998-11-06 | 2005-12-27 | Colorado State University Research Foundation | Method and device for attracting insects |
US6660290B1 (en) | 2000-10-04 | 2003-12-09 | Myco Pesticides Llc | Mycopesticides |
US20040031190A1 (en) * | 2001-10-12 | 2004-02-19 | Collins James Robert | System and methods for monitoring arthropods |
AU2008202148B2 (en) * | 2002-01-29 | 2010-12-23 | Basf Corporation | Optimum density termite bait composition |
US20030152605A1 (en) * | 2002-01-29 | 2003-08-14 | Whitmire Micro-Gen Research Laboratories, Inc. | Optimum density termite bait composition |
US20030167678A1 (en) * | 2002-02-14 | 2003-09-11 | Hunt Seth C. | System to monitor and control subterranean termites by use of a soil additive and method thereof |
EP1462001B1 (en) | 2003-03-25 | 2008-11-12 | Whitmire Micro-Gen Research Laboratories, Inc. | Pest control device |
US7086196B2 (en) * | 2003-03-25 | 2006-08-08 | Whitmire Micro-Gen Research Laboratories, Inc. | Pest control device and method |
DE10333371A1 (en) * | 2003-07-23 | 2005-02-10 | Bayer Ag | Fungicidal drug combinations |
JP4603806B2 (en) * | 2004-03-10 | 2010-12-22 | シンジェンタ ジャパン株式会社 | Ant-injecting trunk injection agent and treatment method thereof |
CN1937916A (en) * | 2004-03-29 | 2007-03-28 | 美国陶氏益农公司 | Pesticide compositions |
EP1811843A4 (en) * | 2004-11-16 | 2008-01-23 | Fmc Corp | Method for control of termite populations |
US20060207164A1 (en) * | 2005-03-21 | 2006-09-21 | David Pearson | Termite monitoring and bait station |
EP1849364A1 (en) * | 2006-04-26 | 2007-10-31 | Basf Aktiengesellschaft | Composition comprising a glucan or a glucan derivative and a pesticide and methods for improving plant health |
CN103461303B (en) | 2006-12-21 | 2018-05-08 | 美国陶氏益农公司 | Include the composite material of thermoplastic polymer, pest food material and insecticide |
US8387306B2 (en) * | 2007-06-28 | 2013-03-05 | Basf Corporation | Method of monitoring and controlling termites with heat-treated wood |
US8407933B2 (en) | 2007-06-28 | 2013-04-02 | Basf Corporation | Above-ground termite station |
CN102480934B (en) * | 2007-06-28 | 2014-04-16 | 巴斯夫公司 | Method of monitoring and controlling termites with heat-treated wood |
MX2010002946A (en) * | 2007-09-18 | 2010-03-31 | Basf Se | Dust composition for combating insects. |
US20090094884A1 (en) * | 2007-10-12 | 2009-04-16 | Whitmire Micro-Gen Research Laboratories, Inc. | Termite station with replaceable cartridge |
US7968525B1 (en) * | 2007-12-03 | 2011-06-28 | University Of Florida Research Foundation, Inc. | Use of RNA interference to validate new termiticide target sites and a method of termite control |
US7987630B2 (en) * | 2008-05-23 | 2011-08-02 | Basf Corporation | Pest control system and method |
TWI478665B (en) | 2008-08-19 | 2015-04-01 | Dow Agrosciences Llc | Bait materials, pest monitoring devices and other pest control devices that include polyurethane foam |
AR076484A1 (en) * | 2009-04-28 | 2011-06-15 | Basf Corp | COMPOSITIONS AND APPLICATORS OF PESTICIDES |
CN102458126B (en) | 2009-04-28 | 2014-07-02 | 巴斯夫公司 | Foamable pesticide compositions |
EA201200375A1 (en) | 2009-08-28 | 2012-09-28 | Басф Корпорейшн | RECESSABLE PESTICIDAL COMPOSITIONS AND APPLICATION METHODS |
EP2491786A4 (en) * | 2009-10-21 | 2013-05-22 | Nippon Soda Co | Tick control bait |
JP2013537040A (en) * | 2010-09-08 | 2013-09-30 | ダウ アグロサイエンシィズ エルエルシー | Pest control systems and methods |
WO2014163978A1 (en) | 2013-03-11 | 2014-10-09 | Dow Agrosciences Llc | Systems and methods for controlling pest infestation of a woody plant |
CA3000425C (en) | 2015-10-05 | 2023-10-10 | Dow Agrosciences Llc | Methods and compositions for pest bait |
CN106070277A (en) * | 2016-05-31 | 2016-11-09 | 刘园 | A kind of compositions preventing and treating Oeobia undalis and preparation method thereof |
ES2684434B1 (en) * | 2017-03-30 | 2019-07-10 | PEREDA Mª PILAR BERGADO | COMPOSITION FOR DETECTION AND / OR MONITORING OF TERMITES |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1597293A (en) * | 1978-03-11 | 1981-09-03 | Atomic Energy Of Australia | Insect control |
US4582901A (en) * | 1984-08-09 | 1986-04-15 | The Research Foundation Of State University Of New York | Fluorinated cellulose esters and the use thereof as termiticidal compositions |
EP0587117A1 (en) * | 1992-09-08 | 1994-03-16 | Barbara L. Thorne | Method and compositions to monitor and control termites |
WO2000062610A1 (en) * | 1999-04-20 | 2000-10-26 | The United States Of America, As Represented By The Secretary Of Agriculture | Termite bait matrix |
US6139858A (en) * | 1999-12-01 | 2000-10-31 | Sumitomo Chemical Company Limited | Termite-controlling agent |
Family Cites Families (17)
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GB1561901A (en) * | 1975-08-06 | 1980-03-05 | Atomic Energy Of Australia | Control of insects |
US4363798A (en) | 1981-07-09 | 1982-12-14 | S. C. Johnson & Son, Inc. | Termite bait composition |
JP2588923B2 (en) * | 1988-03-01 | 1997-03-12 | 住友化学工業株式会社 | Poison bait for pest control |
DE3931303A1 (en) | 1989-09-20 | 1991-03-28 | Desowag Materialschutz Gmbh | PROCESS FOR PREVENTIVE MATERIAL PROTECTION AGAINST TEMPORARY AND / OR TEMPORARY GROUND LIFE, IN PARTICULAR TERMITES |
CA2090256A1 (en) | 1993-02-24 | 1994-08-25 | Timothy George Myles | Method for controlling termites |
US5359806A (en) | 1993-05-24 | 1994-11-01 | Albany International Corp. | Rechargeable termite barrier for buildings |
US5820855A (en) | 1994-06-17 | 1998-10-13 | Ecolab Inc. | Water powder as a synergist in pest baits |
IL139728A (en) * | 1995-01-09 | 2003-06-24 | Penwest Pharmaceuticals Compan | Aqueous slurry composition containing microcrystalline cellulose for preparing a pharmaceutical excipient |
CA2216999A1 (en) | 1995-04-11 | 1996-10-17 | Fmc Corporation | Termite bait station |
US6003266A (en) | 1995-06-07 | 1999-12-21 | American Cyanamid Company | Termiticide bait tube for in ground application |
AUPN515195A0 (en) | 1995-09-01 | 1995-09-21 | Hitchen, John Charles | Method and means for preventing or minimising termite attack |
US5678362A (en) | 1996-04-22 | 1997-10-21 | Owens-Corning Fiberglas Technology, Inc. | Termite control device and method |
AU9693598A (en) | 1997-10-14 | 1999-05-03 | Biostim, Llc | Formulations and methods for insect control |
US6088950A (en) | 1998-03-30 | 2000-07-18 | Jones; Ronald L. | Structural pest control system |
JP2000007516A (en) * | 1998-06-03 | 2000-01-11 | American Cyanamid Co | Termite-bait composition free from ureide |
US5960584A (en) | 1998-07-22 | 1999-10-05 | Aesch, Jr.; Harold W. | Physical termite barrier and termiticide delivery system and method |
US6079150A (en) | 1998-11-09 | 2000-06-27 | Fmc Corporation | Systems and methods for controlling insects under solid substrates |
-
2001
- 2001-01-04 US US09/754,722 patent/US6416752B1/en not_active Expired - Lifetime
- 2001-12-11 AU AU2002228956A patent/AU2002228956B2/en not_active Expired
- 2001-12-11 PT PT01990083T patent/PT1347682E/en unknown
- 2001-12-11 WO PCT/US2001/047636 patent/WO2002052940A1/en active IP Right Grant
- 2001-12-11 DE DE60130921T patent/DE60130921T2/en not_active Expired - Lifetime
- 2001-12-11 MX MXPA03006005A patent/MXPA03006005A/en active IP Right Grant
- 2001-12-11 EP EP01990083A patent/EP1347682B1/en not_active Expired - Lifetime
- 2001-12-11 JP JP2002553905A patent/JP4317364B2/en not_active Expired - Lifetime
- 2001-12-11 ES ES01990083T patent/ES2295231T3/en not_active Expired - Lifetime
- 2001-12-11 AT AT01990083T patent/ATE375083T1/en active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1597293A (en) * | 1978-03-11 | 1981-09-03 | Atomic Energy Of Australia | Insect control |
US4582901A (en) * | 1984-08-09 | 1986-04-15 | The Research Foundation Of State University Of New York | Fluorinated cellulose esters and the use thereof as termiticidal compositions |
EP0587117A1 (en) * | 1992-09-08 | 1994-03-16 | Barbara L. Thorne | Method and compositions to monitor and control termites |
WO2000062610A1 (en) * | 1999-04-20 | 2000-10-26 | The United States Of America, As Represented By The Secretary Of Agriculture | Termite bait matrix |
US6139858A (en) * | 1999-12-01 | 2000-10-31 | Sumitomo Chemical Company Limited | Termite-controlling agent |
Non-Patent Citations (1)
Title |
---|
See also references of WO02052940A1 * |
Also Published As
Publication number | Publication date |
---|---|
WO2002052940A1 (en) | 2002-07-11 |
ATE375083T1 (en) | 2007-10-15 |
US6416752B1 (en) | 2002-07-09 |
AU2002228956B2 (en) | 2004-07-01 |
PT1347682E (en) | 2007-10-24 |
MXPA03006005A (en) | 2003-09-10 |
ES2295231T3 (en) | 2008-04-16 |
JP4317364B2 (en) | 2009-08-19 |
DE60130921T2 (en) | 2008-07-24 |
EP1347682B1 (en) | 2007-10-10 |
DE60130921D1 (en) | 2007-11-22 |
EP1347682A4 (en) | 2004-07-14 |
JP2004517104A (en) | 2004-06-10 |
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