Classifications

• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
  • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
  • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
  • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
  • B01J8/0278—Feeding reactive fluids
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
  • B01D—SEPARATION
  • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
  • B01D3/008—Liquid distribution
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
  • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
  • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
  • B01J2208/00796—Details of the reactor or of the particulate material
  • B01J2208/00823—Mixing elements
  • B01J2208/00858—Moving elements
  • B01J2208/00876—Moving elements outside the bed, e.g. rotary mixer
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
  • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
  • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
  • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
  • B01J2219/322—Basic shape of the elements
  • B01J2219/32203—Sheets
  • B01J2219/3221—Corrugated sheets
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
  • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
  • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
  • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
  • B01J2219/322—Basic shape of the elements
  • B01J2219/32203—Sheets
  • B01J2219/32213—Plurality of essentially parallel sheets
  • B01J2219/3222—Plurality of essentially parallel sheets with sheets having corrugations which intersect at an angle different from 90 degrees
• • B—PERFORMING OPERATIONS; TRANSPORTING
  • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
  • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
  • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
  • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
  • B01J2219/322—Basic shape of the elements
  • B01J2219/32203—Sheets
  • B01J2219/32224—Sheets characterised by the orientation of the sheet
  • B01J2219/32227—Vertical orientation

Definitions

• the present invention relates generally to chemical and petrochemical process reactors, columns, vessels and the like and, more particularly, to an apparatus and method for facilitating distribution of a fluid stream within such reactor, column or vessel.
• the present invention is directed to a fluid distributing element comprising a plurality of sheets disposed radially about a center axis.
• the sheets typically have radially outer ends that lie in a common circular plane so that the element forms the shape of a cylinder.
• the sheets have corrugations that extend at an angle to the center axis and define fluid flow channels having inlets at one end and outlets at an opposite end, typically the lower end.
• the corrugations in adjacent sheets extend in parallel or cris-crossing fashion so that fluid streams flowing along the channels form a full cone spray pattern as the fluid is discharged from the fluid flow channel outlets.
• the element is normally positioned at an outlet of a fluid-carrying conduit, but can also be positioned at a flow opening in a tray, plate or other structure. While the fluid distributing element is preferably used in connection with downwardly flowing fluid streams, it may be readily used in connection with fluid streams flowing horizontally or at other angles. In another aspect, the invention is directed to a method of effecting a more uniform distribution of fluid onto a surface of a bed of material, such as packing or catalyst, by flowing one or more fluid streams through the fluid flow element described above. If a single fluid distributing element is used, it is positioned to cause the full cone spray pattern to extend across substantially the entire surface of the bed of material.
• the fluid streams may contain more than one phase, such as vapor, liquid and/or particulate solid phases, which advantageously become mixed together as they flow through and are discharged from the fluid distributing element.
• FIG. 1 is a fragmentary side elevation view of a fluid distributor containing a radial distributing element constructed in accordance with the present invention
• FIG. 2 is a fragmentary side elevation view of the fluid distributor showing the radial distributing element on an enlarged scale;
• FIG. 3 is a top plan view of the radial distributing element;
• FIG. 4a is a side elevation view of the radial distributing element taken in vertical section along line 4a-4a of FIG. 3 in the direction of the arrows and showing an adjacent pair of corrugated plates;
• FIG. 4b is a side elevation view similar to FIG. 4a but showing an alternate embodiment of the radial distributing element
• FIG. 5 is a side elevation view of the radial distributing element taken in vertical section along line 5-5 of FIG. 3 in the direction of the arrows and showing a corrugated plate;
• FIG.6 is a side elevation view of a vessel taken in vertical section to show the internal positioning of the fluid distributor of the present invention
• FIG. 7 is a fragmentary side elevation view of another vessel taken in vertical section showing a plurality of the fluid distributors positioned on an internal tray;
• FIG. 8 is a top plan view of the vessel taken in horizontal section and showing, somewhat schematically, the fluid spray distribution from the fluid distributors.
• a fluid distributing element of the present invention is designated broadly by the numeral 10 and is shown positioned at a lower outlet 12 of a fluid conduit 14 such as a pipe and tubing.
• the fluid conduit 14 is vertically aligned and is formed by a cylindrical outer wall 16 that is supported on a surface 18 by a flange 20.
• the surface 18 may be an outer shell of a vessel or a tray or other structure within the vessel.
• a conventional static mixing element 19 may be positioned in the fluid conduit upstream from the fluid distributing element 10.
• the fluid distributing element 10 comprises aplurality of individual plates or sheets 22 that are arranged radially about a hub 24 positioned at a center axis of the element 10. At least some of the sheets 22 are fixed at their radially inner ends 26 to the hub 24 by welding, brazing or other securing means or may be integrally formed with the hub by casting, molding or other suitable processes. Other of the sheets 22 need not be directed fixed to the hub 24 and may simply be secured to and carried by those sheets which are fixed to the hub. In the illustrated embodiment, alternating sheets 22a are fixed to the hub 24 and carry the remaining sheets 22b whose inner ends 26 are spaced from the hub.
• the sheets 22 have radially outer ends 28 that preferably lie in a common circular plane so that the fluid distributing element 10 has a cylindrical configuration. Alternative configurations, such as cone-shaped, are possible and may be preferred in certain applications.
• the radial length and the vertically height of the sheets 22 are preselected for the intended applications in which the element 10 will be used. When used in conjunction with the fluid conduit 14, the radial length of the sheets 22 is preferably less than the inner diameter of the conduit outer wall 16 so that the fluid distributing element 10 may be inserted within the conduit 14 a preselected distance at the outlet 12. In some applications, the sheets are sized to extend across substantially the entire inner diameter or cross section of the conduit, while in other applications there will be a substantial gap between the outer ends 28 of the sheets and the conduit wall 16.
• the height of the sheets 22 must also be sufficient to allow a lower portion of the element 10 to extend below the conduit 14 to achieve the desired spray pattern of fluid exiting the element 10. While the element 10 will normally be maintained in a fixed longitudinal position within the conduit, suitable mechanisms (not shown) may be provided to permit the element's longitudinal position within the conduit to be varied as desired.
• the sheets 22 are formed with corrugations 30 that are inclined at one or more preselected angles, such as between 15 and 60 degrees, to the vertical center axis of the element.
• the corrugations 30 form fluid flow channels that have upper inlets and lower outlets.
• the corrugations 30 on adjacent sheets may be arranged in a cris-crossing fashion, so that corrugations and fluid flow channels on adjacent sheets are inclined in opposite radial directions as best seen in FIG. 4a.
• the corrugations may be arranged in parallel on adjacent sheets as shown in FIG. 4b. While some the corrugations 30 on adjacent sheets 22 are shown in contact with each other, this need not be the case in all instances. Instead, the corrugations on adjacent sheets may be spaced apart and/or planar sheets may be interposed between adjacent corrugated sheets.
• the sheets 22 may be formed from any suitable materials, including those materials commonly used for structured packing elements.
• the sheets may be formed from sheet metal, wire screen or gauze, plastics, and ceramics.
• the sheets 22 may also be provided with apertures (not shown) to facilitate mixing and distribution of the fluid stream by allowing it to pass through the corrugated sheets 22. Surface treatments such as grooves, fluting and the like may also be provided on the sheets 22.
• the hub 24 may be formed from the same materials selected for sheets 22 and may have many different configurations depending upon the intended application.
• the hub 24 is typically of solid cylindrical construction to completely block the flow of fluid through the hub or it may be a hollow cylinder that is open at both ends to permit the downward passage of fluid.
• the outer wall of the hollow cylinder may be fluid impermeable or it may be formed from wire screen or gauze or may include suitable apertures to permit fluid to flow through the walls of the cylinder.
• the lower end of the hub 24 may be flared outwardly or have another flow directing shape to facilitate the desired fluid spray pattern issuing from the fluid distributing element 10.
• the fluid distributing element 10 receives one or more fluid streams which enter the inlets and flow along the fluid flow channels defined by corrugations 30 before exiting through the outlets of the channels in a type spray pattern known as a full cone spray.
• the cris-crossing orientation of the corrugations 30 also facilitates mixing of the fluid streams, such as when vapor and liquid streams are present and/or when particulate solids are present in the streams.
• the fluid streams are normally directed to the element 10 by fluid conduit 14, but it will be appreciated that the conduit 14 need not be used in applications where the element 10 is simply positioned within an opening formed in a plate or other structure through which fluid passes.
• the fluid distributing element 10 can be used at an inlet 32 to a vessel 34 such as a chemical or petrochemical reactor or column.
• the conduit 14 is positioned at the inlet 32 formed in the vessel shell 36 and feeds one or more fluid streams to element 10 which is positioned at the conduit outlet 12.
• the fluid streams exiting from the element 10 are then sprayed in a full cone pattern across the entire cross section of an underlying bed 38 of material such as random or structured packings, catalysts, heat exchanger tube sheets, mist eliminators or molecular sieves to achieve uniform distribution of the fluid streams.
• the element 10 can also be positioned at other locations within the open interior region of the vessel to facilitate distribution and mixing of the fluid streams at such locations within the vessel.
• a plurality of fluid distributing elements 10 and conduits 14 are positioned in spaced apart relationship on a horizontally disposed tray 40 positioned within the vessel 34.
• the upper ends of the conduits 14 are open to permit fluid, such as liquid which accumulates on the tray 40, to enter the conduits and flow downwardly to feed the fluid distributing elements 10.
• the fluid is then discharged from the elements 10 in a plurality of full cone sprays that cover the cross section of the underlying bed 38, as illustrated somewhat schematically in FIG. 8.

Landscapes

• Chemical & Material Sciences (AREA)
• Chemical Kinetics & Catalysis (AREA)
• Organic Chemistry (AREA)
• Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
• Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
• Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
• Physical Or Chemical Processes And Apparatus (AREA)
• Nozzles (AREA)

Applications Claiming Priority (3)

Publications (1)

Family

ID=22407396

Family Applications (1)

Country Status (6)

Families Citing this family (2)

Family Cites Families (6)

• 2000
  • 2000-03-08 WO PCT/US2000/006026 patent/WO2000053307A1/en not_active Application Discontinuation
  • 2000-03-08 CA CA002362696A patent/CA2362696A1/en not_active Abandoned
  • 2000-03-08 MX MXPA01009023A patent/MXPA01009023A/es unknown
  • 2000-03-08 BR BR0008820-0A patent/BR0008820A/pt not_active IP Right Cessation
  • 2000-03-08 AU AU35175/00A patent/AU3517500A/en not_active Abandoned
  • 2000-03-08 EP EP00913802A patent/EP1165226A1/de not_active Withdrawn

Non-Patent Citations (1)

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