EP0843837A1 - Fibre optic device for homogenising a laser beam - Google Patents
Fibre optic device for homogenising a laser beamInfo
- Publication number
- EP0843837A1 EP0843837A1 EP96927747A EP96927747A EP0843837A1 EP 0843837 A1 EP0843837 A1 EP 0843837A1 EP 96927747 A EP96927747 A EP 96927747A EP 96927747 A EP96927747 A EP 96927747A EP 0843837 A1 EP0843837 A1 EP 0843837A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- front lenses
- lenses
- laser
- indices
- optical
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B27/00—Optical systems or apparatus not provided for by any of the groups G02B1/00 - G02B26/00, G02B30/00
- G02B27/09—Beam shaping, e.g. changing the cross-sectional area, not otherwise provided for
- G02B27/0938—Using specific optical elements
- G02B27/095—Refractive optical elements
- G02B27/0955—Lenses
- G02B27/0961—Lens arrays
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K26/00—Working by laser beam, e.g. welding, cutting or boring
- B23K26/02—Positioning or observing the workpiece, e.g. with respect to the point of impact; Aligning, aiming or focusing the laser beam
- B23K26/06—Shaping the laser beam, e.g. by masks or multi-focusing
- B23K26/0604—Shaping the laser beam, e.g. by masks or multi-focusing by a combination of beams
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K26/00—Working by laser beam, e.g. welding, cutting or boring
- B23K26/02—Positioning or observing the workpiece, e.g. with respect to the point of impact; Aligning, aiming or focusing the laser beam
- B23K26/06—Shaping the laser beam, e.g. by masks or multi-focusing
- B23K26/064—Shaping the laser beam, e.g. by masks or multi-focusing by means of optical elements, e.g. lenses, mirrors or prisms
- B23K26/066—Shaping the laser beam, e.g. by masks or multi-focusing by means of optical elements, e.g. lenses, mirrors or prisms by using masks
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B27/00—Optical systems or apparatus not provided for by any of the groups G02B1/00 - G02B26/00, G02B30/00
- G02B27/09—Beam shaping, e.g. changing the cross-sectional area, not otherwise provided for
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B27/00—Optical systems or apparatus not provided for by any of the groups G02B1/00 - G02B26/00, G02B30/00
- G02B27/09—Beam shaping, e.g. changing the cross-sectional area, not otherwise provided for
- G02B27/0905—Dividing and/or superposing multiple light beams
Definitions
- Fiber optic device for homogenizing a laser beam
- the present invention relates to a fiber optic device for homogenizing a laser beam.
- the energy distribution along the cross section of a laser beam is of Gaussian appearance, in any case variable according to the cross section of the beam.
- This homogeneity is especially required when the sample to be treated by laser is large (as described in the French Patent Application entitled “Device and method of surface treatment by laser”, filed by the Applicant on August 11 1995 under No. 95 09778., the content of which forms an integral part of this Request, for all practical purposes). It is also required when the incident laser beam is a combination of several laser beams emanating from a chain of laser modules arranged in parallel and / or in series (as described in the Patent Application entitled “Method and device for controlling 'a laser source with several laser modules to optimize surface treatment by laser ", filed by the Applicant on August 11, 1995 under No. 95 09780, the content of which forms an integral part of this Application, for all practical purposes) . Means are already known for homogenizing a laser beam.
- the present invention provides a solution to this problem.
- a fiber optic device for homogenizing a laser beam of the type comprising:
- a plurality of front lenses contiguous, arranged in m rows and n columns, perpendicular to the direction of propagation of the laser beam to be treated, and suitable for cutting said laser beam into mxn laser beams each having a substantially uniform cross section, and a substantially homogeneous energy distribution, and
- At least one collection lens converging, arranged perpendicular to the direction of propagation of the light beam, downstream of the front lenses in the direction of the path of the laser beam, said collection lens being able to focus the beams in a chosen plane from the front lenses.
- the device further comprises:
- a first intermediate plane substantially located in the focal plane of the front lenses, and having a plurality of entrance pupils each arranged substantially at the focal point of a front lens chosen from the plurality of front lenses;
- the collection lens being able to collecting the beams from the plurality of exit pupils
- Optical transmission means capable of individually transmitting the light beams coming from the entrance pupils to the plurality of exit pupils.
- the transmission means are thus able to transfer a plurality of homogeneous portions of the laser energy.
- the device according to the invention thus makes it possible to divide and transfer laser energy into a plurality of homogeneous portions of low power energy. This results in the elimination of the damage that can be caused by the effects of a high laser power, in particular on the optical elements of the device according to the invention.
- Such a device also makes it possible to obtain a homogeneous beam in the near field.
- the beam to be homogenized is a combination of several laser beams emanating from a chain of laser modules placed in parallel and / or in series.
- the optical transmission means comprise a plurality of optical fibers each comprising one end coupled to an entrance pupil and another end coupled to an exit pupil.
- optical fibers have a diameter of around 125 ⁇ m and a length of less than 1 m. As a variant, they have a length greater than 1 m.
- the plurality of optical fibers of indices i, j transmitting the laser beams coming from the front lenses are capable of distributing them according to a distribution of indices k, S. where at least some of the indices k and JE! are different from the indices i and j.
- the indices i and j are respectively equal to the indices k and £.
- the device further comprises a third intermediate plane having a plurality of additional front lenses, contiguous, arranged in q rows and r columns, perpen ⁇ dicular to the direction of propagation of the beams laser from the plurality of exit pupils, and adapted to receive said laser beams from the plurality of exit pupils as well as to cut them each into qr laser beams each having a substantially uniform cross section, and a substantially homogeneous energy distribution ; the collection lens being suitable for collecting in a chosen plane the laser beams coming from the additional front lenses.
- the optical transmission means comprise a plurality of discrete optical elements.
- FIG. 1 is a schematic representation of the essential means of the homogenizer
- FIG. 3 is a homogenizer with two collection lenses
- FIG. 5 schematically shows the plurality of optical fibers receiving the laser beams cut by the front lenses for routing them to the collection lens according to the invention
- FIG. 6 shows schematically ia distribution of laser beams cut by the front lenses according to a crossed distribution of the optical fibers according to the invention
- FIG. 7 shows a variant of the device described with reference to Figure 5 in which the laser beams cut by the front lenses and distributed by the optical fibers are cut again by a plurality of additional front lenses according to the invention.
- FIG. 8 is a variant of the device described with reference to Figure 6 in which the laser beams cut by the front lenses and distributed by the optical fibers are cut again by a plurality of additional front lenses.
- the reference FLA designates the laser beam to be homogenized.
- This laser beam has a non uniform energy distribution in cross section. It emanates for example from a laser or from a chain of laser modules placed in parallel and / or in series.
- this laser beam is intended for annealing amorphous silicon by laser.
- One application is to illuminate a large panel of amorphous silicon for the manufacture of flat liquid crystal screens. This laser beam is applied to the target plane CIB carrying the sample to be treated.
- the optical device for homogenizing a laser beam comprises mxn front lenses LF, convergent, jointed, arranged in m lines and n columns perpendicular (transversely) to the direction of propagation of the laser beam to be treated, m and n are whole numbers, for example m and n are equal to 7.
- the front lenses are arranged according to a straight or oblique rectangular matrix; for example, they are regularly distributed within a rectangle or a parallelogram.
- These lenses cut the FLA laser beam into m ⁇ n laser beams, each having a substantially uniform cross section and a substantially homogeneous energy distribution.
- a collection lens LC convergent, arranged perpendicular to the direction of propagation of the light beam, downstream of the front lenses LF in the direction of travel of the laser beam.
- This collection lens is suitable for focusing, in the target plane CIB, the beams coming from the front lenses.
- m x n DI diaphragms can be associated respectively with m x n front lenses.
- Each diaphragm is arranged substantially in the object focal plane of the associated lens and receives the light beam from the associated front lens in order to filter it spatially.
- the reference “a” designates the width of a front lens LF.
- the reference f designates the focal distance (close to the print) between a front lens and the associated diaphragm DI.
- the reference F designates the distance (which may be different from the focal distance) between a DI diaphragm and the collection lens LC.
- the reference A designates the width of the homogenized laser beam obtained by the homogenizer HO at the level of the plane CIB according to the invention.
- the dimension A is equal to a x F / f.
- Each DI diaphragm comprises an opening of selected shape and dimensions, for example circular.
- a support or mask MA maintains the plurality of diaphragms.
- the front lenses are for example of the convex-plane or biconvex, or convex-concave type. It is made so that the cross section of the light beam coming from each front lens whose shape is determined by the shape of the lenses, is rectangular or hexagonal, downstream of the diaphragms.
- the optical device When the LC collection lens is small in diameter, the optical device is less expensive and has fewer optical aberrations than with a large collection lens.
- the LC collection lens is arranged so that the focal plane of the LF lenses is not confused with that of the LC collection lens. This variant gives a reduction in the size of the homogenizer device.
- the path of the light rays shows here that the homogenizing device is not necessarily afocal.
- the collection lens LC is replaced by two converging lenses LC1 and LC2, arranged perpendicular to the direction of propagation of the light beam, downstream of the front lenses LF and the associated diaphragms DI.
- these collection lenses LC1 and LC2 are movable in translation along the optical axis.
- the distance d between the two lenses LC1 and LC2 is varied to vary the resulting focal length and to obtain, at the level of the target plane CIB, a homogenized beam size suitable for the chosen application, for example the size of the panels to be treated in the case of an amorphous silicon annealing.
- the other optical elements namely the front lenses LF, the diaphragms DI and the target plane CIB can also be movable in translation along the optical axis.
- the choice of the relative distances between the different optical elements makes it possible not only to adapt the size of the homogenized laser beam to the chosen application (possibility of choosing the magnification by varying the distance d), but also to reduce the bulk. of the homogenizer device.
- the choice of the distance d also makes it possible to adjust the energy per unit area delivered by the laser beam, as described in the Patent Application filed by the Applicant for "Method and control device a laser source with several laser modules to optimize the surface treatment by laser "and already mentioned above.
- FIG. 4 the path of several beams is shown through several front lenses LF of the same line m.
- front lenses LF of the same line m.
- These front lenses are for example of the convex-plane type. They are generally rectangular in shape with an inlet face FE, an outlet face FS and four lateral faces FL1 to FL4.
- the convex part receives the laser beam to be treated FLA.
- a lateral face of a front lens is defined for example by the points A2, A'3, B'3 and B2 for the lateral face FL3 of the central lens LF2.
- the laser beam to be treated from point A1 is applied to the central lens LF2 at point A2. This beam passes through the front lens LF2 to point A3 and is then routed to point A4. It should be noted that point A3 is slightly offset from point A'3.
- the convex part of a front lens here comprises two sharp edges such as BV.
- the front lens LF2 comprises a groove EN4 of shallow depth formed transversely in the lateral face FL1.
- the front lens LF2 comprises a groove EN3 of shallow depth formed transversely in the lateral face FL2.
- the grooves are formed near the exit face of the front lens.
- the two adjacent front lenses LF2 and LF3 are attached to each other.
- the cooperation of the respective grooves EN3 and EN2 allows bonding of said lenses by applying glue in said grooves EN3 and EN2, without disturbing the optical properties of the light beams passing through said front lenses LF2 and LF3.
- the path of the beam B1 through the central front lens LF2 passes along the points B2, B3 and B4.
- the front lenses are generally rectangular or hexagonal in shape with sides of the order of 1 cm in length.
- the beam to homogenize FLA is rectangular with sides of the order of 5 to 8 cm.
- the laser beams cut by the front lenses are transferred and distributed to the collection lens using optical transmission means such as optical fibers or discrete optical elements.
- the optical transmission means comprise a plurality of optical fibers FO of indices i and j, capable of individually transferring the laser beams coming from a plurality of entry pupils PE of indices m and n associated with the plurality of front lenses LF of indices m and n to a plurality of exit pupils PS of indices k and £.
- indices m and n or k and £ is meant here a two-dimensional matrix arranged in m columns (or k) and n rows (or £).
- the indices i and j vary here respectively from 1 to m and from 1 to n.
- the plurality of entry pupils PE is located on an intermediate plane PII disposed in the focal plane of the front lenses LF.
- the plurality of exit pupils PS with indices k and £ is arranged on an intermediate plane PI2 which can be separate from or superimposed on the intermediate plane PII.
- the entrance and / or exit pupils can be materialized or not. Materialization improves spatial filtering. Furthermore, the optical correspondence between the entrance pupils and the exit pupils is here advantageously one-to-one.
- each optical fiber FO contributes for its part to the transfer of a portion of the laser energy.
- the device according to the invention thus makes it possible to divide and transfer a high power laser energy into a plurality of lower power portions of energy. This results in the elimination of the damage that can be caused by the effects of high laser power, in particular on the optical elements of the device.
- these optical fibers FO may be arranged in an at least partially crossed bundle. That is to say that at least some of the fibers of indices i, j each connect an exit pupil PS not having the same values of i and / or j. In principle, these crossings are arranged so that any exit pupil remains supplied from one of the entry pupils.
- the bundle of fibers collecting the energies of the lenses LF ij can distribute them according to a distribution PS k _ g where at least some of the k and £ are different from the i and j. This allows the energy distribution at the output to be brought even closer to the characteristics desired for the latter (FIG. 6).
- optical fibers also make it possible to illuminate a target plane CIB situated outside the optical axis of the laser beams FLA.
- the device according to the invention further comprises an intermediate plane PI3 having a plurality of front lenses additional res LFS of indices q and r, arranged in q lines and r colonies, perpendicular to the direction of propagation of the laser beams coming from the plurality of exit pupils PS k _g.
- This plurality of additional front lenses receives the laser beams from the plurality of exit pupils PS ki in order to cut them each into qr laser beams each having a substantially uniform cross section and a substantially homogeneous energy distribution.
- the collection lens (s) collect (s) in the chosen plane CIB the laser beams thus cut by the additional front lenses.
- the laser beams coming from the exit pupils PS ki are cut by the additional front lenses LFS ⁇ r according to a distribution where at least some of the indices k and £ are different from the indices q and r.
- an intermediate plane PI4 has a plurality of diaphragms DI with indices q and r.
- the diaphragms DI with indices q and r receive the laser beams with indices q and r from the plurality of additional front lenses LFS in order to filter them spatially.
- Optical fibers can be long or short. For example, they have a diameter of the order of 125 ⁇ m (core of the fiber).
- a short fiber For a 125 ⁇ m core, a short fiber is less than 1 meter long. It retains the shape of the cross section of the beam which penetrates it.
- a long fiber For a 125 ⁇ m core, a long fiber is longer than 1 m. It depolarizes the light beam which penetrates it and emits a light beam provided with a symmetry of revolution.
- the additional front lenses LFS are arranged at a distance 2f from the plane intermediate PI2 and intermediate plan PI4. Under these conditions, the light beams coming from the exit pupils PS illuminate several additional front lenses.
Landscapes
- Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Engineering & Computer Science (AREA)
- General Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Mechanical Engineering (AREA)
- Laser Beam Processing (AREA)
- Optical Couplings Of Light Guides (AREA)
- Laser Surgery Devices (AREA)
- Lenses (AREA)
- Glass Compositions (AREA)
- Manufacture, Treatment Of Glass Fibers (AREA)
- Recrystallisation Techniques (AREA)
Abstract
Description
Claims
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR9509781 | 1995-08-11 | ||
FR9509781A FR2737786B1 (en) | 1995-08-11 | 1995-08-11 | OPTICAL DEVICE FOR HOMOGENEIZING A LASER BEAM |
PCT/FR1996/001252 WO1997007424A1 (en) | 1995-08-11 | 1996-08-06 | Fibre optic device for homogenising a laser beam |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0843837A1 true EP0843837A1 (en) | 1998-05-27 |
EP0843837B1 EP0843837B1 (en) | 1999-06-16 |
Family
ID=9481901
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP96927746A Expired - Lifetime EP0843836B1 (en) | 1995-08-11 | 1996-08-06 | Optical device for homogenising a laser beam |
EP96927747A Expired - Lifetime EP0843837B1 (en) | 1995-08-11 | 1996-08-06 | Fibre optic device for optically processing a laser beam |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP96927746A Expired - Lifetime EP0843836B1 (en) | 1995-08-11 | 1996-08-06 | Optical device for homogenising a laser beam |
Country Status (9)
Country | Link |
---|---|
US (2) | US6014260A (en) |
EP (2) | EP0843836B1 (en) |
JP (2) | JP2000502190A (en) |
KR (2) | KR100404297B1 (en) |
AT (2) | ATE181425T1 (en) |
CA (2) | CA2224997A1 (en) |
DE (2) | DE69602952T2 (en) |
FR (1) | FR2737786B1 (en) |
WO (2) | WO1997007424A1 (en) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2737806B1 (en) * | 1995-08-11 | 1997-09-12 | Soc D Production Et De Rech Ap | LASER SURFACE TREATMENT DEVICE AND METHOD |
DE19753344A1 (en) * | 1997-12-02 | 1999-06-10 | Rodenstock Instr | Device for homogenizing a light or laser beam |
JP3370612B2 (en) | 1998-09-14 | 2003-01-27 | 富士通株式会社 | Light intensity conversion element, collimating lens, objective lens, and optical device |
IT1316395B1 (en) * | 2000-04-28 | 2003-04-10 | Enea Ente Nuove Tec | OPTICAL SYSTEM FOR SPACE HOMOGENIZATION OF LIGHT BEAMS, SUSPENDED WITH VARIABLE SECTION. |
US6750423B2 (en) * | 2001-10-25 | 2004-06-15 | Semiconductor Energy Laboratory Co., Ltd. | Laser irradiation method, laser irradiation apparatus, and method of manufacturing a semiconductor device |
CA2386952A1 (en) * | 2002-05-17 | 2003-11-17 | Exfo Photonic Solutions Inc. | Radiation power demultiplexer |
US6879448B2 (en) * | 2003-06-26 | 2005-04-12 | International Business Machines Corporation | Apparatus for achromatizing optical beams |
US7016393B2 (en) * | 2003-09-22 | 2006-03-21 | Coherent, Inc. | Apparatus for projecting a line of light from a diode-laser array |
DE102004039936A1 (en) * | 2004-08-17 | 2006-02-23 | Hentze-Lissotschenko Patentverwaltungs Gmbh & Co. Kg | Device for homogenizing light and method for producing the device |
US7265908B2 (en) * | 2005-12-19 | 2007-09-04 | Coherent, Inc. | Apparatus for projecting a line of light from a diode-laser array |
JP2007286211A (en) * | 2006-04-14 | 2007-11-01 | Alps Electric Co Ltd | Optical member and optical communication module |
GB2437496A (en) * | 2006-04-28 | 2007-10-31 | Rolls Royce Plc | A laser shaping arrangement |
JP2009251381A (en) * | 2008-04-08 | 2009-10-29 | Mitsubishi Electric Corp | Laser irradiation device |
KR102425180B1 (en) * | 2020-07-15 | 2022-07-29 | (주)프로옵틱스 | Line beam forming device |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4293190A (en) * | 1978-05-31 | 1981-10-06 | Oakeridge Management Services B.V. | Transparency viewers |
US4516832A (en) * | 1982-06-23 | 1985-05-14 | International Business Machines Corporation | Apparatus for transformation of a collimated beam into a source of _required shape and numerical aperture |
DE3634847A1 (en) * | 1985-10-11 | 1987-04-16 | Ricoh Kk | Ridge mirror/lens arrangement and frame for the arrangement |
EP0266120A3 (en) * | 1986-10-31 | 1990-07-11 | AT&T Corp. | Generating an array of light spots having uniform intensity |
JPH01286478A (en) * | 1988-05-13 | 1989-11-17 | Hitachi Ltd | Beam uniformizing optical system and manufacture thereof |
US5253110A (en) * | 1988-12-22 | 1993-10-12 | Nikon Corporation | Illumination optical arrangement |
CN1052956A (en) * | 1989-12-25 | 1991-07-10 | 中国科学院上海光学精密机械研究所 | Line focusing system of cylindrical lenses array |
IL101471A (en) * | 1991-05-01 | 1995-03-30 | Coherent Inc | Coupler for a laser delivery system |
DE4220705C2 (en) * | 1992-06-24 | 2003-03-13 | Lambda Physik Ag | Device for splitting a light beam into homogeneous partial beams |
US5363240A (en) * | 1992-11-13 | 1994-11-08 | Ricoh Company, Ltd. | Image forming device and method for producing it |
US5463200A (en) * | 1993-02-11 | 1995-10-31 | Lumonics Inc. | Marking of a workpiece by light energy |
US5610733A (en) * | 1994-02-28 | 1997-03-11 | Digital Optics Corporation | Beam-homogenizer |
FR2737814B1 (en) * | 1995-08-11 | 1997-09-12 | Soc D Production Et De Rech Ap | METHOD AND DEVICE FOR CONTROLLING A LASER SOURCE WITH MULTIPLE LASER MODULES TO OPTIMIZE LASER SURFACE TREATMENT |
FR2737806B1 (en) * | 1995-08-11 | 1997-09-12 | Soc D Production Et De Rech Ap | LASER SURFACE TREATMENT DEVICE AND METHOD |
-
1995
- 1995-08-11 FR FR9509781A patent/FR2737786B1/en not_active Expired - Fee Related
-
1996
- 1996-08-06 WO PCT/FR1996/001252 patent/WO1997007424A1/en active IP Right Grant
- 1996-08-06 EP EP96927746A patent/EP0843836B1/en not_active Expired - Lifetime
- 1996-08-06 EP EP96927747A patent/EP0843837B1/en not_active Expired - Lifetime
- 1996-08-06 US US09/000,001 patent/US6014260A/en not_active Expired - Lifetime
- 1996-08-06 KR KR10-1998-0700877A patent/KR100404297B1/en not_active IP Right Cessation
- 1996-08-06 CA CA002224997A patent/CA2224997A1/en not_active Abandoned
- 1996-08-06 AT AT96927747T patent/ATE181425T1/en not_active IP Right Cessation
- 1996-08-06 JP JP9508983A patent/JP2000502190A/en not_active Ceased
- 1996-08-06 JP JP9508984A patent/JP2000502191A/en not_active Ceased
- 1996-08-06 KR KR10-1998-0700876A patent/KR100404298B1/en not_active IP Right Cessation
- 1996-08-06 CA CA002224998A patent/CA2224998C/en not_active Expired - Fee Related
- 1996-08-06 WO PCT/FR1996/001251 patent/WO1997007423A1/en active IP Right Grant
- 1996-08-06 AT AT96927746T patent/ATE181424T1/en not_active IP Right Cessation
- 1996-08-06 DE DE69602952T patent/DE69602952T2/en not_active Expired - Lifetime
- 1996-08-06 US US09/000,111 patent/US6055346A/en not_active Expired - Lifetime
- 1996-08-06 DE DE69602951T patent/DE69602951T2/en not_active Expired - Fee Related
Non-Patent Citations (1)
Title |
---|
See references of WO9707424A1 * |
Also Published As
Publication number | Publication date |
---|---|
FR2737786A1 (en) | 1997-02-14 |
KR19990036208A (en) | 1999-05-25 |
FR2737786B1 (en) | 1997-09-12 |
CA2224997A1 (en) | 1997-02-27 |
US6014260A (en) | 2000-01-11 |
KR100404297B1 (en) | 2004-01-31 |
EP0843837B1 (en) | 1999-06-16 |
JP2000502191A (en) | 2000-02-22 |
ATE181425T1 (en) | 1999-07-15 |
DE69602952T2 (en) | 2000-02-17 |
DE69602951T2 (en) | 2000-02-17 |
KR100404298B1 (en) | 2004-01-28 |
EP0843836B1 (en) | 1999-06-16 |
DE69602952D1 (en) | 1999-07-22 |
KR19990036209A (en) | 1999-05-25 |
CA2224998A1 (en) | 1997-02-27 |
US6055346A (en) | 2000-04-25 |
JP2000502190A (en) | 2000-02-22 |
CA2224998C (en) | 2007-10-30 |
EP0843836A1 (en) | 1998-05-27 |
ATE181424T1 (en) | 1999-07-15 |
WO1997007424A1 (en) | 1997-02-27 |
DE69602951D1 (en) | 1999-07-22 |
WO1997007423A1 (en) | 1997-02-27 |
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