EP0668478A1 - Receptacle with stirring device - Google Patents
Receptacle with stirring device Download PDFInfo
- Publication number
- EP0668478A1 EP0668478A1 EP94117059A EP94117059A EP0668478A1 EP 0668478 A1 EP0668478 A1 EP 0668478A1 EP 94117059 A EP94117059 A EP 94117059A EP 94117059 A EP94117059 A EP 94117059A EP 0668478 A1 EP0668478 A1 EP 0668478A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- gas
- container
- gas guide
- pipe socket
- guide cartridge
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Images
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B11/00—Machines or apparatus for drying solid materials or objects with movement which is non-progressive
- F26B11/12—Machines or apparatus for drying solid materials or objects with movement which is non-progressive in stationary drums or other mainly-closed receptacles with moving stirring devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/40—Mixers using gas or liquid agitation, e.g. with air supply tubes
- B01F33/409—Parts, e.g. diffusion elements; Accessories
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B21/00—Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
- F26B21/003—Supply-air or gas filters
Definitions
- the invention relates to an agitator container for drying and possibly granulating pourable products according to the preamble of the main claim.
- the invention has for its object to achieve a uniform flow through the product to be treated in a stirrer tank with trailing gas, but the gas inlet openings can be inspected at any time and thus qualifiable and validatable machines can be offered to the pharmaceutical industry.
- the gas is supplied through the insulating jacket, the gas being conducted into a cylindrical cartridge unit.
- This unit has a cylindrical element with a conical taper, which is equipped with a sieve fabric of 10 ⁇ m or smaller and which enables the gas to enter the product of the agitator tank through this stainless steel sieve fabric.
- the gas supply through the insulating jacket construction of the actual agitator tank is designed so that no dead zones are created in this area in the event of cleaning, but instead the gas is discharged at the deepest point and any cleaning and disinfection liquid can also be supplied.
- the removable cartridges can be closed vacuum-tight with the inside of the container using a quick-release fastener in the form of a clamping ring. This ensures that the towing gas cannot escape to the outside.
- Air with sufficient filtering according to pharmaceutical quality with a normal room temperature can be used as the trailing gas, but also an inert gas.
- the new device it is possible to remove a water-bound granulating aid from the product within a third of the normal vacuum drying time.
- a section of a container bottom wall 1 is shown, which has a gas inlet opening 2.
- the container bottom wall is traversed by a pipe socket 6, which is welded firmly to the metallic wall parts of the bottom wall 1, with part of the insulating jacket 14 and part of the water jacket 15 being still visible in the illustrated embodiment.
- the pipe socket 6 connects to the opening of the container bottom wall in such a way that an annular step is created, on which a gas guide cartridge 3 which can be inserted into the pipe socket 6 is supported.
- the support takes place with the interposition of an annular seal 9.
- the actual gas inlet opening 2 of the container bottom 1 or the gas guide cartridge 3 is closed by a sieve fabric 4 which is very close-meshed, for example has a mesh size of 10 ⁇ m.
- the gas guide cartridge 3 has on its outside an annular collar 8 with which it is supported on the outer part of the pipe socket 6, again again with the interposition of an annular seal 10.
- the gas guide cartridge 3 is fixed on the pipe socket 6 via a clamping ring 11, so that a vacuum-tight connection between the gas guide cartridge 3 and the pipe socket 6 and the In nenraum of the actual agitator tank is created.
- gas guide cartridges 3 and pipe sockets 6 can be provided in an agitator tank which is designed in accordance with the innovation, and the emptying flap arranged in the center of the agitator tank bottom can additionally be provided with a gas guide cartridge 3 and a pipe connector 6.
- the new device enables the supply of entraining gas to a large extent in an agitator container, so that the drying time of the container contents can thereby be considerably reduced.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Drying Of Solid Materials (AREA)
- Catching Or Destruction (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Accessories For Mixers (AREA)
Abstract
Description
Die Erfindung bezieht sich auf einen Rührwerksbehälter zum Trocknen und ggf. Granulieren von schüttfähigen Produkten gemäß dem Oberbegriff des Hauptanspruches.The invention relates to an agitator container for drying and possibly granulating pourable products according to the preamble of the main claim.
In bekannten Vorrichtungen zum Trocknen und ggf. Granulieren von pulverisiertem Materal für pharmazeutische Produkte, z. B. gemäß der EP-385 965 B1, erfolgt das Zuführen des sogenannten "Schleppgases" zum Abführen der Feuchte aus dem Trocknungsprozeß durch einen dreiarmigen Rührflügel hindurch in das Produkt. Dieses hat den Nachteil, daß es nur drei Einlaßstellen in einem Rührwerksbehälter gibt, da der dreiarmige Rührflügel eben nur an drei Stellen das Gas in das Produkt ablassen kann. Hierbei bilden sich im Stillstand des Rührflügels schnell Zonen, durch die das Gas in Kanälen entweicht, und das übrige Produkt kommt nicht mit dem Trocknungsgas in Berührung. Nur wenn der Rührflügel in Bewegung ist, ist eine einigermaßen gleichmäßige Durchflutung des zu bearbeitenden Produktes mit Gas sicherzustellen. Da aber bei einer Granulation mit anschließender oder gleichzeitiger Trocknung das Wesentliche darin besteht, daß das Produkt nicht zu stark durch einen Rührer mechanisch beansprucht wird, ist es vorteilhaft, wenn man den Rührer nicht sehr oft in Bewegung setzen muß, sondern die Schleppgasverteilung auf den Umfang des Produktes durch andere Maßnahmen sicherstellen könnte.In known devices for drying and possibly granulating pulverized material for pharmaceutical products, e.g. B. according to EP-385 965 B1, the supply of the so-called "entraining gas" for removing the moisture from the drying process takes place through a three-armed impeller into the product. This has the disadvantage that there are only three inlet points in an agitator tank, since the three-armed impeller can only release the gas into the product at three points. When the agitator blade is at a standstill, zones quickly form through which the gas escapes in channels, and the rest of the product does not come into contact with the drying gas. Only when the impeller is in motion can a reasonably uniform flow of gas through the product to be processed be ensured. However, since in a granulation with subsequent or simultaneous drying the essential thing is that the product is not mechanically stressed too much by a stirrer, it is advantageous if one does not have to set the stirrer very often, but rather the trailing gas distribution over the circumference of the product by other measures.
Bei den bekannten Anordnungen entsteht auch ein hygienisches Problem. Die Aussparungen in den Rührwerksflügeln werden über Sintermetalle oder ähnliche poröse Werkstoffe erreicht, die sich aber schlecht oder gar nicht reinigen lassen, so daß derartige Einrichtungen für pharmazeutische Produkte nicht einsetzbar sind.In the known arrangements, there is also a hygienic problem. The recesses in the agitator blades are achieved via sintered metals or similar porous materials, which are difficult or impossible to clean, so that such devices cannot be used for pharmaceutical products.
Der Erfindung liegt die Aufgabe zugrunde, eine gleichmäßige Durchströmung des zu behandelnden Produktes in einem Rührwerksbehälter mit Schleppgas zu erreichen, wobei aber die Gaseintrittsöffnungen jederzeit inspizierbar sind und somit qualifizierbare und validierbare Maschinen der pharmazeutischen Industrie angeboten werden können.The invention has for its object to achieve a uniform flow through the product to be treated in a stirrer tank with trailing gas, but the gas inlet openings can be inspected at any time and thus qualifiable and validatable machines can be offered to the pharmaceutical industry.
Diese der Erfindung zugrundeliegende Aufgabe wird durch die Lehre des Hauptanspruches gelöst.This object on which the invention is based is achieved by the teaching of the main claim.
Vorteilhafte Ausgestaltungen sind in den Unteransprüchen erläutert.Advantageous configurations are explained in the subclaims.
Mit anderen Worten ausgedrückt erfolgt bei der neuen Einrichtung die Gaszufuhr durch den Isoliermantel, wobei das Gas in eine zylindrische Cartridge-Einheit geleitet wird. Diese Einheit weist ein zylindrisches Element mit konischer Verjüngung auf, das mit einem Siebgewebe von 10 um oder kleiner ausgestattet ist und dem Gas die Möglichkeit gibt, durch dieses Edelstahlsiebgewebe in das Produkt des Rührwerksbehälters einzutreten. Die Gaszufuhr durch die Isoliermantelkonstruktion des eigentlichen Rührwerksbehälters ist so ausgebildet, daß im Reinigungsfall keine Totzonen in diesem Bereich geschaffen werden, sondern an der tiefsten Stelle jeweils der Austritt des Gases erfolgt und somit auch eine eventuelle Reinigungs- und Desinfektionsflüssigkeit zugeführt werden kann. Über einen Schnellverschluß in Form eines Spannringes lassen sich die demontierbaren Patronen vakuumdicht mit dem Behälterinneren verschließen. So ist sichergestellt, daß das Schleppgas nicht nach außen dringen kann.In other words, in the new device, the gas is supplied through the insulating jacket, the gas being conducted into a cylindrical cartridge unit. This unit has a cylindrical element with a conical taper, which is equipped with a sieve fabric of 10 µm or smaller and which enables the gas to enter the product of the agitator tank through this stainless steel sieve fabric. The gas supply through the insulating jacket construction of the actual agitator tank is designed so that no dead zones are created in this area in the event of cleaning, but instead the gas is discharged at the deepest point and any cleaning and disinfection liquid can also be supplied. The removable cartridges can be closed vacuum-tight with the inside of the container using a quick-release fastener in the form of a clamping ring. This ensures that the towing gas cannot escape to the outside.
Als Schleppgas kann sowohl Luft mit einer ausreichenden Filtrierung nach Pharma-Qualität mit einer ganz normalen Raumtemperatur eingesetzt werden, aber auch ein Inertgas. Mit der neuerungsgemäßen Einrichtung ist es möglich, ein wassergebundenes Granulierhilfsmittel innerhalb eines Drittels der normalen Vakuumtrocknungszeit aus dem Produkt zu entfernen.Air with sufficient filtering according to pharmaceutical quality with a normal room temperature can be used as the trailing gas, but also an inert gas. With the new device, it is possible to remove a water-bound granulating aid from the product within a third of the normal vacuum drying time.
Ein Ausführungsbeispiel der Erfindung wird nachfolgend anhand der Zeichnung erläutert.An embodiment of the invention is explained below with reference to the drawing.
In der Zeichnung ist ein Ausschnitt aus einer Behälterbodenwand 1 dargestellt, die eine Gaseinlaßöffnung 2 aufweist. Die Behälterbodenwand wird von einem Rohrstutzen 6 durchquert, der fest mit den metallischen Wandteilen der Bodenwand 1 verschweißt ist, wobei bei dem dargestellten Ausführungsbeispiel weiterhin ein Teil des Isoliermantels 14 und ein Teil des Wassermantels 15 erkennbar ist.In the drawing, a section of a
Bei dem dargestellten Ausführungsbeispiel schließt der Rohrstutzen 6 an die Öffnung der Behälterbodenwand so an, daß eine Ringstufe geschaffen wird, auf die sich eine in den Rohrstutzen 6 einsetzbare Gasführungspatrone 3 abstützt. Die Abstützung erfolgt dabei unter Zwischenschaltung einer Ringdichtung 9.In the illustrated embodiment, the
Die eigentliche Gaseinlaßöffnung 2 des Behälterbodens 1 oder der Gasführungspatrone 3 wird durch ein Siebgewebe 4 verschlossen, das sehr engmaschig ist, beispielsweise eine Maschenweite von 10 um aufweist.The actual gas inlet opening 2 of the
In den Raum des Rohrstutzens 6 führt eine Gaszuführungsleitung 7, die frei im Raum des Rohrstutzens 6 mündet, wobei zwischen dem Inneren dieser Gaszuführungsleitung 7 und dem Innenraum 5 der Gasführungspatrone 3 eine Verbindung durch Gasöffnungen 12 hergestellt wird, die in der Zeichnung erkennbar sind.In the space of the
Die Gasführungspatrone 3 weist an ihrer Außenseite einen Ringkragen 8 auf, mit dem sie sich auf dem äußeren Teil des Rohrstutzens 6 abstützt, und zwar ebenfalls wiederum unter Zwischenschaltung einer Ringdichtung 10. Die Festlegung der Gasführungspatrone 3 an dem Rohrstutzen 6 erfolgt über einen Spannring 11, so daß eine vakuumdichte Verbindung zwischen der Gasführungspatrone 3 und dem Rohrstutzen 6 sowie dem Innenraum des eigentlichen Rührwerksbehälters geschaffen wird.The
In einem Rührwerksbehälter, der neuerungsgemäß ausgebildet ist, können sechs solcher Gasführungspatronen 3 und Rohrstutzen 6 vorgesehen sein, und auch die im Zentrum des Rührwerksbehälterbodens angeordnete Entleerungsklappe kann zusätzlich mit einer Gasführungspatrone 3 und einem Rohrstutzen 6 versehen sein.Six such
Die neue Vorrichtung ermöglicht die Zufuhr von Schleppgas in einen Rührwerksbehälter in 35großem Umfang, so daß dadurch die Trocknungszeit des Behälterinhaltes erheblich verringert werden kann.The new device enables the supply of entraining gas to a large extent in an agitator container, so that the drying time of the container contents can thereby be considerably reduced.
Claims (8)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE9402499U | 1994-02-16 | ||
DE9402499U DE9402499U1 (en) | 1994-02-16 | 1994-02-16 | Agitator tank |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0668478A1 true EP0668478A1 (en) | 1995-08-23 |
EP0668478B1 EP0668478B1 (en) | 1998-07-22 |
Family
ID=6904618
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP94117059A Expired - Lifetime EP0668478B1 (en) | 1994-02-16 | 1994-10-28 | Receptacle with stirring device |
Country Status (2)
Country | Link |
---|---|
EP (1) | EP0668478B1 (en) |
DE (2) | DE9402499U1 (en) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20040081704A1 (en) | 1998-02-13 | 2004-04-29 | Centerpulse Biologics Inc. | Implantable putty material |
US20020114795A1 (en) | 2000-12-22 | 2002-08-22 | Thorne Kevin J. | Composition and process for bone growth and repair |
US7166133B2 (en) | 2002-06-13 | 2007-01-23 | Kensey Nash Corporation | Devices and methods for treating defects in the tissue of a living being |
US7718616B2 (en) | 2006-12-21 | 2010-05-18 | Zimmer Orthobiologics, Inc. | Bone growth particles and osteoinductive composition thereof |
JP2013542837A (en) | 2010-11-15 | 2013-11-28 | ジンマー オーソバイオロジクス,インコーポレイティド | Bone void filler |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB191312232A (en) * | 1912-08-26 | 1914-01-08 | Theodor Otto Franke | Improvements in Processes and Apparatus for Heating Material Containing Liquid. |
US3829022A (en) * | 1973-04-04 | 1974-08-13 | Material Control Inc | Aerating device for pulverulent material |
US3862707A (en) * | 1973-05-04 | 1975-01-28 | Material Control Inc | Bin aerator assembly or unit |
US3913238A (en) * | 1972-07-20 | 1975-10-21 | Day J H Co | Method and apparatus for drying particulate materials |
EP0019594A1 (en) * | 1979-05-21 | 1980-11-26 | Glatt Maschinen- und Apparatebau AG | Apparatus for producing granules or agglomerates |
US4465238A (en) * | 1981-09-04 | 1984-08-14 | Jhina Patel | Filter for hot air nozzle |
GB2158365A (en) * | 1985-05-09 | 1985-11-13 | Littleford Bros Inc | Combined mixing, reacting, drying and filtering device |
EP0268691A1 (en) * | 1986-11-20 | 1988-06-01 | Thomas Lammers | Device for drying construction parts furnished with a surface layer |
-
1994
- 1994-02-16 DE DE9402499U patent/DE9402499U1/en not_active Expired - Lifetime
- 1994-10-28 DE DE59406496T patent/DE59406496D1/en not_active Expired - Lifetime
- 1994-10-28 EP EP94117059A patent/EP0668478B1/en not_active Expired - Lifetime
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB191312232A (en) * | 1912-08-26 | 1914-01-08 | Theodor Otto Franke | Improvements in Processes and Apparatus for Heating Material Containing Liquid. |
US3913238A (en) * | 1972-07-20 | 1975-10-21 | Day J H Co | Method and apparatus for drying particulate materials |
US3829022A (en) * | 1973-04-04 | 1974-08-13 | Material Control Inc | Aerating device for pulverulent material |
US3862707A (en) * | 1973-05-04 | 1975-01-28 | Material Control Inc | Bin aerator assembly or unit |
EP0019594A1 (en) * | 1979-05-21 | 1980-11-26 | Glatt Maschinen- und Apparatebau AG | Apparatus for producing granules or agglomerates |
US4465238A (en) * | 1981-09-04 | 1984-08-14 | Jhina Patel | Filter for hot air nozzle |
GB2158365A (en) * | 1985-05-09 | 1985-11-13 | Littleford Bros Inc | Combined mixing, reacting, drying and filtering device |
EP0268691A1 (en) * | 1986-11-20 | 1988-06-01 | Thomas Lammers | Device for drying construction parts furnished with a surface layer |
Also Published As
Publication number | Publication date |
---|---|
DE9402499U1 (en) | 1994-07-14 |
EP0668478B1 (en) | 1998-07-22 |
DE59406496D1 (en) | 1998-08-27 |
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