EP0655507A3 - Process for preparing crystallized sugar from aqueous sugar juice, e.g. sugar cane juice a sugar beet juice. - Google Patents

Process for preparing crystallized sugar from aqueous sugar juice, e.g. sugar cane juice a sugar beet juice. Download PDF

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Publication number
EP0655507A3
EP0655507A3 EP94402540A EP94402540A EP0655507A3 EP 0655507 A3 EP0655507 A3 EP 0655507A3 EP 94402540 A EP94402540 A EP 94402540A EP 94402540 A EP94402540 A EP 94402540A EP 0655507 A3 EP0655507 A3 EP 0655507A3
Authority
EP
European Patent Office
Prior art keywords
sugar
juice
crystalline
aqueous
manufacture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP94402540A
Other languages
German (de)
French (fr)
Other versions
EP0655507A2 (en
EP0655507B1 (en
Inventor
Robert J Kwok
Xavier Lancrenon
Marc-Andre Theoleyre
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Applexion SAS
Original Assignee
Applexion SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Applexion SAS filed Critical Applexion SAS
Publication of EP0655507A2 publication Critical patent/EP0655507A2/en
Publication of EP0655507A3 publication Critical patent/EP0655507A3/en
Application granted granted Critical
Publication of EP0655507B1 publication Critical patent/EP0655507B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B35/00—Extraction of sucrose from molasses
    • C13B35/02—Extraction of sucrose from molasses by chemical means
    • C13B35/06—Extraction of sucrose from molasses by chemical means using ion exchange
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00—Purification of sugar juices
    • C13B20/02—Purification of sugar juices using alkaline earth metal compounds
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00—Purification of sugar juices
    • C13B20/12—Purification of sugar juices using adsorption agents, e.g. active carbon
    • C13B20/123—Inorganic agents, e.g. active carbon
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00—Purification of sugar juices
    • C13B20/14—Purification of sugar juices using ion-exchange materials
    • C13B20/144—Purification of sugar juices using ion-exchange materials using only cationic ion-exchange material
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00—Purification of sugar juices
    • C13B20/16—Purification of sugar juices by physical means, e.g. osmosis or filtration
    • C13B20/165—Purification of sugar juices by physical means, e.g. osmosis or filtration using membranes, e.g. osmosis, ultrafiltration
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
    • C13B30/02—Crystallisation; Crystallising apparatus

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Water Supply & Treatment (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Saccharide Compounds (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Seasonings (AREA)
  • Fats And Perfumes (AREA)

Abstract

The subject of the present invention is a process for the manufacture of crystalline sugar from an aqueous sugar juice (liquor) containing sugars and organic and inorganic impurities, including Ca<2+> and/or Mg<2+> ions, such as a sugar cane juice or a sugar beet juice, which comprises the operations: (a) of concentrating the said sugar juice, in order to obtain a syrup, and (b) of crystallising the said syrup, in order to obtain a crystalline sugar and a molasses, characterised in that it additionally comprises an operation: (c) of tangential microfiltration, of tangential ultrafiltration or of tangential nanofiltration, this operation being carried out before the operation (a). Another subject of the invention is a process for the manufacture of crystalline white sugar from a sugar juice of the sugar cane juice type, comprising the abovementioned process for the manufacture of crystalline sugar, completed by remelting, decolorisation and crystallisation operations. <IMAGE>
EP94402540A 1993-11-12 1994-11-09 Process for preparing crystallized sugar from aqueous sugar juice, e.g. sugar cane juice or sugar beet juice Expired - Lifetime EP0655507B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US151383 1993-11-12
US08/151,383 US5554227A (en) 1993-11-12 1993-11-12 Process of manufacturing crystal sugar from an aqueous sugar juice such as cane juice or sugar beet juice

Publications (3)

Publication Number Publication Date
EP0655507A2 EP0655507A2 (en) 1995-05-31
EP0655507A3 true EP0655507A3 (en) 1996-03-20
EP0655507B1 EP0655507B1 (en) 2002-07-17

Family

ID=22538521

Family Applications (1)

Application Number Title Priority Date Filing Date
EP94402540A Expired - Lifetime EP0655507B1 (en) 1993-11-12 1994-11-09 Process for preparing crystallized sugar from aqueous sugar juice, e.g. sugar cane juice or sugar beet juice

Country Status (14)

Country Link
US (2) US5554227A (en)
EP (1) EP0655507B1 (en)
CN (1) CN1105705A (en)
AT (1) ATE220727T1 (en)
AU (1) AU698506B2 (en)
BR (1) BR9404350A (en)
CO (1) CO4370065A1 (en)
CU (1) CU22541A3 (en)
DE (1) DE69430978T2 (en)
DK (1) DK0655507T3 (en)
EG (1) EG20282A (en)
ES (1) ES2177569T3 (en)
GT (1) GT199900088A (en)
ZA (1) ZA948722B (en)

Families Citing this family (43)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5554227A (en) * 1993-11-12 1996-09-10 Societe Nouvelle De Recherches Et D'applications Industrielles D'echangeurs D'ions Applexion Process of manufacturing crystal sugar from an aqueous sugar juice such as cane juice or sugar beet juice
AUPN118095A0 (en) * 1995-02-16 1995-03-09 Csr Limited Improved process for the refining of sugar
IT1275974B1 (en) * 1995-03-27 1997-10-24 Resindion S R L TREATMENT PROCEDURE WITH AN ION EXCHANGE RESIN OF A SUGAR SOLUTION DERIVED FROM BEET
US6096136A (en) * 1996-10-18 2000-08-01 Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Method for producing white sugar
US5759283A (en) * 1996-05-14 1998-06-02 The Western Sugar Company Method for processing sugar beets to produce a purified beet juice product
AU731295B2 (en) * 1996-07-31 2001-03-29 Kumphawapi Sugar Co., Ltd., The Noncentrifugal sugar composition and a process for the preparation of a sugar product
FR2753456B1 (en) * 1996-09-18 1998-12-31 Generale Sucriere Sa PROCESS FOR REGENERATION OF ION EXCHANGE RESINS IN THE DECALCIFICATION PROCESS OF SWEET JUICES
US6051075A (en) * 1996-11-15 2000-04-18 Amalgamated Research, Inc. Process for sugar beet juice clarification
US6037456A (en) * 1998-03-10 2000-03-14 Biosource Technologies, Inc. Process for isolating and purifying viruses, soluble proteins and peptides from plant sources
IT1304373B1 (en) * 1998-05-13 2001-03-15 Eridania S P A PROCEDURE FOR THE PRODUCTION OF COMMERCIAL WHITE SUGAR OPENING FROM MICROFILTRATED OR ULTRAFILTERED BEET CRUDE.
US6159302A (en) * 1999-01-13 2000-12-12 Betzdearborn Inc. Neutral phosphate pre-coagulant composition for clarification in white sugar production
US6146465A (en) * 1999-01-13 2000-11-14 Betzdearborn Inc. Methods for clarifying sugar solutions
AU781362B2 (en) * 1999-04-07 2005-05-19 Ufion (Proprietary) Limited Treatment of sugar juice
IT1311938B1 (en) * 1999-04-21 2002-03-20 Eridania S P A METHOD OF DEPURATION OF CRUDE BEET SAUCE.
EP1204767B1 (en) * 1999-08-19 2007-03-28 Tate & Lyle Sugar Holdings, Inc. Sugar beet membrane filtration process
US6387186B1 (en) 1999-08-19 2002-05-14 Tate & Lyle, Inc. Process for production of purified beet juice for sugar manufacture
US6440222B1 (en) * 2000-07-18 2002-08-27 Tate & Lyle Industries, Limited Sugar beet membrane filtration process
US6406547B1 (en) 2000-07-18 2002-06-18 Tate & Lyle Industries, Limited Sugar beet membrane filtration process
US6174378B1 (en) 1999-08-19 2001-01-16 Tate Life Industries, Limited Process for production of extra low color cane sugar
US6406548B1 (en) 2000-07-18 2002-06-18 Tate & Lyle Industries, Limited Sugar cane membrane filtration process
AU6906400A (en) * 1999-08-19 2001-03-19 Tate And Lyle Industries, Limited Sugar cane membrane filtration process
US6375751B2 (en) 1999-08-19 2002-04-23 Tate & Lyle, Inc. Process for production of purified cane juice for sugar manufacture
US6355110B1 (en) 1999-11-17 2002-03-12 Tate & Lyle Industries, Limited Process for purification of low grade sugar syrups using nanofiltration
DE60224680T2 (en) * 2001-08-24 2009-01-15 Danisco Sugar A/S METHOD FOR PRODUCING WHITE AND BROWN SUGAR BEETS FROM SUGAR BEETS
FR2838751B1 (en) * 2002-04-17 2007-03-09 Applexion Ste Nouvelle De Rech PROCESS AND PLANT FOR MANUFACTURING REFINED SUGAR FROM SUGAR JUICE
PL377399A1 (en) * 2002-11-06 2006-02-06 Danisco Sugar Oy Edible flavor improver, process for its production and use
BRPI0406483B1 (en) * 2003-01-23 2014-04-22 Prayas Goel Method for simultaneous clarification and discoloration of sugarcane juice without the use of any chemicals for any purpose by use of ultrafiltration flat membrane module
US7077953B2 (en) * 2003-09-11 2006-07-18 Harris Group, Inc. Nanofilter system and method of use
KR20060026616A (en) * 2004-09-21 2006-03-24 박상영 Alkalic mineral sugar of rich minerals and production method thereof
US7226511B2 (en) * 2004-10-29 2007-06-05 Board Of Supervisors Of Louisiana State University And Agricultural And Mechanical College Direct production of white sugar from sugarcane juice or sugar beet juice
FR2907687B1 (en) * 2006-10-30 2008-12-26 Applexion PROCESS FOR PURIFYING SIALYLLACTOSE BY CHROMATOGRAPHY
CN100507007C (en) * 2006-11-21 2009-07-01 华南理工大学 Method for producing natural colored sugar
FR2925349A1 (en) * 2007-12-20 2009-06-26 Applexion Separation on resin by multicolumn sequential selective retention to separate an ionic metal derivative e.g. uranium, gold, and zinc, from a leaching solution containing ionic metal derivative, by passing the solution on a fixed resin bed
CN102659855B (en) * 2012-05-16 2014-09-03 成都连接流体分离科技有限公司 Energy-saving environment-friendly sucrose production process
FR2999606B1 (en) * 2012-12-18 2015-09-04 Lesaffre & Cie PROCESS FOR PURIFYING BEET JUICE
TWI599544B (en) * 2013-01-21 2017-09-21 三菱化學股份有限公司 Metal concentration method, metal recovery method, metal concentration apparatus, and metal recovery apparatus
CN103710470B (en) * 2013-12-26 2016-03-23 江苏久吾高科技股份有限公司 A kind of technique of two step method sugaring and device
US9757688B2 (en) 2014-03-07 2017-09-12 Sidel Systems USA Inc. Systems and methods of capturing carbon dioxide and minimizing production of carbon dioxide
CN104004860A (en) * 2014-05-29 2014-08-27 江苏久吾高科技股份有限公司 Production process and device of golden sugar
RU2589789C1 (en) * 2015-01-30 2016-07-10 Федеральное государственное бюджетное образовательное учреждение высшего образования "Воронежский государственный университет инженерных технологий" (ФГБОУ ВО "ВГУИТ") Method of producing brown sugar syrup
WO2018029500A1 (en) * 2016-08-08 2018-02-15 Rhodia Poliamida E Especialidades S.A. New components to clarify sugar cane juice in a process for producing crystal or raw sugar
CN108998578A (en) * 2018-08-22 2018-12-14 柳州味泉食品科技有限公司 A kind of method that cane molasses and zero addition granulated sugar are added in coproduction zero
CN110016525A (en) * 2019-04-10 2019-07-16 中国科学院近代物理研究所 A kind of functional food sugar grass syrup and preparation method thereof

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3799806A (en) * 1972-04-20 1974-03-26 Danske Sukkerfab Process for the purification and clarification of sugar juices,involving ultrafiltration
US4115147A (en) * 1976-04-01 1978-09-19 Mitsui Sugar Co., Ltd. Process for producing nutritive sugar from cane juice
EP0016992A1 (en) * 1979-03-15 1980-10-15 Giuseppe Assalini Process and installation for regenerating ion exchange resins in sugar juice processing
EP0357901A2 (en) * 1988-09-09 1990-03-14 Isi Industria Saccarifera Italiana Agroindustriale S.P.A. Procedure and equipment for differentiated juice defecation in two resin packed ion exchange columns
WO1992008810A1 (en) * 1990-11-09 1992-05-29 Applied Membrane Systems Pty. Ltd. A method and apparatus for fractionation of sugar containing solution
EP0629707A2 (en) * 1993-06-11 1994-12-21 Applexion Process for softening a sugar containing juice such as molasses and the application thereof to a process for the recovery of the sugars contained in this juice
EP0635578A1 (en) * 1993-07-19 1995-01-25 Applexion Process for refining raw sugar, especially brown sugar from the cane sugar industry

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2413844A (en) * 1941-01-31 1947-01-07 Dorr Co Ion exchange treatment of sugar
US3808050A (en) * 1965-07-01 1974-04-30 L Paley Clarification and treatment of sugar juice
GB1350261A (en) * 1970-10-16 1974-04-18 Hitachi Shipbuilding Eng Co Sugar refining process
SE441932B (en) 1981-01-14 1985-11-18 Danske Sukkerfab PROCEDURE FOR PURIFICATION OF SUGAR SOFT PREPARED BY EXTRACTION OF SUGAR BEETS
US5176832A (en) * 1991-10-23 1993-01-05 The Dow Chemical Company Chromatographic separation of sugars using porous gel resins
US5554227A (en) * 1993-11-12 1996-09-10 Societe Nouvelle De Recherches Et D'applications Industrielles D'echangeurs D'ions Applexion Process of manufacturing crystal sugar from an aqueous sugar juice such as cane juice or sugar beet juice
US5468300A (en) * 1994-04-07 1995-11-21 International Food Processing Incorporated Process for producing refined sugar directly from sugarcane

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3799806A (en) * 1972-04-20 1974-03-26 Danske Sukkerfab Process for the purification and clarification of sugar juices,involving ultrafiltration
US4115147A (en) * 1976-04-01 1978-09-19 Mitsui Sugar Co., Ltd. Process for producing nutritive sugar from cane juice
EP0016992A1 (en) * 1979-03-15 1980-10-15 Giuseppe Assalini Process and installation for regenerating ion exchange resins in sugar juice processing
EP0357901A2 (en) * 1988-09-09 1990-03-14 Isi Industria Saccarifera Italiana Agroindustriale S.P.A. Procedure and equipment for differentiated juice defecation in two resin packed ion exchange columns
WO1992008810A1 (en) * 1990-11-09 1992-05-29 Applied Membrane Systems Pty. Ltd. A method and apparatus for fractionation of sugar containing solution
EP0629707A2 (en) * 1993-06-11 1994-12-21 Applexion Process for softening a sugar containing juice such as molasses and the application thereof to a process for the recovery of the sugars contained in this juice
EP0635578A1 (en) * 1993-07-19 1995-01-25 Applexion Process for refining raw sugar, especially brown sugar from the cane sugar industry

Also Published As

Publication number Publication date
DE69430978T2 (en) 2002-11-21
US5902409A (en) 1999-05-11
ES2177569T3 (en) 2002-12-16
CN1105705A (en) 1995-07-26
EP0655507A2 (en) 1995-05-31
AU7776394A (en) 1995-05-18
AU698506B2 (en) 1998-10-29
DE69430978D1 (en) 2002-08-22
EP0655507B1 (en) 2002-07-17
ZA948722B (en) 1995-07-03
CO4370065A1 (en) 1996-10-07
US5554227A (en) 1996-09-10
DK0655507T3 (en) 2002-10-28
CU22541A3 (en) 1999-03-31
EG20282A (en) 1998-07-30
GT199900088A (en) 1999-06-17
ATE220727T1 (en) 2002-08-15
BR9404350A (en) 1995-07-04

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