EP0363861A3 - Process for obtaining impure argon - Google Patents
Process for obtaining impure argon Download PDFInfo
- Publication number
- EP0363861A3 EP0363861A3 EP89118671A EP89118671A EP0363861A3 EP 0363861 A3 EP0363861 A3 EP 0363861A3 EP 89118671 A EP89118671 A EP 89118671A EP 89118671 A EP89118671 A EP 89118671A EP 0363861 A3 EP0363861 A3 EP 0363861A3
- Authority
- EP
- European Patent Office
- Prior art keywords
- impure argon
- obtaining impure
- obtaining
- argon
- impure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04151—Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
- F25J3/04187—Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
- F25J3/04193—Division of the main heat exchange line in consecutive sections having different functions
- F25J3/04206—Division of the main heat exchange line in consecutive sections having different functions including a so-called "auxiliary vaporiser" for vaporising and producing a gaseous product
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
- F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
- F25J3/04096—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of argon or argon enriched stream
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04006—Providing pressurised feed air or process streams within or from the air fractionation unit
- F25J3/04078—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
- F25J3/04103—Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression using solely hydrostatic liquid head
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04248—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
- F25J3/04284—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
- F25J3/0429—Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of feed air, e.g. used as waste or product air or expanded into an auxiliary column
- F25J3/04303—Lachmann expansion, i.e. expanded into oxygen producing or low pressure column
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04406—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
- F25J3/04412—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system in a classical double column flowsheet, i.e. with thermal coupling by a main reboiler-condenser in the bottom of low pressure respectively top of high pressure column
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04642—Recovering noble gases from air
- F25J3/04648—Recovering noble gases from air argon
- F25J3/04654—Producing crude argon in a crude argon column
- F25J3/04666—Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system
- F25J3/04672—Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2250/00—Details related to the use of reboiler-condensers
- F25J2250/30—External or auxiliary boiler-condenser in general, e.g. without a specified fluid or one fluid is not a primary air component or an intermediate fluid
- F25J2250/40—One fluid being air
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2250/00—Details related to the use of reboiler-condensers
- F25J2250/30—External or auxiliary boiler-condenser in general, e.g. without a specified fluid or one fluid is not a primary air component or an intermediate fluid
- F25J2250/58—One fluid being argon or crude argon
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S62/00—Refrigeration
- Y10S62/923—Inert gas
- Y10S62/924—Argon
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S62/00—Refrigeration
- Y10S62/939—Partial feed stream expansion, air
Landscapes
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Mechanical Engineering (AREA)
- Thermal Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Separation By Low-Temperature Treatments (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE3834793 | 1988-10-12 | ||
DE3834793A DE3834793A1 (de) | 1988-10-12 | 1988-10-12 | Verfahren zur gewinnung von rohargon |
Publications (3)
Publication Number | Publication Date |
---|---|
EP0363861A2 EP0363861A2 (de) | 1990-04-18 |
EP0363861A3 true EP0363861A3 (en) | 1990-06-20 |
EP0363861B1 EP0363861B1 (de) | 1992-06-03 |
Family
ID=6364973
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP89118671A Expired - Lifetime EP0363861B1 (de) | 1988-10-12 | 1989-10-07 | Verfahren zur Gewinnung von Rohargon |
Country Status (5)
Country | Link |
---|---|
US (1) | US4932212A (de) |
EP (1) | EP0363861B1 (de) |
CN (1) | CN1052940A (de) |
CA (1) | CA2000595A1 (de) |
DE (2) | DE3834793A1 (de) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4126945A1 (de) * | 1991-08-14 | 1993-02-18 | Linde Ag | Verfahren zur luftzerlegung durch rektifikation |
US5235816A (en) * | 1991-10-10 | 1993-08-17 | Praxair Technology, Inc. | Cryogenic rectification system for producing high purity oxygen |
US5255522A (en) * | 1992-02-13 | 1993-10-26 | Air Products And Chemicals, Inc. | Vaporization of liquid oxygen for increased argon recovery |
US5255524A (en) * | 1992-02-13 | 1993-10-26 | Air Products & Chemicals, Inc. | Dual heat pump cycles for increased argon recovery |
US5245831A (en) * | 1992-02-13 | 1993-09-21 | Air Products And Chemicals, Inc. | Single heat pump cycle for increased argon recovery |
US5365741A (en) * | 1993-05-13 | 1994-11-22 | Praxair Technology, Inc. | Cryogenic rectification system with liquid oxygen boiler |
FR2706195B1 (fr) † | 1993-06-07 | 1995-07-28 | Air Liquide | Procédé et unité de fourniture d'un gaz sous pression à une installation consommatrice d'un constituant de l'air. |
US5366239A (en) * | 1993-09-27 | 1994-11-22 | Trw Inc. | Air bag inflator assembly |
US6269659B1 (en) | 1998-04-21 | 2001-08-07 | L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Method and installation for air distillation with production of argon |
FR2787562B1 (fr) * | 1998-12-22 | 2001-02-09 | Air Liquide | Procede et installation de distillation d'air avec production d'argon |
FR2777641B1 (fr) * | 1998-04-21 | 2000-05-19 | Air Liquide | Procede et installation de distillation d'air avec production d'argon |
US6397632B1 (en) | 2001-07-11 | 2002-06-04 | Praxair Technology, Inc. | Gryogenic rectification method for increased argon production |
DE102007051183A1 (de) * | 2007-10-25 | 2009-04-30 | Linde Aktiengesellschaft | Verfahren zur Tieftemperatur-Luftzerlegung |
FR2943773B1 (fr) * | 2009-03-27 | 2012-07-20 | Air Liquide | Procede et appareil de separation d'air par distillation cryogenique |
CN113959179B (zh) * | 2021-12-22 | 2022-05-03 | 杭州制氧机集团股份有限公司 | 一种用于液氩提纯的装置及方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3643359A1 (de) * | 1986-12-18 | 1988-06-23 | Linde Ag | Verfahren und vorrichtung zur luftzerlegung durch zweistufige rektifikation |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2982107A (en) * | 1957-12-16 | 1961-05-02 | Air Reduction | Separation of the elements of air |
US3181306A (en) * | 1961-01-11 | 1965-05-04 | Air Prod & Chem | Argon separation |
DE1229561B (de) * | 1962-12-21 | 1966-12-01 | Linde Ag | Verfahren und Vorrichtung zum Zerlegen von Luft durch Verfluessigung und Rektifikation mit Hilfe eines Inertgaskreislaufes |
DE1667639A1 (de) * | 1968-03-15 | 1971-07-08 | Messer Griesheim Gmbh | Verfahren zum Gewinnen eines Krypton-Xenon-Gemisches aus Luft |
DE1922956B1 (de) * | 1969-05-06 | 1970-11-26 | Hoechst Ag | Verfahren zur Erzeugung von argonfreiem Sauerstoff durch Rektifikation von Luft |
US4615716A (en) * | 1985-08-27 | 1986-10-07 | Air Products And Chemicals, Inc. | Process for producing ultra high purity oxygen |
US4705548A (en) * | 1986-04-25 | 1987-11-10 | Air Products And Chemicals, Inc. | Liquid products using an air and a nitrogen recycle liquefier |
US4737177A (en) * | 1986-08-01 | 1988-04-12 | Erickson Donald C | Air distillation improvements for high purity oxygen |
EP0269342B1 (de) * | 1986-11-24 | 1991-06-12 | The BOC Group plc | Luftverflüssigung |
US4817394A (en) * | 1988-02-02 | 1989-04-04 | Erickson Donald C | Optimized intermediate height reflux for multipressure air distillation |
-
1988
- 1988-10-12 DE DE3834793A patent/DE3834793A1/de not_active Withdrawn
-
1989
- 1989-09-16 CN CN89107084A patent/CN1052940A/zh not_active Withdrawn
- 1989-10-07 EP EP89118671A patent/EP0363861B1/de not_active Expired - Lifetime
- 1989-10-07 DE DE8989118671T patent/DE58901598D1/de not_active Expired - Fee Related
- 1989-10-11 US US07/421,563 patent/US4932212A/en not_active Expired - Fee Related
- 1989-10-12 CA CA002000595A patent/CA2000595A1/en not_active Abandoned
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3643359A1 (de) * | 1986-12-18 | 1988-06-23 | Linde Ag | Verfahren und vorrichtung zur luftzerlegung durch zweistufige rektifikation |
Also Published As
Publication number | Publication date |
---|---|
EP0363861B1 (de) | 1992-06-03 |
DE3834793A1 (de) | 1990-04-19 |
CA2000595A1 (en) | 1990-04-12 |
DE58901598D1 (de) | 1992-07-09 |
US4932212A (en) | 1990-06-12 |
EP0363861A2 (de) | 1990-04-18 |
CN1052940A (zh) | 1991-07-10 |
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