EP0342044A1 - Metal sheeting - Google Patents
Metal sheeting Download PDFInfo
- Publication number
- EP0342044A1 EP0342044A1 EP89304807A EP89304807A EP0342044A1 EP 0342044 A1 EP0342044 A1 EP 0342044A1 EP 89304807 A EP89304807 A EP 89304807A EP 89304807 A EP89304807 A EP 89304807A EP 0342044 A1 EP0342044 A1 EP 0342044A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- sheet
- formation
- hook
- valley
- formations
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002184 metal Substances 0.000 title claims abstract description 17
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 17
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 56
- 238000005755 formation reaction Methods 0.000 claims abstract description 56
- 239000000463 material Substances 0.000 claims description 6
- 102100034742 Rotatin Human genes 0.000 claims 1
- 101710200213 Rotatin Proteins 0.000 claims 1
- 229910000838 Al alloy Inorganic materials 0.000 description 4
- 239000011324 bead Substances 0.000 description 4
- 238000005253 cladding Methods 0.000 description 2
- 239000007769 metal material Substances 0.000 description 1
- 239000003566 sealing material Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Images
Classifications
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04D—ROOF COVERINGS; SKY-LIGHTS; GUTTERS; ROOF-WORKING TOOLS
- E04D3/00—Roof covering by making use of flat or curved slabs or stiff sheets
- E04D3/36—Connecting; Fastening
- E04D3/361—Connecting; Fastening by specially-profiled marginal portions of the slabs or sheets
- E04D3/362—Connecting; Fastening by specially-profiled marginal portions of the slabs or sheets by locking the edge of one slab or sheet within the profiled marginal portion of the adjacent slab or sheet, e.g. using separate connecting elements
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
- E04F13/00—Coverings or linings, e.g. for walls or ceilings
- E04F13/07—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor
- E04F13/08—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor composed of a plurality of similar covering or lining elements
- E04F13/12—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor composed of a plurality of similar covering or lining elements of metal or with an outer layer of metal or enameled metal
Definitions
- This invention relates to metal sheeting.
- Metal profiled sheets are frequently used as roof panels and for other building cladding purposes. It is well known to provide a metal sheet which is pre-formed with integral ribbing so that it may readily be interlocked at adjoining edges with a similar sheet and which may be fastened to a support without the fastening means being exposed to the environment or being on the visible side of the sheet. These products may include separate fixing clips and involve on site roll forming to close the interlocking seams. All such products are usually referred to as "raised seam cladding". Many examples of such profiled sheets are known and they are frequently roll-formed from an aluminium alloy as well as other metallic materials.
- each sheet has a first upstanding hook formation along one edge and a second upstanding formation along an opposite edge of the sheet with a hook receiving part and a valley in the plane of the sheet through which fasteners can be passed.
- first formation of one sheet hooks on to the hook receiving part of an adjoining sheet and covers the valley and its fasteners.
- the sheets From their outer surfaces the sheets then present a generally flat appearance having spaced apart upstanding ribs with no fasteners visible. These ribs are usually referred to as "raised seam”.
- the sheets when used as roof panels, the sheets need to be fully supported on a pre-prepared flat surface and are not strong enough to span any worthwhile distance between supporting purlins. It is however clearly desirable to provide sheets that can be supported at intervals, as between spaced apart purlins, and it is further desirable that the sheet should be wider so that the spacing between the raised seams is increased. In addition the sheets should be strong enough to support snow loads, wind loads both in pressure and suction and so that, for example, operatives can walk on them.
- a metal sheet having a first upstanding hood formation along one edge and a second, upstanding hook receiving formation and a valley along an opposite edge the arrangement being such that the sheet can be fastened directly to a support without the interposition of separate clips and so that the first formation of one sheet can hook over the second formation of an adjoining sheet and cover its valley characterised by latching means acting between the formations so that after interlocking the sheets said one sheet can be rotated about the hook receiving formation of the other sheet through at least 25° before the formations can be disengaged.
- the rotation preferably occurs without significant distortion of the material of either sheet.
- the latching action ceases to function, and further rotation through at least 10° is required before the formations can be disengaged.
- a roll-formed aluminium alloy sheet 1 has along one side edge 2 a first, hook, formation indicated generally at 3 which is upstanding from the outer surface 4 of the sheet. At its other side edge 5 the sheet has a second, hook receiving, formation indicated generally at 6 and a valley 7. The formations 3 and 6 are separated by a web 8 which is coplanar with the floor 9 of the valley 7. A number of stiffening ribs 8 b may be formed in the sheet.
- the hook formation 3 comprises a sloping part 10, a wall 11 approximately at right angles to the web 8, a flat 12 and downwardly and inwardly projecting parts 13 and 14 constituting a hook having a curved part 15. As shown the outer end of the part 14 is curved to be approximately parallel with the wall 11 and to allow run-out on the edge of the sheet material on roll forming.
- the hook receiving formation comprises a sloping part 16 the upper end 16 b of which is approximately at right angles to the web 8 and is then folded at a part 17 which, together with the wall 16 b defines a hook receiving formation as will be described later.
- the lower end of the folded part 17 is formed as a hollow bead 18 and the rolled material of the sheet is then formed as a platform 19 with a recess 20, a side wall 21 approximately at right angles to the web 8 leading to the valley 7, the floor 9 of which has an upwardly turned part 22 and a lip 23 at the same angle to the web 8 as the sloping part 10.
- the lip 23 allows run out of the edge of the sheet material on roll forming.
- Fig. 3 shows how the hook formation 3 engages over the hook receiving part 6 of an adjoining sheet.
- the same reference numerals have been used except that for the "adjoining" sheet suffixes "a" have been added to each reference numeral.
- the sheet 1 a is already mounted on suitably spaced-apart purlins (not shown) and secured thereto through the valley floor 9 a .
- the fixings used can be conventional and may be arranged to accommodate longitudinal expansion of the sheet 1 a .
- the sheet 1 is then held with its web 8 approximately vertically and its hook formation 3 engaged around the bead 18 a .
- the sheet 1 is then pivoted to the position shown in cross-hatched lines in Fig. 3 and secured to the purlins.
- the sloping part 10 engages with the lip 23 a and the wall 11, the flat 12, the part 13 and the curved part 15 respectively embrace the upper part of the side wall 21 a , the platform 19 a , the part 17 a and the curved part 15 a .
- Sealing material (not shown) may be disposed in the recess 20 a .
- the dimensions of the formations 3 and 6 are such that the upper part of the formation 2 is a "latching fit" over the upper part of the formation 6.
- wind flow across the outer surfaces 4 and 4 a can cause high suction forces to be applied to the webs of the sheets and lift these webs so that their formations 3 and 6 distort and move laterally to disengage the formations 3 and 6.
- the close, "latching fit” engagement between the upper parts of the formations ensures that the wall 11 constitutes latching means for the hook by its close fit against the upper part of the side wall 21 a .
- the edge of the sheet 1 can rotate about the bead 18 a through successive positions indicated at A, B, C and D before reaching the postion E shown as a solid line.
- the wall 11 rides up the side wall 21 a and retains its latching action.
- the corner between the sloping part 10 and the wall 11 rides over the corner between the side wall 21 a and the platform 19 a .
- the chain line 25 represents the angle between the edge of the web 8 and the line of the web 8 a .
- the angle defined is G.
- the chain line 24 represents the angle between the edge of the web 8 and the line of the web 8 a .
- the angle defined is F.
- the precise angle F reached for position E is determined by the detailed dimensions of the upper parts of the formations 3 and 6, the width of the web 8 and the thickness of the sheet. We have found the following criteria achieve good results:-
- Height of the formations 3 and 6 a minimum of 10% (preferably 12.5%) of the total sheet width. This is to achieve a basic stiffness to the whole profile so as to allow it to support the imposed loads.
- Length of the vertical wall 11 between 20% to 30% (preferably 24%) of the height of the rib formation 3 and 6.
- Sheet thickness lies in the range of 0.15% to 0.25% of total formation width.
- the angle G is in the range 25° to 30° (preferably 28°).
- the angle F is in the range 10° to 35° greater than angle G (preferably 30°).
- the basic strength of sheets 500 mm wide can be increased sufficiently to enable the sheets to span purlins with spacings in excess of 2.0 m and still readily support snow and wind loads both in pressure and suction and carry the weight of an operative between the purlins.
- the latching feature of the present invention the disadvantages of increasing the height of the seams can be obviated and increased protection given against suction induced by wind force.
Landscapes
- Engineering & Computer Science (AREA)
- Architecture (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Mechanical Engineering (AREA)
- Roof Covering Using Slabs Or Stiff Sheets (AREA)
- Superconductors And Manufacturing Methods Therefor (AREA)
- Tents Or Canopies (AREA)
- Building Environments (AREA)
- Finishing Walls (AREA)
- Floor Finish (AREA)
- Laminated Bodies (AREA)
- Glass Compositions (AREA)
- Connection Of Plates (AREA)
- Hooks, Suction Cups, And Attachment By Adhesive Means (AREA)
Abstract
Description
- This invention relates to metal sheeting.
- Metal profiled sheets are frequently used as roof panels and for other building cladding purposes. It is well known to provide a metal sheet which is pre-formed with integral ribbing so that it may readily be interlocked at adjoining edges with a similar sheet and which may be fastened to a support without the fastening means being exposed to the environment or being on the visible side of the sheet. These products may include separate fixing clips and involve on site roll forming to close the interlocking seams. All such products are usually referred to as "raised seam cladding". Many examples of such profiled sheets are known and they are frequently roll-formed from an aluminium alloy as well as other metallic materials. Usually each sheet has a first upstanding hook formation along one edge and a second upstanding formation along an opposite edge of the sheet with a hook receiving part and a valley in the plane of the sheet through which fasteners can be passed. When the sheets are interlocked the first formation of one sheet hooks on to the hook receiving part of an adjoining sheet and covers the valley and its fasteners. From their outer surfaces the sheets then present a generally flat appearance having spaced apart upstanding ribs with no fasteners visible. These ribs are usually referred to as "raised seam".
- In general, when used as roof panels, the sheets need to be fully supported on a pre-prepared flat surface and are not strong enough to span any worthwhile distance between supporting purlins. It is however clearly desirable to provide sheets that can be supported at intervals, as between spaced apart purlins, and it is further desirable that the sheet should be wider so that the spacing between the raised seams is increased. In addition the sheets should be strong enough to support snow loads, wind loads both in pressure and suction and so that, for example, operatives can walk on them.
- We have found that there are conflicting factors between, on the one hand, increasing the strength and stiffness of the sheet and, on the other hand, ensuring adequate locking against suction forces under high wind conditions.
- It is therefore an object of the present invention to provide an improved interlocking metal sheet which has good strength characteristics and improved interlocking formations.
- According to the present invention there is provided a metal sheet having a first upstanding hood formation along one edge and a second, upstanding hook receiving formation and a valley along an opposite edge the arrangement being such that the sheet can be fastened directly to a support without the interposition of separate clips and so that the first formation of one sheet can hook over the second formation of an adjoining sheet and cover its valley characterised by latching means acting between the formations so that after interlocking the sheets said one sheet can be rotated about the hook receiving formation of the other sheet through at least 25° before the formations can be disengaged.
- The rotation preferably occurs without significant distortion of the material of either sheet.
- Preferably upon said relative rotation the latching action ceases to function, and further rotation through at least 10° is required before the formations can be disengaged.
- The above and other aspects of the present invention will now be described with reference to the accompanying drawing in which:-
- Fig. 1 is a transverse section through a metal sheet,
- Fig. 2 is a view similar to Fig. 1 showing part of two sheets distorted by suction forces, and
- Fig. 3 is a similar section, to a larger scale, of an interconnection between two metal sheets.
- Referring to Fig. 1 a roll-formed aluminium alloy sheet 1 has along one side edge 2 a first, hook, formation indicated generally at 3 which is upstanding from the
outer surface 4 of the sheet. At itsother side edge 5 the sheet has a second, hook receiving, formation indicated generally at 6 and a valley 7. Theformations 3 and 6 are separated by aweb 8 which is coplanar with the floor 9 of the valley 7. A number of stiffening ribs 8b may be formed in the sheet. - The
hook formation 3 comprises asloping part 10, awall 11 approximately at right angles to theweb 8, a flat 12 and downwardly and inwardly projectingparts curved part 15. As shown the outer end of thepart 14 is curved to be approximately parallel with thewall 11 and to allow run-out on the edge of the sheet material on roll forming. - The hook receiving formation comprises a sloping
part 16 the upper end 16b of which is approximately at right angles to theweb 8 and is then folded at apart 17 which, together with the wall 16b defines a hook receiving formation as will be described later. The lower end of the foldedpart 17 is formed as ahollow bead 18 and the rolled material of the sheet is then formed as a platform 19 with a recess 20, aside wall 21 approximately at right angles to theweb 8 leading to the valley 7, the floor 9 of which has an upwardly turned part 22 and alip 23 at the same angle to theweb 8 as thesloping part 10. Thelip 23 allows run out of the edge of the sheet material on roll forming. - Fig. 3 shows how the
hook formation 3 engages over the hook receiving part 6 of an adjoining sheet. In Fig. 3 the same reference numerals have been used except that for the "adjoining" sheet suffixes "a" have been added to each reference numeral. - It will be assumed that the
sheet 1a is already mounted on suitably spaced-apart purlins (not shown) and secured thereto through the valley floor 9a. The fixings used can be conventional and may be arranged to accommodate longitudinal expansion of thesheet 1a. The sheet 1 is then held with itsweb 8 approximately vertically and itshook formation 3 engaged around thebead 18a. The sheet 1 is then pivoted to the position shown in cross-hatched lines in Fig. 3 and secured to the purlins. In this position the slopingpart 10 engages with thelip 23a and thewall 11, the flat 12, thepart 13 and thecurved part 15 respectively embrace the upper part of theside wall 21a, theplatform 19a, thepart 17a and thecurved part 15a. Sealing material (not shown) may be disposed in therecess 20a. The dimensions of theformations 3 and 6 are such that the upper part of the formation 2 is a "latching fit" over the upper part of the formation 6. - As mentioned above we have found that conflicting requirements exist in increasing the strength of the sheets without at the same time increasing the risk that suction forces under high wind conditions will tear off one of the sheets. When the sheets are mounted on spaced-apart purlins this reduces the number of edge fastenings that can be used.
- Although innately higher strength aluminium alloys than are usually employed can be used this does not, of itself, increase the strength of the sheets sufficiently. Increasing the height of the "raised seams" constituted by the
formations 3 and 6 does significantly increase the strength of the sheets and enables them to be unsupported across suitably spaced purlins. However such a change significantly alters the pattern of distortion of the "other"sheet 1a raised by suction forces on theweb 8a resulting from wind flow across theouter surfaces - As shown in Fig. 2, wind flow across the
outer surfaces formations 3 and 6 distort and move laterally to disengage theformations 3 and 6. - With the present invention the close, "latching fit", engagement between the upper parts of the formations ensures that the
wall 11 constitutes latching means for the hook by its close fit against the upper part of theside wall 21a. As shown in Fig. 3 the edge of the sheet 1 can rotate about thebead 18a through successive positions indicated at A, B, C and D before reaching the postion E shown as a solid line. During the movement A to approximately C thewall 11 rides up theside wall 21a and retains its latching action. At the approximate position C the corner between thesloping part 10 and thewall 11 rides over the corner between theside wall 21a and theplatform 19a. As a result of the "latching fit" referred to above this transition occurs suddenly. In positions D and E the hook still remains engaged since the outer end of thepart 14 remains in engagement with a part of thebead 18a which extends parallel with the upper end of thesloping part 16. Once a sheet has been distorted to the extent represented in position E the strains to which it is subjected are extremely complex and not readily predictable. However it would be expected that position E represents the point at which the edge of the sheet 1 will move laterally and the formations will disengage. - In position C the
chain line 25 represents the angle between the edge of theweb 8 and the line of theweb 8a. The angle defined is G. - In position E the chain line 24 represents the angle between the edge of the
web 8 and the line of theweb 8a. The angle defined is F. The precise angle F reached for position E is determined by the detailed dimensions of the upper parts of theformations 3 and 6, the width of theweb 8 and the thickness of the sheet. We have found the following criteria achieve good results:- - Height of the
formations 3 and 6 a minimum of 10% (preferably 12.5%) of the total sheet width. This is to achieve a basic stiffness to the whole profile so as to allow it to support the imposed loads. - Length of the
vertical wall 11 between 20% to 30% (preferably 24%) of the height of therib formation 3 and 6. - Centre of radius of tip of the hook receiving formation in the
range 10 to 20% (preferably 14%) below the top of the rib formation 6. - Distance of centre of radius of tip of hook receiving formation to
vertical wall 11 when assembled in the range 3.75% to 6.25% (preferably 5%) of the total formation width. - Sheet thickness lies in the range of 0.15% to 0.25% of total formation width.
- The angle G is in the
range 25° to 30° (preferably 28°). - The angle F is in the
range 10° to 35° greater than angle G (preferably 30°). - By using a high strength aluminium alloy such as 3105 or 3004 in standard roofing sheet thicknesses and tempers and by increasing the height of the raised seams the basic strength of sheets 500 mm wide can be increased sufficiently to enable the sheets to span purlins with spacings in excess of 2.0 m and still readily support snow and wind loads both in pressure and suction and carry the weight of an operative between the purlins. By utilising the latching feature of the present invention the disadvantages of increasing the height of the seams can be obviated and increased protection given against suction induced by wind force.
- It will be understood that with the interlocking formations described above then should the sheet 1 be rotated through an angle significantly greater than the angle F (position E) the sheets will again interlock as the
part 14 extends upwardly behind the foldedpart 17. Depending upon the dimensions of these parts this re-engagement is likely to occur with an angle F of about 75°.
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT89304807T ATE73192T1 (en) | 1988-05-13 | 1989-05-11 | METALLIC COVERING ELEMENT. |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB888811397A GB8811397D0 (en) | 1988-05-13 | 1988-05-13 | Metal sheeting |
GB8811397 | 1988-05-13 |
Publications (3)
Publication Number | Publication Date |
---|---|
EP0342044A1 true EP0342044A1 (en) | 1989-11-15 |
EP0342044B1 EP0342044B1 (en) | 1992-03-04 |
EP0342044B2 EP0342044B2 (en) | 1995-01-25 |
Family
ID=10636874
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP89304807A Expired - Lifetime EP0342044B2 (en) | 1988-05-13 | 1989-05-11 | Metal sheeting |
Country Status (7)
Country | Link |
---|---|
EP (1) | EP0342044B2 (en) |
AT (1) | ATE73192T1 (en) |
AU (1) | AU616515B2 (en) |
CA (1) | CA1317433C (en) |
DE (1) | DE68900905D1 (en) |
GB (1) | GB8811397D0 (en) |
PT (1) | PT90550B (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0430619A1 (en) * | 1989-11-25 | 1991-06-05 | Brohome Limited | Improvements relating to roofing panels |
WO1992001129A1 (en) * | 1990-07-06 | 1992-01-23 | Euroclad (South Wales) Limited | Building covering |
FR2789104A1 (en) * | 1998-11-19 | 2000-08-04 | Jean Velut | Method of assembling sheet metal fencing panels has offset hollow ribs on sheet edges clipped by retaining keys |
GB2578659A (en) * | 2018-10-01 | 2020-05-20 | Maple Sunscreening Ltd | Pivotable building-facade panel |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB817238A (en) * | 1956-06-21 | 1959-07-29 | Eric Sigfrid Persson | Improvements in and relating to the securing of surface sheets of roofs and the like |
GB899446A (en) * | 1960-09-13 | 1962-06-20 | Metal Holding Company | An apparatus for joining the edges of metal sheets or strips |
US3394524A (en) * | 1964-11-05 | 1968-07-30 | Edward A.P. Howarth | Joints for sheet metal |
US3511011A (en) * | 1968-12-03 | 1970-05-12 | Reynolds Metals Co | Metal panel and building construction using same |
DE2136584A1 (en) * | 1971-07-22 | 1973-02-08 | Hunter Douglas | PANELS FOR WALL OR CEILING CLADDING |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DK465883D0 (en) * | 1983-04-18 | 1983-10-11 | Wilfried Josef Schenach | roofing |
-
1988
- 1988-05-13 GB GB888811397A patent/GB8811397D0/en active Pending
-
1989
- 1989-05-11 EP EP89304807A patent/EP0342044B2/en not_active Expired - Lifetime
- 1989-05-11 AT AT89304807T patent/ATE73192T1/en active
- 1989-05-11 DE DE8989304807T patent/DE68900905D1/en not_active Expired - Fee Related
- 1989-05-12 AU AU34743/89A patent/AU616515B2/en not_active Ceased
- 1989-05-12 PT PT90550A patent/PT90550B/en not_active IP Right Cessation
- 1989-05-12 CA CA000599559A patent/CA1317433C/en not_active Expired - Fee Related
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB817238A (en) * | 1956-06-21 | 1959-07-29 | Eric Sigfrid Persson | Improvements in and relating to the securing of surface sheets of roofs and the like |
GB899446A (en) * | 1960-09-13 | 1962-06-20 | Metal Holding Company | An apparatus for joining the edges of metal sheets or strips |
US3394524A (en) * | 1964-11-05 | 1968-07-30 | Edward A.P. Howarth | Joints for sheet metal |
US3511011A (en) * | 1968-12-03 | 1970-05-12 | Reynolds Metals Co | Metal panel and building construction using same |
DE2136584A1 (en) * | 1971-07-22 | 1973-02-08 | Hunter Douglas | PANELS FOR WALL OR CEILING CLADDING |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0430619A1 (en) * | 1989-11-25 | 1991-06-05 | Brohome Limited | Improvements relating to roofing panels |
GB2238559B (en) * | 1989-11-25 | 1994-07-27 | Brohome Ltd | Improvements relating to roofing panels |
WO1992001129A1 (en) * | 1990-07-06 | 1992-01-23 | Euroclad (South Wales) Limited | Building covering |
FR2789104A1 (en) * | 1998-11-19 | 2000-08-04 | Jean Velut | Method of assembling sheet metal fencing panels has offset hollow ribs on sheet edges clipped by retaining keys |
GB2578659A (en) * | 2018-10-01 | 2020-05-20 | Maple Sunscreening Ltd | Pivotable building-facade panel |
GB2578659B (en) * | 2018-10-01 | 2021-04-14 | Maple Sunscreening Ltd | Pivotable building-facade panel |
Also Published As
Publication number | Publication date |
---|---|
EP0342044B1 (en) | 1992-03-04 |
AU616515B2 (en) | 1991-10-31 |
DE68900905D1 (en) | 1992-04-09 |
EP0342044B2 (en) | 1995-01-25 |
GB8811397D0 (en) | 1988-06-15 |
ATE73192T1 (en) | 1992-03-15 |
PT90550B (en) | 1997-06-30 |
AU3474389A (en) | 1989-11-16 |
CA1317433C (en) | 1993-05-11 |
PT90550A (en) | 1989-11-30 |
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