EP0156264A2 - Multi-component cutting element using triangular, rectangular and higher order polyhedral-shaped polycrystalline diamond disks - Google Patents

Multi-component cutting element using triangular, rectangular and higher order polyhedral-shaped polycrystalline diamond disks Download PDF

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Publication number
EP0156264A2
EP0156264A2 EP85103002A EP85103002A EP0156264A2 EP 0156264 A2 EP0156264 A2 EP 0156264A2 EP 85103002 A EP85103002 A EP 85103002A EP 85103002 A EP85103002 A EP 85103002A EP 0156264 A2 EP0156264 A2 EP 0156264A2
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EP
European Patent Office
Prior art keywords
diamond
cutting
elements
cutter
pcd
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP85103002A
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German (de)
French (fr)
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EP0156264B1 (en
EP0156264A3 (en
Inventor
Alexander K. Meskin
Leo Merrill
Clifford R. Pay
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Baker Hughes Oilfield Operations LLC
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Norton Christensen Inc
Eastman Christensen Co
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Publication of EP0156264A2 publication Critical patent/EP0156264A2/en
Publication of EP0156264A3 publication Critical patent/EP0156264A3/en
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    • EFIXED CONSTRUCTIONS
    • E21EARTH DRILLING; MINING
    • E21BEARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B10/00Drill bits
    • E21B10/46Drill bits characterised by wear resisting parts, e.g. diamond inserts
    • E21B10/56Button-type inserts
    • E21B10/567Button-type inserts with preformed cutting elements mounted on a distinct support, e.g. polycrystalline inserts
    • E21B10/5676Button-type inserts with preformed cutting elements mounted on a distinct support, e.g. polycrystalline inserts having a cutting face with different segments, e.g. mosaic-type inserts

Definitions

  • the present invention relates to the field of earth boring tools and in particular relates to diamond cutters used on rotating bits.
  • Rotating diamond drill bits were initially manufactured with natural diamonds of industrial quality.
  • the diamonds were square, round or of irregular shape and fully embedded in a metallic bit body, which was generally fabricated by powder metallurgical techniques.
  • the natural diamonds were of a small size ranging from various grades of grit to larger sizes where natural diamonds of 5 or 6 stones per carat were fully embedded in the metal matrix. Because of the small size of the natural diamonds, it was necessary to fully embed the diamonds within the matrix in order to retain them on the bit face under the tremendous pressures and forces to which a drill bit is subjected during rock drilling.
  • PCD polycrystalline diamond
  • prior art diamond synthesizers have developed a polycrystalline sintered diamond element from which the metallic interstitial components, typically cobalt, carbide and the like, have been leached or otherwise removed.
  • leached polycrystalline synthetic diamond is manufactured by the General Electric Company under the trademark GEOSET, for example 2102 GEOSETS, which are formed in the shape of an equilateral prismatic triangle 4 mn, on a side and 2.6 mm deep (3 per carat), and as a 2103 GEOSET shaped in the form of an equilateral triangular prismatic element 6 mm on a side and 3.7 mm deep (1 per carat).
  • the diamond compact slug cutters STRATAPAX
  • the diamond compact slug cutters STRATAPAX
  • the leached triangular prismatic diamonds GEOSETS
  • the cutting rate of a diamond rotating bit is substantially improved by the size of the exposed diamond element available for useful cutting. Therefore, according to the prior art, the increased temperature stability of leached diamond products has been achieved only at the sacrifice of the size of the diamond elements and therefore the amount of diamond available in a bit design for useful cutting action.
  • PCD cutter which is characterised by the temperature stability and characteristics of leached diamond products, and yet has the size available for useful cutting action which is characterised by the larger unleached diamond products.
  • the invention is a diamond cutter for use in a drill bit.
  • the diamond cutter comprises a plurality of thermally stable, prefabricated, synthetic polycrystalline diamond (P CD ) elements.
  • a cutting slug is provided and is characterized by a cutting face.
  • the cutting slug is comprised of a metallic matrix material.
  • the PCD elements are disposed in the cutting slug and retained therein by the matrix material.
  • the matrix material also incorporates a dispersion of diamond grit, at least in that portion of the matrix material adjacent to the cutting face of the cutting slug.
  • the invention is a diamond cutter for use in a rotating drill bit comprising a plurality of leached PCI triangular prismatic and prefabricated elements.
  • a cutting slug is provided and is comprised of a metallic matrix material anc characterized by a cutting face.
  • the plurality of PCD elements are disposed in an array within the cutting slug. Each one o: the PCD elements has at least one surface which is fully exposes on the cutting face of the cutting slug.
  • the matrix materia also incorporates diamond grit in at least that portion of th cutting slug adjacent to the cutting face, and preferabl uniformally throughout the volume of the matrix material.
  • a cutting slug i provided which has a geometry similar to that now only obtained by unleached PCD product but is characterised by the physical temperature and wear properties of leached PCD product.
  • the invention is an enlarged diamond cutter in a rotating bit comprised of a plurality of synthetic polycrystalline diamond elements.
  • the diamond elements are bonded or embedded in a cutting slug formed of matrix material.
  • the matrix material further incorporates diamond grit so that the arrayed PCD elements, each of which have exposed surfaces on the cutting face of the cutting slug, together with the diamond impregnated matrix material therebetween simulates an integral enlarged diamond table.
  • the composite diamond table made from these components in turn is characterised by the physical, temperature and wear characteristics of the smaller components which may be chosen from leached diamond product. Therefore, diamond cutters having the geometric size and design configuration of the traditionally larger unleached diamond compacts can be fabricated using a multiple component array of leached diamond elements according to the invention.
  • the invention is better understood by first considering the embodiment in Figure 1.
  • Diamond cutter 10 is diagrammatically depicted in perspective view as forming the diamond table for an infiltrated integral matrix tooth, also generally denoted by reference numeral 12.
  • Diamond cutter 10 is comprised of a plurality of synthetic PCD elements 14.
  • diamond elements 14 are triangular prismatic elements such as are sold by General Electric Company under the trademarks 2102 GEOSET and 2103 GEOSET. This material is leached diamond material which exerts greater temperature stability and improved wear characteristics than unleached diamond material, such as sold by General Electric Company under the trademark STRATAPAX.
  • Diamond elements 14 are arranged and grouped in an array which collectively comprises diamond cutter 10.
  • diamond elements 14 are equilateral triangular prismatic elements
  • four such elements can be arranged to collectively form a larger equilaterial triangular prismatic shape.
  • 2103 GEOSETs are used as diamond elements 14
  • four such elements can be combined to form an equilateral prismatic triangular shape having a side of 12 mm, and not 6 mm as in the case of a 2103 GEOSET.
  • the number of PCD elements 14 can be increased to construct even larger triangular arrays than that depicted in Figure 1.
  • the triangular array formed by diamond cutter 10 contemplates a compact array of diamond elements 14 wherein each diamond element is in contact with, or in the immediate proximity of, at least one adjacent diamond element 14.
  • each diamond element 14 in the array is bonded to an adjacent diamond by a thin layer of matrix material generally constituted of tungsten carbide and such other elements and compounds as are well known in the art in powder metullurgy for inclusion in such metallic matrices.
  • Matrix material layer 16 is shown in Figure 1 simply as a dimensionless line. It is entirely within the scope of the invention that diamond elements 14 may also be arranged in a spaced-apart relationship with the interstitial spaces completely filled with matrix material 16.
  • PCD elements in the invention in a compact array may actually touch each other or may be separated by a thin layer of matrix material which tends to bond the adjacent elements together.
  • either situation or its equivalent shall be defined as an "immediately proximate* configuration.
  • matrix material 16 as shown in Figure 1 includes diamond grit dispersed at least in that portion of matrix material 16 in the proximity of the cutting face of diamond cutter 10.
  • the mesh or grit size of the natural or synthetic diamond incorporated then matrix material 16 may be of any magnitude or range according to the granularity and wear resistance properties ultimately desired as dictated by well known principles. Generally, a grit diameter in the range of 0.01 inch (0.254mm) to 0.05 inch (1.27mm) suffices. Generally, a diamond grit concentration uniformly dispersed Throught matrix material 16 of 50% to 100% by volume is utilized.
  • a diamond cutter generally denoted by reference numeral 18 is shown as a part of an integral matrix tooth in a matrix body bit.
  • Diamond cutter 18 is comprised of a plurality of triangular prismatic diamond elements 14 disposed within a cutting slug 20.
  • Cutting slug 20 may have a variety of geometric shapes such as semicircular as shown in Figure 2.
  • Diamond elements 14 in the illustrated embodiment of Figure are set within cutting slug 20 in a spaced-apart relationship wherein matrix material 16 is disposed between adjacent diamond elements 14.
  • Diamond elements 14 and matrix material 16 are identical to the like numbered elements described above in connection with the embodiment of Figure 1.
  • the first and second embodiments of Figures 1 and 2 respectively are-formed as part of a infiltrated matrix body bit, only the tooth of which is diagrammatically shown in the figures.
  • Cutting slugs 10 and 20 can be formed by conventional hot press techniques or by infiltration techniques separately from the matrix body bit or may be formed simultaneously through infiltration techniques with the bit body.
  • Triangular prefabricated synthetic diamonds 14 are placed within an appropriately shaped mold in the desired array. Thereafter, a mixture of metallic powder containing the dispersed diamond grit is tamped into the mold and distributed between diamond elements 14.
  • a substantially greater thickness of diamond bearing metallic powder is placed in the mold than the thickness of PCDs 14.
  • This differential thickness is to compensate for the greater compressibility of the powder as compare6 to the relatively noncompressible diamonds 14.
  • the mold is closed by one or more anvils, typically made with the same material as the mold, such as carbon.
  • the filled mold and anvils are then placed within a conventional hot press which typically heats the mold and its contents by an induction heater. Pressure and temperature is then applied to the filled mold, causing the diamond impregnated metallic powder to amalgamate and sinter, ultimately compressing to the shape of cutting slug 10 or 20, as defined by the mold.
  • a pressure of 200 psi and a temperature of 1900°F held for 3 minutes is generally suitable for producing the desired cutting slug.
  • the pressures and temperatures employed are well outside the diamond synthesis or diamond-to-graphite conversion phase regions so that substantially no diamond is created or destroyed in the process.
  • An infiltration technique may also be employed to either separately manufacture cutting-slugs 10 and 20 or to manufacture cutting slugs 10 and 20 integrally with the matrix tooth.
  • an appropriately shaped carbon mold is fabricated and diamonds 14 set therein in the desired array.
  • diamond impregnated metallic matrix powder is filled within the mold and mold then furnaced. The powder is allowed to sinter and infiltrate between diamonds 14 to form the finished cutting sluc.
  • the preformed cutting slug may then be placed within a carbon mold for a matrix bit and fabricated into the bit in a conventional manner.
  • diamond elements 14 may be individually glued into a mold for a matrix body bit in the desired array and position.
  • the matrix body bit is filled first with a layer of diamond impregnated metallic powder and then is continued to be filled with various grades of metallic powder according to conventional matrix bit fabrication techniques.
  • the entire mold is then furnaced so that the cutting slug is simultaneously and integrally formed with the body of the matrix bit.
  • cutting slug 22 is comprised of an array of a plurality of prefabricated, synthetic PCDs 14a and 14b. Again, these diamonds are generally triangular prismatic elements such as 2103 and 2102 GEOSETS and are disposed in a diamond impregnated metallic matrix 16.
  • the array of diamonds shown in the embodiment of Figure 3 is comprised of a first grouping of diamonds 14a and a second grouping 14b.
  • grouping 14a are a plurality of diamonds in spaced apart relationship to form staggered rows of exposed triangular faces in an alternating inverted pattern.
  • Group 14b of diamonds are placed along the circumference of circular cutting slug 22 so that their apical points 26 are directed in a generally radially 5outward direction. As cutting slug 22 wears, the apical points will begin to be exposed and provide for an aggressive cuttinc action along the edge of cutting slug 22.
  • Diamonds in grouping 14a simulate a planar diamond table adapted for cutting salt rock.
  • the two groupings 14a and 14b of diamonds in the embodiment of Figure 3 are only shown hypothetically to illustrate that different arrays which can be employed, and to demonstrate that diamond groupings on a single cutting slug 22 may be varied at different regions within the cutting slug in order to provide edges or faces characterised by a different diamond profile and cutting behavior.
  • Cutting slug 22 is bonded by soldering, brazing and other means as diagrammatically indicated by braze layer 28, shown in greatly exaggerated view in Figure 3. Stud 24 is then press fit, soldered or otherwise fitted into a bit body, typically a steel bit body as is well known to the art. Many such studs are known and could be advantageously combined with the cutting slugs of the present invention.
  • FIG. 4 a fourth embodiment of the invention is illustrated, again shown as a cutting tooth of a matrix bit body.
  • the cutting slug generally denoted by reference numerals 30, is rectangular or square in gross geometric outline and is comprised of an array of prefabricated PCDs 14 which are again generally triangular and prismatic in shape.
  • Diamonds 14 are mounted within cutting slug 30 in a spaced apart relationship so that the interstitial spaces between diamonds 14 are again filled with diamond impregnated matrix material 16.
  • Those diamonds 14 along the periphery of cutting slug 30 are oriented to have one side face 32 exposed and art coplanar with the flat sides of rectangular cutting slug 30.
  • the end faces 34 of diamonds 14 are similarly exposed on the cutting face 36 of cutting slug 30.
  • a rectangular cutting slug 30 such as shown in Figure 4 could be well adapted to a step bit where it could be bonded, soldered or brazed to the corners of the rectangular steps of the bit.
  • a cutting slug is comprised of a plurality of compactly arrayed diamonds 14. More particularly, diamonds 14 are bonded together in groups of six to form a regular hexagonal slug 40. Individual diamond elements 14 are bonded together by a thin matrix layer 16 between each adjacent diamond element 14.
  • cutting slug 40 is fabricated by a conventional hot press or infiltration technique. The completed cutting slug 40 is similarly bonded to a stud 42 by soldering, brazing or other means as diagrammatically depicted by brazing layer 44.
  • the equilateral triangular prismatic diamond elements 14 of the embodiment of Figure 5 can be generalized to form larger structures as shown in plan view in Figure 6.
  • a number of hexagonal arrays, each generally denoted by reference numeral 48, :an be combined to form a larger cutting slug 46.
  • Each hexagonal subarray 48 which forms part of larger array 46 is bonded together by diamond impregnated matrix material 16 as previously described.
  • FIG. 7 Heretofore, the cutting slugs in each embodiment have been described as being built up of triangular prismatic prefabricated synthetic PCDs.
  • the embodiment of Figure 7 generalizes the teachings of the prior embodiments by incorporating prefabricated rectangular prismatic PC D or cubic diamond elements 50. Cubic diamond elements 50 are then combined and bonded together by thin layers of diamond impregnated metallic matrix 16 as before to form a larger cutting slug, generally denoted by reference numeral 52.
  • matrix material 16 may also frame or provide an outer encapsulating rectangular enclosure for the array of diamonds 50 for additional security.
  • the rectangular or square cutting slug 52 of the embodiment of Figure 7 can then be bonded to a stud cutter or integrally formed within a matrix body bit.
  • FIG. 8 wherein a higher order, regular polyhedral shaped diamond element 54 is combined with other like-shaped diamond elements of the same or different orders of polyhedral shapes in a compact or spaced-apart array to form an enlarged cutting slug, generally denoted by reference numeral 56.
  • pentagonal elements 54 are employed in an array wherein some of the elements 54 may contact each other while others remain in spaced-apart relationship.
  • elements 54 are bound to each other and in cutting slug 56 by amalgamation in a diamond impregnated matrix material 16 formed by hot pressing or infiltration.

Abstract

A diamond cutter (18) for use in a drill bit having a geometric size and shape normally characterised by unleached diamond product, such as STRATAPAX diamond cutters, can be fabricated by assembling a plurality of prefabricated leached polycrystalline diamond (PCD) elements (14) in an array in a cutting slug (20). A cutting slug is formed of matrix (16) material which in one embodiment is impregnated with diamond grit. The cutting face of the cutting slug (20) is characterized by exposing at least one surface of each of the PCD elements (14) disposed therein. The diamond elements (14) may be set within the cutting slug (20) either in a compact touching array or in a spaced-apart relationship. More than one type of array may also be employed within a single cutting slug (20). The diamond elements (14) can assume a variety of polyhedral shapes such as triangular prismatic elements, rectangular elements, hexagonal elements and the like. The plurality of diamond elements (14) and the cutting slug (20) are fabricated using hot pressing or infiltration techniques (Figure 2).

Description

    BACKGROUND OF THE INVENTION 1. Field of the Invention
  • The present invention relates to the field of earth boring tools and in particular relates to diamond cutters used on rotating bits.
  • 2. Description of the Prior Art
  • Rotating diamond drill bits were initially manufactured with natural diamonds of industrial quality. The diamonds were square, round or of irregular shape and fully embedded in a metallic bit body, which was generally fabricated by powder metallurgical techniques. Typically, the natural diamonds were of a small size ranging from various grades of grit to larger sizes where natural diamonds of 5 or 6 stones per carat were fully embedded in the metal matrix. Because of the small size of the natural diamonds, it was necessary to fully embed the diamonds within the matrix in order to retain them on the bit face under the tremendous pressures and forces to which a drill bit is subjected during rock drilling.
  • Later, the commercial production of synthetically produced diamond grit and polycrystalline stones became a reality. For example, synthetic diamond was sintered into larger 3isk shapes and were formed as metal compacts, typically forming an amalgam of polycrystalline sintered diamond and cobalt carbide. Such diamond tables are commercially manufactured by General Electric Company. under the trademark STRATAPAX. The diamond tables are bonded, usually within a diamond press to a cobalt carbide slug and sold as an integral slug cutter. The slug cutters are then attached by the drill bit manufacturers to a tungsten carbide slug which is fixed within a drill bit body according to the design of the bit manufacturer.
  • However, such prior art polycrystalline diamond (PCD) compact cutting slugs are characterised by a low temperature stability. Therefore, their direct incorporation into an infiltrated matrix bit body is not practical or possible at this time.
  • In an attempt to manufacture diamond cutting elements of improved hardness, abrasion resistance and temperature stability, prior art diamond synthesizers have developed a polycrystalline sintered diamond element from which the metallic interstitial components, typically cobalt, carbide and the like, have been leached or otherwise removed. Such leached polycrystalline synthetic diamond is manufactured by the General Electric Company under the trademark GEOSET, for example 2102 GEOSETS, which are formed in the shape of an equilateral prismatic triangle 4 mn, on a side and 2.6 mm deep (3 per carat), and as a 2103 GEOSET shaped in the form of an equilateral triangular prismatic element 6 mm on a side and 3.7 mm deep (1 per carat). However, due to present fabrication techniques, in order to leach the synthetic sintered PCD and achieve the improved temperature stability, it is necessary that these diamond elements be limited in size. Therefore, whereas the diamond compact slug cutters, STRATAPAX, may be formed in the shape of circular disks of 3/8" (9.5 mm) to 1/2" (12.7 mm) in diameter, the leached triangular prismatic diamonds, GEOSETS, have maximum dimensions of 4 mm to 6 mm. It is well established that the cutting rate of a diamond rotating bit is substantially improved by the size of the exposed diamond element available for useful cutting. Therefore, according to the prior art, the increased temperature stability of leached diamond products has been achieved only at the sacrifice of the size of the diamond elements and therefore the amount of diamond available in a bit design for useful cutting action.
  • What is needed then is a PCD cutter which is characterised by the temperature stability and characteristics of leached diamond products, and yet has the size available for useful cutting action which is characterised by the larger unleached diamond products.
  • BRIEF SUMMARY OF THE INVENTION
  • The invention is a diamond cutter for use in a drill bit. The diamond cutter comprises a plurality of thermally stable, prefabricated, synthetic polycrystalline diamond (PCD) elements. A cutting slug is provided and is characterized by a cutting face. The cutting slug is comprised of a metallic matrix material. The PCD elements are disposed in the cutting slug and retained therein by the matrix material. The matrix material also incorporates a dispersion of diamond grit, at least in that portion of the matrix material adjacent to the cutting face of the cutting slug. By reason of this combination of elements, an enlarged diamond cutter is provided for mounting in the drill bit.
  • More particularly, the invention is a diamond cutter for use in a rotating drill bit comprising a plurality of leached PCI triangular prismatic and prefabricated elements. A cutting slug is provided and is comprised of a metallic matrix material anc characterized by a cutting face. The plurality of PCD elements are disposed in an array within the cutting slug. Each one o: the PCD elements has at least one surface which is fully exposes on the cutting face of the cutting slug. The matrix materia also incorporates diamond grit in at least that portion of th cutting slug adjacent to the cutting face, and preferabl uniformally throughout the volume of the matrix material. B reason of this combination of elements, a cutting slug i provided which has a geometry similar to that now only obtained by unleached PCD product but is characterised by the physical temperature and wear properties of leached PCD product.
  • These and other embodiments of the invention can best be understood by considering the following figures wherein like elements are referenced by like numerals.
  • BRIEF DESCRIPTION OF THE DRAWINGS
    • Figure I is a diagrammatic perspective view of a first embodiment incorporating a triangular PCD element.
    • Figure 2 is a diagrammatic perspective view of a second embodiment of the invention incorporating a triangular diamond element.
    • Figure 3 is a diagrammatic perspective view of a third embodiment of the invention incorporating a triangular diamond element.
    • Figure 4 is a perspective view of a fourth embodiment of the invention incorporating a triangular diamond element.
    • Figure 5 is a perspective view of a fifth embodiment of the invention incorporating a triangular diamond element.
    • Figure 6 is a plan view of a sixth embodiment of the invention incorporating a triangular diamond element.
    • Figure 7 is a perspective view of a seventh embodimen of the invention incorporating a rectangular diamond element.
    • Figure 8 is a diagrammatic perspective view of th eighth embodiment of the invention incorporating a higher orde polyhedral shaped diamond element.
  • The invention and its various embodiments are better understood by considering the above Figures in light of the following detailed description.
  • DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS
  • The invention is an enlarged diamond cutter in a rotating bit comprised of a plurality of synthetic polycrystalline diamond elements. The diamond elements are bonded or embedded in a cutting slug formed of matrix material. The matrix material further incorporates diamond grit so that the arrayed PCD elements, each of which have exposed surfaces on the cutting face of the cutting slug, together with the diamond impregnated matrix material therebetween simulates an integral enlarged diamond table. However, the composite diamond table made from these components in turn is characterised by the physical, temperature and wear characteristics of the smaller components which may be chosen from leached diamond product. Therefore, diamond cutters having the geometric size and design configuration of the traditionally larger unleached diamond compacts can be fabricated using a multiple component array of leached diamond elements according to the invention. The invention is better understood by first considering the embodiment in Figure 1.
  • Turn now to Figure 1 wherein a diamond cutter, generally denoted by reference numeral 10, is diagrammatically depicted in perspective view as forming the diamond table for an infiltrated integral matrix tooth, also generally denoted by reference numeral 12. Diamond cutter 10 is comprised of a plurality of synthetic PCD elements 14. In the illustrated embodiment, diamond elements 14 are triangular prismatic elements such as are sold by General Electric Company under the trademarks 2102 GEOSET and 2103 GEOSET. This material is leached diamond material which exerts greater temperature stability and improved wear characteristics than unleached diamond material, such as sold by General Electric Company under the trademark STRATAPAX.
  • Diamond elements 14 are arranged and grouped in an array which collectively comprises diamond cutter 10. In the case of Figure 1, wherein diamond elements 14 are equilateral triangular prismatic elements, four such elements can be arranged to collectively form a larger equilaterial triangular prismatic shape. For example, in the case where 2103 GEOSETs are used as diamond elements 14, four such elements can be combined to form an equilateral prismatic triangular shape having a side of 12 mm, and not 6 mm as in the case of a 2103 GEOSET. Clearly, the number of PCD elements 14 can be increased to construct even larger triangular arrays than that depicted in Figure 1.
  • The triangular array formed by diamond cutter 10 contemplates a compact array of diamond elements 14 wherein each diamond element is in contact with, or in the immediate proximity of, at least one adjacent diamond element 14. In the illustrated embodiment, each diamond element 14 in the array is bonded to an adjacent diamond by a thin layer of matrix material generally constituted of tungsten carbide and such other elements and compounds as are well known in the art in powder metullurgy for inclusion in such metallic matrices. Matrix material layer 16 is shown in Figure 1 simply as a dimensionless line. It is entirely within the scope of the invention that diamond elements 14 may also be arranged in a spaced-apart relationship with the interstitial spaces completely filled with matrix material 16. PCD elements in the invention in a compact array may actually touch each other or may be separated by a thin layer of matrix material which tends to bond the adjacent elements together. For the purposes of this specification, either situation or its equivalent shall be defined as an "immediately proximate* configuration.
  • Again, according to the invention, matrix material 16 as shown in Figure 1, for example, includes diamond grit dispersed at least in that portion of matrix material 16 in the proximity of the cutting face of diamond cutter 10. The mesh or grit size of the natural or synthetic diamond incorporated then matrix material 16 may be of any magnitude or range according to the granularity and wear resistance properties ultimately desired as dictated by well known principles. Generally, a grit diameter in the range of 0.01 inch (0.254mm) to 0.05 inch (1.27mm) suffices. Generally, a diamond grit concentration uniformly dispersed Throught matrix material 16 of 50% to 100% by volume is utilized.
  • Turn now to Figure 2, wherein the second embodiment is illustrated in perspective view. Again, a diamond cutter generally denoted by reference numeral 18 is shown as a part of an integral matrix tooth in a matrix body bit. Diamond cutter 18 is comprised of a plurality of triangular prismatic diamond elements 14 disposed within a cutting slug 20. Cutting slug 20 may have a variety of geometric shapes such as semicircular as shown in Figure 2. Diamond elements 14 in the illustrated embodiment of Figure are set within cutting slug 20 in a spaced-apart relationship wherein matrix material 16 is disposed between adjacent diamond elements 14. Diamond elements 14 and matrix material 16 are identical to the like numbered elements described above in connection with the embodiment of Figure 1.
  • The first and second embodiments of Figures 1 and 2 respectively are-formed as part of a infiltrated matrix body bit, only the tooth of which is diagrammatically shown in the figures. Cutting slugs 10 and 20 can be formed by conventional hot press techniques or by infiltration techniques separately from the matrix body bit or may be formed simultaneously through infiltration techniques with the bit body. Consider first a fabrication technique using a hot press method. Triangular prefabricated synthetic diamonds 14 are placed within an appropriately shaped mold in the desired array. Thereafter, a mixture of metallic powder containing the dispersed diamond grit is tamped into the mold and distributed between diamond elements 14. Typically, a substantially greater thickness of diamond bearing metallic powder is placed in the mold than the thickness of PCDs 14. This differential thickness is to compensate for the greater compressibility of the powder as compare6 to the relatively noncompressible diamonds 14. Thereafter, the mold is closed by one or more anvils, typically made with the same material as the mold, such as carbon. The filled mold and anvils are then placed within a conventional hot press which typically heats the mold and its contents by an induction heater. Pressure and temperature is then applied to the filled mold, causing the diamond impregnated metallic powder to amalgamate and sinter, ultimately compressing to the shape of cutting slug 10 or 20, as defined by the mold. For example, a pressure of 200 psi and a temperature of 1900°F held for 3 minutes is generally suitable for producing the desired cutting slug. The pressures and temperatures employed are well outside the diamond synthesis or diamond-to-graphite conversion phase regions so that substantially no diamond is created or destroyed in the process.
  • An infiltration technique may also be employed to either separately manufacture cutting- slugs 10 and 20 or to manufacture cutting slugs 10 and 20 integrally with the matrix tooth. In the case where the cutting slugs are separately manufactured, an appropriately shaped carbon mold is fabricated and diamonds 14 set therein in the desired array. Once again, diamond impregnated metallic matrix powder is filled within the mold and mold then furnaced. The powder is allowed to sinter and infiltrate between diamonds 14 to form the finished cutting sluc. Thereafter, the preformed cutting slug may then be placed within a carbon mold for a matrix bit and fabricated into the bit in a conventional manner. Alternatively, diamond elements 14 may be individually glued into a mold for a matrix body bit in the desired array and position. Thereafter, the matrix body bit is filled first with a layer of diamond impregnated metallic powder and then is continued to be filled with various grades of metallic powder according to conventional matrix bit fabrication techniques. The entire mold is then furnaced so that the cutting slug is simultaneously and integrally formed with the body of the matrix bit.
  • Turn now to Figure 3 wherein a third embodiment is illustrated showing a cutting slug, generally denoted by reference numeral 22, bonded to a steel or tungsten carbide stud 24 also well known to the art. Again, cutting slug 22 is comprised of an array of a plurality of prefabricated, synthetic PCDs 14a and 14b. Again, these diamonds are generally triangular prismatic elements such as 2103 and 2102 GEOSETS and are disposed in a diamond impregnated metallic matrix 16. The array of diamonds shown in the embodiment of Figure 3 is comprised of a first grouping of diamonds 14a and a second grouping 14b. First ; grouping 14a are a plurality of diamonds in spaced apart relationship to form staggered rows of exposed triangular faces in an alternating inverted pattern. Group 14b of diamonds are placed along the circumference of circular cutting slug 22 so that their apical points 26 are directed in a generally radially 5outward direction. As cutting slug 22 wears, the apical points will begin to be exposed and provide for an aggressive cuttinc action along the edge of cutting slug 22. Diamonds in grouping 14a simulate a planar diamond table adapted for cutting salt rock. The two groupings 14a and 14b of diamonds in the embodiment of Figure 3 are only shown hypothetically to illustrate that different arrays which can be employed, and to demonstrate that diamond groupings on a single cutting slug 22 may be varied at different regions within the cutting slug in order to provide edges or faces characterised by a different diamond profile and cutting behavior.
  • Cutting slug 22 is bonded by soldering, brazing and other means as diagrammatically indicated by braze layer 28, shown in greatly exaggerated view in Figure 3. Stud 24 is then press fit, soldered or otherwise fitted into a bit body, typically a steel bit body as is well known to the art. Many such studs are known and could be advantageously combined with the cutting slugs of the present invention.
  • Turn now to Figure 4 wherein a fourth embodiment of the invention is illustrated, again shown as a cutting tooth of a matrix bit body. Here the cutting slug, generally denoted by reference numerals 30, is rectangular or square in gross geometric outline and is comprised of an array of prefabricated PCDs 14 which are again generally triangular and prismatic in shape. Diamonds 14 are mounted within cutting slug 30 in a spaced apart relationship so that the interstitial spaces between diamonds 14 are again filled with diamond impregnated matrix material 16. Those diamonds 14 along the periphery of cutting slug 30 are oriented to have one side face 32 exposed and art coplanar with the flat sides of rectangular cutting slug 30. The end faces 34 of diamonds 14 are similarly exposed on the cutting face 36 of cutting slug 30. Although diagrammatically depicted as incorporated within a matrix tooth 38, a rectangular cutting slug 30 such as shown in Figure 4 could be well adapted to a step bit where it could be bonded, soldered or brazed to the corners of the rectangular steps of the bit.
  • Turn now to Figure 5 wherein yet a fifth embodiment of the invention is diagrammatically illustrated in perspective view. In the fifth embodiment a cutting slug, generally denoted by reference numeral 40, is comprised of a plurality of compactly arrayed diamonds 14. More particularly, diamonds 14 are bonded together in groups of six to form a regular hexagonal slug 40. Individual diamond elements 14 are bonded together by a thin matrix layer 16 between each adjacent diamond element 14. As with the prior embodiments, cutting slug 40 is fabricated by a conventional hot press or infiltration technique. The completed cutting slug 40 is similarly bonded to a stud 42 by soldering, brazing or other means as diagrammatically depicted by brazing layer 44.
  • The equilateral triangular prismatic diamond elements 14 of the embodiment of Figure 5 can be generalized to form larger structures as shown in plan view in Figure 6. Thus, a number of hexagonal arrays, each generally denoted by reference numeral 48, :an be combined to form a larger cutting slug 46. Each hexagonal subarray 48 which forms part of larger array 46 is bonded together by diamond impregnated matrix material 16 as previously described.
  • Turn now to Figure 7. Heretofore, the cutting slugs in each embodiment have been described as being built up of triangular prismatic prefabricated synthetic PCDs. The embodiment of Figure 7 generalizes the teachings of the prior embodiments by incorporating prefabricated rectangular prismatic PCD or cubic diamond elements 50. Cubic diamond elements 50 are then combined and bonded together by thin layers of diamond impregnated metallic matrix 16 as before to form a larger cutting slug, generally denoted by reference numeral 52. In addition to forming the thin interstitial layer, bonding adjacent diamond elements 50, matrix material 16 may also frame or provide an outer encapsulating rectangular enclosure for the array of diamonds 50 for additional security. The rectangular or square cutting slug 52 of the embodiment of Figure 7 can then be bonded to a stud cutter or integrally formed within a matrix body bit.
  • Turn finally to the embodiment of Figure 8 wherein a higher order, regular polyhedral shaped diamond element 54 is combined with other like-shaped diamond elements of the same or different orders of polyhedral shapes in a compact or spaced-apart array to form an enlarged cutting slug, generally denoted by reference numeral 56. In the embodiment of Figure 8, pentagonal elements 54 are employed in an array wherein some of the elements 54 may contact each other while others remain in spaced-apart relationship. Again, elements 54 are bound to each other and in cutting slug 56 by amalgamation in a diamond impregnated matrix material 16 formed by hot pressing or infiltration.
  • Many other modifications or alterations may be made by those having ordinary skill in the art without departing from the spirit and scope of the invention. The illustrated embodiment has only been shown by way of an example and should not be taken as limiting the invention which is defined in the following claims.

Claims (21)

1. A diamond cutter for use in a drill bit comprising:
a plurality of thermally stable, prefabricated synthetic polycrystalline diamond (PCD) elements; and
a cutting slug having a cutting face and comprised of natrix material, said PCD elements disposed in said cutting slug and retained therein by said matrix material,
whereby an enlarged diamond cutter may be provided for nounting in said bit.
2. The cutter of Claim 1 wherein said matrix material incorporating a dispersion of diamond grit at least in that portion of said matrix material adjacent to said cutting face of said cutting slug
3. The cutter of Claim 1 wherein said plurality of PCD elements are each comprised of a prefabricated triangular prismatic diamond element.
4.. The cutter of Claim 3 wherein said plurality of PCD elements are disposed within said cutting slug in a compact array wherein each PCD element is immediately proximate to at least one adjacent PCD element.
5. The cutter of Claim 4 wherein said plurality of PCD elements are arranged and configured to form a triangular prismatic array.
6. The cutter of Claim 4 wherein said plurality of PCD diamond elements are arranged and configured to form a hexagonal prismatic array.
7. The cutter of Claim 6 wherein said hexagonal array is comprised of six triangular prismatic elements forming a subarray.
8. The cutter of Claim 7 wherein a plurality of hexagonal subarrays are arranged and configured to form a larger composite array.
9. The cutter of Claim 3 wherein said plurality of PCD elements are arranged and configured in a spaced-apart relationship, said matrix material being disposed between said spaced-apart PCD elements.
10. The cutter of Claim 9 wherein said cutting slug is formed in the shape of a semicircular disk.
11. The-cutter of Claim 9 wherein said cutting slug is formed in the shape of a full circular disk.
12. The cutter of Claim 9 wherein said cutting slug is formed in a rectangular shape.
13. The cutter of Claim 1 wherein said plurality of PCD elements are rectangular prismatic shape prefabricated synthetic diamond elements arranged and configured within said cutting slug in a compact array wherein each PCD element is immediately proximate to at least one adjacent PCD_element.
14. The cutter of Claim 1 wherein each of said PCD elements is in the shape of a regular polyhedral.
15. The cutter of Claim 1 further comprising a matrix body bit including cutting teeth and wherein said cutting slug comprises a portion of a cutting tooth of said matrix body bit.
16. The cutter of Claim 1 further comprising a bit body, and a plurality of studs disposed in said bit body wherein each said stud has one cutting slug affixed thereto, said cutting face of said slug forming a cutting face of said stud.
17. A diamond cutter for use in a drill bit comprising:
a plurality of leached PCD triangular prismatic and prefabricated elements; and
a cutting slug comprised of metallic matrix material and characterised by a cutting face, said plurality of PCD elements being disposed in an array within said cutting slug, each one of said PCD elements having at least one surface fully exposed on said cutting face of said cutting slug, said matrix material incorporating diamond grit at least in that portion of said cutting slug adjacent to said cutting face,
whereby a cutting slug having a geometry similar to unleached PCD product can be provided and characterised by the physical properties of leached PCD product.
18. The cutter of Claim 17 wherein said diamond grit impregnated in said matrix material is uniformly dispersed throughout said volume of matrix material.
19. The cutter of Claim 18 wherein said plurality of said PCD elements are disposed in said cutting slug in a compact array wherein each PCD element is immediately proximate to at least one adjacent PCD element.
20. The cutter of Claim 18 wherein said plurality of PCD elements are disposed in said array in said cutting slug in a spaced-apart relationship wherein said matrix material is disposed between each adjacent PCD element and no PCD element is immediately proximate to any adjacent element.
21. The cutter of Claim 17 wherein said plurality of PCD elements are arranged and configured in said cutting slug in a plurality of distinguishable arrays.
EP85103002A 1984-03-26 1985-03-15 Multi-component cutting element using triangular, rectangular and higher order polyhedral-shaped polycrystalline diamond disks Expired - Lifetime EP0156264B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US59310284A 1984-03-26 1984-03-26
US593102 1996-01-30

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EP0156264A2 true EP0156264A2 (en) 1985-10-02
EP0156264A3 EP0156264A3 (en) 1986-06-11
EP0156264B1 EP0156264B1 (en) 1990-09-05

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EP (1) EP0156264B1 (en)
JP (1) JPS60226995A (en)
AU (1) AU4021885A (en)
CA (1) CA1241946A (en)
DE (1) DE3579484D1 (en)

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2177144A (en) * 1985-06-18 1987-01-14 De Beers Ind Diamond Cutting tool for a mining machine
GB2181472A (en) * 1985-08-22 1987-04-23 Anderson Strathclyde Plc Cutter tools and tip inserts therefor
GB2190412A (en) * 1986-05-16 1987-11-18 Nl Petroleum Prod Improvements in or relating to rotary drill bits
US4943488A (en) * 1986-10-20 1990-07-24 Norton Company Low pressure bonding of PCD bodies and method for drill bits and the like
US5030276A (en) * 1986-10-20 1991-07-09 Norton Company Low pressure bonding of PCD bodies and method
US5116568A (en) * 1986-10-20 1992-05-26 Norton Company Method for low pressure bonding of PCD bodies
GB2304358A (en) * 1995-08-22 1997-03-19 Smith International Polycrystalline diamond composite cutters
GB2309991A (en) * 1995-08-22 1997-08-13 Smith International A method of making multiple layer polycrystalline diamond composite cutters
US5979578A (en) * 1997-06-05 1999-11-09 Smith International, Inc. Multi-layer, multi-grade multiple cutting surface PDC cutter
GB2353810A (en) * 1999-09-03 2001-03-07 Camco Internat Polycrystalline diamond insert including carbonate as a sintering binder catalyst
GB2429471A (en) * 2005-02-08 2007-02-28 Smith International Thermally stable polycrystalline diamond cutting elements
CN102409981A (en) * 2010-09-25 2012-04-11 中国石油集团渤海石油装备制造有限公司 Assembled diamond compound sheet
US8622154B2 (en) 2008-10-03 2014-01-07 Smith International, Inc. Diamond bonded construction with thermally stable region

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH03202278A (en) * 1989-12-28 1991-09-04 Mitsui Mining & Smelting Co Ltd Composite grindstone
JP2006321006A (en) * 2005-05-19 2006-11-30 Naniwa Kenma Kogyo Kk Manufacturing method of grinding chip body and rotating grinding wheel for peeling coating film

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1522593A (en) * 1919-10-13 1925-01-13 Rowland O Pickin Rotary drilling tool
GB576757A (en) * 1944-04-28 1946-04-17 Nachmann Julius Slutzky Improvements in or relating to diamond tools
DE2013198A1 (en) * 1969-03-19 1971-01-07 Kennametal Inc Diamond products and processes and apparatus for their manufacture
US3902864A (en) * 1970-06-03 1975-09-02 Gen Dynamics Corp Composite material for making cutting and abrading tools
US4190126A (en) * 1976-12-28 1980-02-26 Tokiwa Industrial Co., Ltd. Rotary abrasive drilling bit
US4244432A (en) * 1978-06-08 1981-01-13 Christensen, Inc. Earth-boring drill bits
US4299297A (en) * 1979-06-06 1981-11-10 Lloyd Thomas C Rotary percussion bit
GB2081347A (en) * 1980-08-08 1982-02-17 Christensen Inc Drill tool for deep wells
US4452325A (en) * 1982-09-27 1984-06-05 Conoco Inc. Composite structure for cutting tools
EP0127077A2 (en) * 1983-05-20 1984-12-05 Eastman Christensen Company A rotatable drill bit

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1522593A (en) * 1919-10-13 1925-01-13 Rowland O Pickin Rotary drilling tool
GB576757A (en) * 1944-04-28 1946-04-17 Nachmann Julius Slutzky Improvements in or relating to diamond tools
DE2013198A1 (en) * 1969-03-19 1971-01-07 Kennametal Inc Diamond products and processes and apparatus for their manufacture
US3902864A (en) * 1970-06-03 1975-09-02 Gen Dynamics Corp Composite material for making cutting and abrading tools
US4190126A (en) * 1976-12-28 1980-02-26 Tokiwa Industrial Co., Ltd. Rotary abrasive drilling bit
US4244432A (en) * 1978-06-08 1981-01-13 Christensen, Inc. Earth-boring drill bits
US4299297A (en) * 1979-06-06 1981-11-10 Lloyd Thomas C Rotary percussion bit
GB2081347A (en) * 1980-08-08 1982-02-17 Christensen Inc Drill tool for deep wells
US4452325A (en) * 1982-09-27 1984-06-05 Conoco Inc. Composite structure for cutting tools
EP0127077A2 (en) * 1983-05-20 1984-12-05 Eastman Christensen Company A rotatable drill bit

Cited By (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2177144A (en) * 1985-06-18 1987-01-14 De Beers Ind Diamond Cutting tool for a mining machine
GB2181472A (en) * 1985-08-22 1987-04-23 Anderson Strathclyde Plc Cutter tools and tip inserts therefor
GB2190412A (en) * 1986-05-16 1987-11-18 Nl Petroleum Prod Improvements in or relating to rotary drill bits
EP0246789A2 (en) * 1986-05-16 1987-11-25 Nl Petroleum Products Limited Cutter for a rotary drill bit, rotary drill bit with such a cutter, and method of manufacturing such a cutter
EP0246789A3 (en) * 1986-05-16 1988-12-14 Nl Petroleum Products Limited Cutter for a rotary drill bit, rotary drill bit with such a cutter, and method of manufacturing such a cutter
US4943488A (en) * 1986-10-20 1990-07-24 Norton Company Low pressure bonding of PCD bodies and method for drill bits and the like
US5030276A (en) * 1986-10-20 1991-07-09 Norton Company Low pressure bonding of PCD bodies and method
US5116568A (en) * 1986-10-20 1992-05-26 Norton Company Method for low pressure bonding of PCD bodies
GB2304358A (en) * 1995-08-22 1997-03-19 Smith International Polycrystalline diamond composite cutters
GB2309991A (en) * 1995-08-22 1997-08-13 Smith International A method of making multiple layer polycrystalline diamond composite cutters
GB2309991B (en) * 1995-08-22 1997-10-29 Smith International A method of making multiple diamond layer polycrystalline diamond composite cutters
GB2304358B (en) * 1995-08-22 1997-10-29 Smith International Multiple diamond layer polycrystalline diamond composite cutters and a method for making the same
US5979578A (en) * 1997-06-05 1999-11-09 Smith International, Inc. Multi-layer, multi-grade multiple cutting surface PDC cutter
US6272753B2 (en) 1997-06-05 2001-08-14 Smith International, Inc. Multi-layer, multi-grade multiple cutting surface PDC cutter
GB2353810A (en) * 1999-09-03 2001-03-07 Camco Internat Polycrystalline diamond insert including carbonate as a sintering binder catalyst
US6248447B1 (en) 1999-09-03 2001-06-19 Camco International (Uk) Limited Cutting elements and methods of manufacture thereof
GB2353810B (en) * 1999-09-03 2003-10-08 Camco Internat Cutting elements and methods of manufacture thereof
GB2429471B (en) * 2005-02-08 2009-07-01 Smith International Thermally stable polycrystalline diamond cutting elements and bits incorporating the same
US7533740B2 (en) 2005-02-08 2009-05-19 Smith International Inc. Thermally stable polycrystalline diamond cutting elements and bits incorporating the same
GB2429471A (en) * 2005-02-08 2007-02-28 Smith International Thermally stable polycrystalline diamond cutting elements
US7836981B2 (en) 2005-02-08 2010-11-23 Smith International, Inc. Thermally stable polycrystalline diamond cutting elements and bits incorporating the same
US7946363B2 (en) 2005-02-08 2011-05-24 Smith International, Inc. Thermally stable polycrystalline diamond cutting elements and bits incorporating the same
US8157029B2 (en) 2005-02-08 2012-04-17 Smith International, Inc. Thermally stable polycrystalline diamond cutting elements and bits incorporating the same
US8567534B2 (en) 2005-02-08 2013-10-29 Smith International, Inc. Thermally stable polycrystalline diamond cutting elements and bits incorporating the same
US8622154B2 (en) 2008-10-03 2014-01-07 Smith International, Inc. Diamond bonded construction with thermally stable region
US9404309B2 (en) 2008-10-03 2016-08-02 Smith International, Inc. Diamond bonded construction with thermally stable region
CN102409981A (en) * 2010-09-25 2012-04-11 中国石油集团渤海石油装备制造有限公司 Assembled diamond compound sheet

Also Published As

Publication number Publication date
EP0156264B1 (en) 1990-09-05
CA1241946A (en) 1988-09-13
DE3579484D1 (en) 1990-10-11
AU4021885A (en) 1985-10-03
JPS60226995A (en) 1985-11-12
EP0156264A3 (en) 1986-06-11

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