DK2516948T3 - Fremgangsmåde til overvågning af primær tørring i en frysetørringsproces - Google Patents

Fremgangsmåde til overvågning af primær tørring i en frysetørringsproces

Info

Publication number
DK2516948T3
DK2516948T3 DK10814744.8T DK10814744T DK2516948T3 DK 2516948 T3 DK2516948 T3 DK 2516948T3 DK 10814744 T DK10814744 T DK 10814744T DK 2516948 T3 DK2516948 T3 DK 2516948T3
Authority
DK
Denmark
Prior art keywords
procedure
drying
freezing
monitoring primary
drying process
Prior art date
Application number
DK10814744.8T
Other languages
English (en)
Inventor
Davide Fissore
Roberto Pisano
Antonello A Barresi
Original Assignee
Azbil Telstar Technologies S L
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Azbil Telstar Technologies S L filed Critical Azbil Telstar Technologies S L
Application granted granted Critical
Publication of DK2516948T3 publication Critical patent/DK2516948T3/da

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00—Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • F26B5/06—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing

Landscapes

  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Drying Of Solid Materials (AREA)
DK10814744.8T 2009-12-23 2010-12-22 Fremgangsmåde til overvågning af primær tørring i en frysetørringsproces DK2516948T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ITMO2009A000309A IT1397930B1 (it) 2009-12-23 2009-12-23 Metodo per monitorare l'essiccamento primario di un processo di liofilizzazione.
PCT/IB2010/056011 WO2011077390A2 (en) 2009-12-23 2010-12-22 Method for monitoring primary drying of a freeze-drying process

Publications (1)

Publication Number Publication Date
DK2516948T3 true DK2516948T3 (da) 2014-06-30

Family

ID=42536411

Family Applications (1)

Application Number Title Priority Date Filing Date
DK10814744.8T DK2516948T3 (da) 2009-12-23 2010-12-22 Fremgangsmåde til overvågning af primær tørring i en frysetørringsproces

Country Status (7)

Country Link
US (1) US9170049B2 (da)
EP (1) EP2516948B1 (da)
CN (1) CN102753923B (da)
DK (1) DK2516948T3 (da)
ES (1) ES2471016T3 (da)
IT (1) IT1397930B1 (da)
WO (1) WO2011077390A2 (da)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1397930B1 (it) * 2009-12-23 2013-02-04 Telstar Technologies S L Metodo per monitorare l'essiccamento primario di un processo di liofilizzazione.
JP5827178B2 (ja) * 2012-06-05 2015-12-02 北越紀州製紙株式会社 セルロース多孔質体及びその製造方法
WO2015078898A1 (en) 2013-11-27 2015-06-04 Laboratorio Reig Jofré, S.A. Process for controlling the quality of a freeze-drying process
US20150226617A1 (en) * 2014-02-12 2015-08-13 Millrock Technology, Inc Using in-process heat flow and developing transferable protocols for the monitoring, control and characerization of a freeze drying process
US10266292B2 (en) 2015-01-22 2019-04-23 Neptune Research, Llc Carriers for composite reinforcement systems and methods of use
WO2018194925A1 (en) * 2017-04-21 2018-10-25 Mks Instruments, Inc. End point detection for lyophilization
JP7449235B2 (ja) * 2018-04-10 2024-03-13 アイエムエー ライフ ノース アメリカ インコーポレーテッド 凍結乾燥プロセス及び機器健全性モニタリング
US10914717B2 (en) 2018-05-09 2021-02-09 Mks Instruments, Inc. Method and apparatus for partial pressure detection
US11287185B1 (en) 2020-09-09 2022-03-29 Stay Fresh Technology, LLC Freeze drying with constant-pressure and constant-temperature phases

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2994132A (en) 1956-08-22 1961-08-01 Neumann Karlheinz Freeze drying apparatus
FR1286002A (fr) 1961-01-17 1962-03-02 Usifroid Procédé pour la régulation des opérations de congélation-dessication et installation pour sa mise en oeuvre
US3266169A (en) * 1962-10-31 1966-08-16 Hupp Corp Vacuum freeze drying apparatus
DE1604803A1 (de) * 1962-03-01 1971-01-07 Carlo Barbareschi Verfahren zur kontinuierlichen Absorbierung und Beseitigung von Wasserdampf oder anderen Loesungsmitteln durch Verdampfung oder Sublimation bei niedriger Temperatur unter Vakuum
US4780964A (en) * 1987-11-30 1988-11-01 Fts Systems, Inc. Process and device for determining the end of a primary stage of freeze drying
FR2719656B1 (fr) * 1994-05-03 1996-07-26 Agronomique Inst Nat Rech Procédé et dispositif de contrôle de la lyophilisation sous vide.
WO1996022496A1 (en) * 1995-01-20 1996-07-25 Freezedry Specialties, Inc. Freeze dryer
DE19719398A1 (de) * 1997-05-07 1998-11-12 Amsco Finn Aqua Gmbh Verfahren zur Steuerung eines Gefriertrocknungsprozesses
US6226997B1 (en) 1999-12-07 2001-05-08 Cryo-Cell International, Inc. Method and device for maintaining temperature integrity of cryogenically preserved biological samples
SE0001453D0 (sv) * 2000-04-19 2000-04-19 Astrazeneca Ab Method of monitoring a freeze drying process
WO2002077555A1 (en) 2000-12-06 2002-10-03 Eisai Co., Ltd. System and method for measuring freeze dried cake resistance
NL1020603C2 (nl) * 2002-05-15 2003-11-18 Tno Werkwijze voor het drogen van een product met behulp van een regeneratief adsorbens.
US6971187B1 (en) * 2002-07-18 2005-12-06 University Of Connecticut Automated process control using manometric temperature measurement
US20060208191A1 (en) 2005-01-07 2006-09-21 Kessler William J System for monitoring a drying process
WO2007115965A1 (en) * 2006-04-10 2007-10-18 F. Hoffmann-La Roche Ag Apparatus for monitoring freeze-drying process
ITTO20060270A1 (it) * 2006-04-11 2007-10-12 Torino Politecnico Ottimazione e controllo del processo di liofilizzazione di prodotti farmaceutici
EP1903291A1 (en) * 2006-09-19 2008-03-26 Ima-Telstar S.L. Method and system for controlling a freeze drying process
MX2009003389A (es) * 2006-10-03 2009-04-09 Wyeth Corp Metodos y aparatos de liofilizacion.
ATE532016T1 (de) * 2008-07-23 2011-11-15 Telstar Technologies S L Verfahren zur überwachung der zweiten trocknung in einem gefriertrocknungsverfahren
EP2509873B1 (en) * 2009-12-11 2019-03-20 Wyssmont Company Inc. Apparatus and method for continuous lyophilization
IT1397930B1 (it) * 2009-12-23 2013-02-04 Telstar Technologies S L Metodo per monitorare l'essiccamento primario di un processo di liofilizzazione.
AU2011318436B2 (en) * 2010-09-28 2015-07-02 Baxter Healthcare Sa Optimization of nucleation and crystallization for lyophilization using gap freezing
US8898928B2 (en) * 2012-10-11 2014-12-02 Lam Research Corporation Delamination drying apparatus and method

Also Published As

Publication number Publication date
US20130006546A1 (en) 2013-01-03
ITMO20090309A1 (it) 2011-06-24
EP2516948B1 (en) 2014-03-19
CN102753923B (zh) 2015-03-04
WO2011077390A3 (en) 2011-08-18
IT1397930B1 (it) 2013-02-04
ES2471016T3 (es) 2014-06-25
US9170049B2 (en) 2015-10-27
EP2516948A2 (en) 2012-10-31
CN102753923A (zh) 2012-10-24
WO2011077390A2 (en) 2011-06-30

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