DEP0000415BA - Process for the production of resinous polyesters - Google Patents

Description

Description
for patent registration & tng 4er
Imperial Ohemioal Industries limited, London όψ 1,

■ concerning!
Process for the production of η-boards »harsh-like polyesters.

Prior it from Änglanä Mq. 117/48 of January 2, 1946.

Me $ rfiMäung refers to a manufacturing process for the manufacture of new man-made, tough yrodufcten, the series in particular have a favorable combination of physical and malevolent properties. They made the new gentäaa of the cargo Synthetic resin-like substances are poly-condensation products, which then have the same character as iron lim-aran eroasatic polyphosphates, in which the phosphorus atoms are arranged in the long chain and attached to silicate-forming

and see η at a branched arc · raati

The new substances are insoluble in water, alcohol, ether and paraffin Bsnaol and alcohol have been in sneezing and in door

sofaie & enea asderen Misofoungiaa slide of organic I'liissi which individually besitsea not solved Sigensehaften to these substances, you can sash in verisältnismässig succeed part ron Benssöl UNAE foluol be solved arise zn to concentrated solutions "You solutions of these resins are clear, durcäa-" portant, viscous I114ssi riding »The new resinous products sa melting soft UNAE if they" are still warm enough you own aas sish not by sKiriae hardening specially eh aft en _f leDodi by entspreohewde oheisiselie amendment can be made unsehaielgbar * & hen flüohtiee i iungeiaitt @l be applied "k.'6xmßtL the resins äuroh fuel» aem ₈ Aistreidien or hiss as Bela§asteziaL for metals, glass, Iolg _t Qvami xixä tfLele other substances knmn dung find and Belagaohiehten thus produced have a high Slans and eiiie gate Biegemkel-w ^ wmn you Mr the covering for Set all above fl see τ erwen dei; are s AUt they sen against corrosion * Uieee resins have a ausseior & antlieh gate, egg η high Tlreelra & gBTe xm.ösmj

f arblosj ^ s a »» siHd "extremely geaubex de-r fiinwirlcang toh water and

Acid »You have egg» enough sntflimab & Äeit uca can

be mentioned on about 300, ohaae that one occurs »Be as © resin © of this kind si M aadi not flammable, when they are decomposed in the Flasnae by Warsaw. At ^ insaertemperatEir the Harz have re-appointed shepherds, what iron depends on the fabrics, what depends on their manufacture

Do you know new harsartigon fabrics as Semente for H®besv?

For SLae geferaTsat ₉ usfeer are given due to the fact that Geflss® have selected Harae Hot Bredatiagsintex like S3a.s. You köxmsn aacäi -stam Terlinden το a Met allen ₉ assem, HoIg aaä «r®a s> to ff en ^ erwenäet werdea * ΊΆ® ee Harse aiM

jäindssiit t @ 1 for 3.nl ^ sll.üh @ -J ¹ UlIs to ff β »ie aaä dergl« lareh-liswerlelisen ileßes fabric »In dl« ge mme α. @ τ Srikia & auag manufactured artificial hardy substances "at 2ima®rtemp ®! Ra1 »Br ©!» Erfetalife d © p J2lrwei <± iimgpunktes weröoa fcheraoplasti see 1oita '> Bas ^ fi: tone bigger

iM, ^ aea ^ .gaaöebaftea © rhalteoa, -thermopläB-tl®che η ^ ° e £ ^% & a ^ sw ^ 4 # @ ^^ cr can

en werän _f ta äs Biöh with extraordinarily sharp

lasssa »

8ar «e T © rtrag @ a &%, ok ail iKlisien alleren © TganiseBaen

So joiaä si "ijeis-pielsweie" is all old initaettiell 1 @ jf he puts Htro-Ib ^ «T & ssem conditions such ai.- with

"dsä τ © rs cäiie dejieii suidsreii

1 for

^ i © se ^ Ι ,, Ίο &Ι.ΙΑ'βΒ, Άθΐΐ Stoffs gtssMSBO sit äsn n@u.$si & ü3 ^ tli ~ ch ^ a hargartigffli Fabrics will slide into solution, coverings, di @ taster ^ © rwesä ^ äötää ^ äi # se3? ώ. © β.-θ & kiirs tlioiien hsirsarti ssn fabric «lms @ ffi @ sm With PitFD ^ ell-oloss ₅ sisd little © τ lsi cht sntfl ^ ambsr alB s oliihe aas Sitro ^ aLlulos® a3.3sia _f mi -fe -aasler®! ¥ © rt © a lia ¥ ea äiese aeti®a Muesa cloth ice Siariartigea stoffe ice ias Sjife fisüafflea fratüokliaitein & e effect aiif ca.e Hit rotellulose ₀

(tenäes der SrfLadsiag erJ & lgt the production Ast saeasi art-2io! i®Jä! coffin-like Steffi * tarefc Xoadaasi-g-ia-e- ACT ^ Loxy «

sit «run» * · G ^ feföa? ® ^ f-8a? © 2iatis säi en fSkiifeei & e Hydrosylgrappen lcsna healthy en si saä. and as. sees b ^ iaohliart en coal m to ff atoms lie,

This ioMeseaUon takes place over a period of time by warming a d «g geptajotBs. fesdä ^ uluagent lais oils required properties are in äep üeaKtionsmisohung dergWBäkmäs.al.g weä the -S & aäs dui ^ li Mehrstlin-

O

XOQ MB ISO at $ egxnxi der i * eeig * 4 © Sr / 5fo ^ 190 tos 240 "

It is -BTfJeokm ^ eig _f the Seaktioj3S3aie.chung easy umsrarührea _s * asbes © aäere wsnn de res. Viscosity & ± .dh. to

»3a is s.self ^ gxstäiiälickj, 4ass wsL33rend. JUmJctl ^ a ier üutrl tt ^ & n f ^ eaditigkeii ^ »ifaiisäsrt is» will 4ie O-j -ia eisisr .jsexEfcralen .atmosphere

as * he, StiekatoiX -oäer

The S © ^ E-ä ^ & takes place ^ .vseGkmMs-sif. auoh feel normal, fa i «t it for-teilliaft * a & eh Äi ^ J ^ iga ^ g 4er

eimea STnterdraok: ansuwenaen., um Spiren τοη hydrogen chloride sas 4em Hr ^ ee® ^ i? 0 <liikt sa e & tfem-em » «Ea fäll ©» i®t se swedfem ^ ei ^, wean ^ i e Biltong water si © ff uafeerstütseniie catalysts? like jsetellis without β

1 «do © reu b ^ den ia war sete ge ^ situation quantities, present siisd ₉ camouflage you iJurohfilhrtmg the -S®« fc4ian su support «,

RLe © rmhJite! Oaäejaaati © a kaam da & arela. occur * that ikryloxy | irliC (Splior | -lj (iii! shlori% Biit e

a gemeiflaamea L & euÄgsÄlttel b & ha »delt

* where & ei üe-tstee X & ix & gssäittel aatäi «iiiem ^ h.i0 ^ aeser fabric safaÄi®33lea fabric holds»

Al® Example ^ Ix together * I-8sra.Egs2d.ttel Seiea «awMhnt t & ^ 83Ki2ol _f ÖM.orefo3rm» The Oii

can be for example «in" bia & res AntLn, «» B * dln ·

You new © Mnarti geö öto-ffif «, teicäi ^ geaali®« the srfiiidtmg produced w®rt «m _f can GewüBBehteaf & ll® be riislgt» So ISimem ei β lebeispielawüff «» · i * n SezMioi «eff-golBst un # in the -

te? eih filsjsufi ^ ag voa ether aas to be felled. «A1istÄ.eiide ^ ederecäxlag * of the iia form © Ibbt diokea

^ liffiiei-glEfelii aaffall, kana-weiter aiit Stber g © wa®öhs ^ ®.3ö4 SaaiSL üiÄsr normal oäer ^ eTTlEgentern Urmok gfetroekaet werdea, "eam it is wttoBcäit, #ie Sätar © - sä & l ^ L'eeer Sarse w ^ .tsr au T * rii" nge! M »as lcaaii this da ~

"# rfölgsa _f dass äie liöeiaxigeii äer Saa? ze« lis elag-m orga-I «^ u & gs®: ittel aiii was® © Tfrei» m fetalTiasarTsonat "treated who € © a»

The mms © SjmtliarTse g®iä ^ dier Srilsiäasag laesitBea AOf1ist * _s w © "fe®i felgejaie taä.βäerkeIrrende

If

- f ~ 0 - S '* - 0 0

i.

In di® @ $ r Bormel bejeelshnst B "da © ind" dloialorid yorlying aro ^, tisefoe

I!

oil - P -

Ü * ^f is the ®i © ajatisc] ae _r -EadlkaL, welekes in the «arsrälmten

ollen FerlälEdtaag Tgriandea is «

The eriätot e ^ ä43agtageay «arcaBati eoh ^ ftTerttMung ^ Hydrosylgrappea g-u'boi ^ Hft ate iiicht isanaolb-

iJohXeas tof f atomen gyind ad , Wtoaym. el neu or rere ar © n®, tiaoh © Lerae in ikrem molecule have * Ia the latter i'all can have their hydroxyl groups in the gwei Tersohi @ ä @ iasaa Kexnesa sugegeia eeia _f lneisjpi © leweise la der ÄPsxs ¹ - oöer ® ©% ® # feellt su «iEaiader in a moaoisyklisoben Biifhlajx ^ erMaäuag oäer in the 2s2 * - odex 4J4 'position in desfalls eiaes MplaenjlderiTsteB«, Ss can also

Find"

Ä3a Aryloxyphosphcaryldiahlorid can "for example

Äar # o ^ eiplienoxypho «iüb.oiyiai ehlorld

or ö ^ feofialorplieiioxypii ^ pliaryldidilorid AmtmäSLiig fiiaäeai,

or ^ .lae 'öielisliige 4 © r folsffladea aeajm

, 2 «4 * 6-2» 4 ^ pJypiy

or

2-Ä «tfeyl ~ 4f6« -dtclil © rpfeenoxypfeoephorylÄebloild · Ze but sash üsÄmiges τ © η Isos3i "rem or Te ^ seMe & ea. Stfbsti-

se fertiluages Könaea dnreii B ^ aaadlrmg yvn ΈΆ @ η & 1 ₉

-Tr
Phenol, Os ^ tfeolkLorphenol, pasUaesresol od «r 2 ~ lethyl-4j§ ~ diehlorpheael or J & selKuagea of these substances with feiaperatttrea with more than 1 mol. part
manufactured werdsa, gewänsefateaf alls la © egeiwart eins® talysators, bl® äle ganae amount of äer

verbzmdit is »

Ib t ia_d £ 3LJsayOärii «a ^^

Ale t $ ÄBt ^ ÄPtr ^ -ai ^ i ^ tisclae ^^ i ^ iiäxi.ii ^ ^ laeid © Ä ke! »· A- to ßiclit" tJsmada ^ arten coal

"ToffatsBissa litg" a _f germinate, for example, HydrocMjaoa or Eesorsinol "Uer chl & ± i ecrtea Hjdrochiaoia, or Bifes ^ ea: ^ aphth & lin oäer JEfeyilroSiräiptLejajle ,, for example, 2i lie-feiäii4'iol ^{: ä} äioa ^ cÜp1ieK ^ l or

Isiea following @ a examples «iaä some © embodiments of the

SÜflKämog: Vi »a ^ p @ * h * iaol # lplmrei3. ! © »gen from

244 p6 «aä EjdrocMiiom vsiri on @Laem

Oil bath old ice © 4 »a ^ r laagsaa arbsiteaten ßühy ^ orii data ■>% aasg © sta1rfcet © n älÄsg« fis® warmed »An -difeaer apparatus let eta £ a £ Äte ^ se * fe ^ T Törgeeelea, τβη dsna das - a sin gii 6iüer 0hlO2wasseratoff aböorM ersin-ea ^ liisBi gkiÄt leads «Jer lüäalt tes Eessels wispd against the entrance voa? eiusa Oalciuaiohloridrohree

ö23. Hydrogen oil is heated when the sad

Q ^

ttapfera1ar latsg © d ^ hr is 120 to 13OyS.mad äie ®eiu? € itet lsi this overhaul for a few hours, whereby the actioisaischmög «llmählioh la ®Lm clear Ilüssigjteei *

“Whose- flak oat fet Im? the time increases,

ο ladtoapemt & 3 * v & r & isllmälilioft increased to 205 Ms 215 to © iss gsatigänds TPlüsügseit of äat ^ eent jsa / exfemltani wod & reTi fie JS5gliöK £ eL t is given, ■ ä & ss al «Ba ^ fe ti ο» progresses * Si «Srwtramng will uister-

nmh an ÖesamterMtie-öngeit m> a 2 0 Tals 26 ofcua _t womtsia aie Itafcnd oklanj von IHlorwass only often

bat usä saoMes ti® Yisitöisität äex Bg «fc'tionsmi ~ © cinnsg t> ei 2fO xdislrfc ^ te aas dough t *

«Sssteheaä« xoiie harsajrtlg-e product i? Irä., Soa ^ isg © it still £ LOsst g'ist, ätä sem StefSss aasgegoB®®ß tmd Isei

alsktlhlen gelaseem, Sg then lies in ^ or © 'of an Äsrtsb * i * ö: tigea HörjEee -iror, weleliee ^ te laft * ⁵ O ¹ IaS rujff Ute share Isesitsjt »older he-

f nait- <

mn -to 60 ftmtswtellt · this "substance asked EaltSlieseeigexisefescXteii * Si © 'Säuresab.l des

'betarSgt IS, orä es © Ethält
7th

Sy & roffiW.aoD imfl. Plienoxypliospiiorfläiehlorid «ϊ3 * <* β äes ieehen iiarüartigea Piöäuktss ψίτά cleaned» Is & m es is B @ n * söl on dissolved * & r & _t whereupon äan & the resulting lMsT £ Eg is extracted _{with Itfaer 4} ^ ϊ & τψίττήι weröea

all®
Si φ iiämr * stahl vlrd ¹ TO ^ Ii iigert. In the ü & rig ^ i all-

Β «π®ιϊ1 © atferzit. Per Ixtraktio ^ räetetanö öiähält gisügesäe Mesge to Itliefisoliem Stoif ^ do a swollen FLHS ^ iffcfeitsseiiiiiit amfüekaua ^ t ea, ii "sicäa Yon of daaf- ■ ä% @ r * t" ÄeA®Ei 36hiotot ä * s imr% Täa.ai- ben Itlseys deutliscfcie abo-eitet * Dl © s © r aoali liquid swollen ßiäßkstand

Benaol-Alkohaladeellung brewed in Wswag / uai an UeberselnaBa aa anhydrous

Mis cjlrang,! Haet ms about 1 stand long, Ale .Srgebrdss of this treatment arises sack äem Srooknen turt er Terrizigertem ΰναιϋε. a fearsairtigss product with an öftuyesslil 2 # Sss troekeaegereinigte fi ^ rs owns Tor s # liB3f Behaaäluag lait liatriianäefirTBOiiat Xolgenä ©

7f ^ * hydrogen ^

, J for 41 « ^¥ © rbimäöiig S _fi H Ö - m (* ®} ~ vQ ^ EQ

or 3 I ₀ OP is dear. Eob.le.nst © ffgeiialt # 1 12 "4

Hydrogen content 5 _? 2 $ uisä ä © r Pbo@pb.orgÄtalt

■ Sine Sg ßisiölaktila y® Misöhtmg tob

in s.ime® ϋ, ββββΐ ^ SlmlSeli as in

Pi © Bad temp © ratiar ^! Bsi & he the

tion toegianti * is 130 to 140 fi.wßä 4ie & pÄra «B |! 12 to 15 Stianälea laag ftrtgesetst, «obei, H * T emüeratur increased to 205 to 215 ^ rd» Cmiaeh safeäist

ätar <ÄLgeÄbrt gm fiein *% s yohe ia ^ ehaiditig® is almost colorless mad biMst ssaf metals »© inen hard *

uaä ® © hr üihea ^ elag * Ber JSrwei efe-taiagsisisfcf is its Säuresshl is 14- · Senn äl «© ® ^ substance in the manner given in Example 1 g@rei2d.gi waä siit anhydrous Satriiaimarboimt weä * betrögt his ' MvTe saal Qm Wena @ia dtü ^ c, oieg ^ s Bar sea in "Lsex o ££ ext." Sa Flam® © is heated, 4 © r J & toff does not burn any further but it is removed * 3> ®r Kiäjoststoff ! juicy - fat so. Metal tsuid

• 10 «·
Example 5 _a
Sine

{Sie4 © fuakfe Dß ^ Tirä. l _t 6 © a) «M ^ f & x · © oiiisoii will

heated in a nitrogen stream for 10 hours ₃ with

<Si®! Bü'Gisaperatiit "70m 2 ^ 0 Mb, 135 feel l®efe ^« ns beginning at 23jO ttU £ 30 ^ T iMd 'S®Ä® 4 «P fffcä .g estd gcrt is # 23iese ilrd under ÄtiseehlOss the fluidity

The result is 70h® non-deflaamable resin I) BsItAt iron

mm XöS

it 1st «'something harder than 4ssa» «ti BeL-spisl S preserved bars tgt bass ex © Flamin β iteäa-end® Sigeischaf'teaa. in limit kit χ © ^ aLIuIGQe ₄ , Im tjb2i-g @ ai © t it in his arm "

seimn Ägsasohaftea iimlidi dan produced according to Example 2 © a
Example 4.
Sin ©

rjlüelalo3? id (Sohi ^ Isptmlct € 8 Hi® 70? Siedeprmkt $ 12 ° at

becomes mater iuasohluss τ © η

tesit la ÄH @ r ta bei s $ ± & l 1 ^ seJaiie'biaie-m w «is® arwäüat ₉ where

m £ 29f% is 2 © © increased w. is “you

Required response time is 10 hours _o The raw lat strohfarfem and feeaitet «1 mn Mrweu. öhxmgsptmM; won 115 ° o

1 © 1st target flammable mtu fee ei t st in mixture salt kit bigger flsamea asphyxiating® liigsEBehaftea than that Example 3 produced

BMjB Pi® I ^>

Mo © Ifiimele ^ alsr © Äeüfcraag

mad 4i4 * -li ^ tee% y <ilplieafl n & yd in ter öblieiaem leise rerar-

% eit © t _s w © "b®l Ma Stieltet © f £ @ 1; * Q® about you migeasiiirt * Ieaktienradsehaag ge3» i% - # t ift? 4U Baa Ear * iafl toaaatfaxM g and la tiaaaes Hlmta aor «&& ieh .tlg »Es evgfb-t hard © nztä. tgjx * Rubbers weleh © selected © ielaaet« a S © tall # a jua Slas Moss, These rubbers are located ^ θ iss sasssrordestlich good »I.ideri3-fcands»

disser Sir M H ^; a-gt hmi
6 »

ssii. 4i 4 ⁱ "" Si ^^^ S'0 ^ yÄip ^ @ Ssi ^! 'l "^ iJ ¹ A Aß

us-fer Ktssrnfägaag föH IfS Bort2lfliioriMia © etat _? fcesogen aaf das fesamtgeweht € '®r% aktloBS-ffli © Qhtifig uirtef application

T © rarl © itet _e The £ ® ^^ ®ii l> eginirfe% © i ei ^ ör -Baätesperatar of ISO jf · tJsj but you fi @ AtiJ> n upright SU preservation is't the gate »laaMeaseia des Bert ^ ifMoriifeataiysators required. The feai- «n Sshliss ier ^rM.tsungs^@i1; τοπ IS votes

. Jas ^ r s ^ .e resinous Frodulrfe leads ei-He Sfwei oh-

i & ^.m@T g »0®tey« m let one. Dünas filse of this fabric siM aurdimat pink »Si® teildai Mi? T © imä säla feafteade loading

f.

(Slüäpunkt & $ & ^) becomes ssastei

in l®isfiel 1 amge

ft'bei? äi «B @ äkw will be« Im ia »ilg®

la Ä ^ r gH @ iiää3, «af« iee ti «Im B® £ §ptisl I ₁ Ssb aa far ^ © e® ttürefeselieiaeaäe roi® Mars ®rw © ielit

a © Saures oil YQm-H ₀ Bs is a little harden & L @ das im l ^ ifirplsl 1 "besefart $ t>« a © Warn vM flieset B & fl & t in the cold «Vena ®is is & ek äiesee hard in els # r © ffpas © ^ Jams® heatsrb

it goes away © ehwaeh. iait a leticlitenden llaime-s when m » the? laaiB8 sur-äökgeBöf @a becomes»

Sine Mis elmag t © s teÄSH-Ökloxf] teMr «hl9X- jaat 2 # 4-

^ 3ßh # S5 * 8 ^ Jbyäyöli-sbarenefi Siilor * iiit Sj ^ ochlaiQiL im
the © for each © molecule el »β
eliLllel ^ fctl lyto «-dhia & a TwxfcaaiiÄii is _f -rt3? t.sLS hours em long

HO Täe 2 ^ 0 ° ß £ la 4ä «r ijlHoiiem ffde«

(«, Ts-tehsnaäe Jfer» «re ^ idst%« 1 100 _f ajää wmam ^ fl In the

at.t istüi «« isi * feoj3at fce-

«Ardea ip ^% ®sitst. es · * ®! * »Slnr ^^ ahl fßa 4» I> a © y nad te trioßi: inflammatory

lüg®ns®Mfta »sisd SScmllA düm ^ fflMsi. Igi ^ pitl ten

msd E # s. © rsiü © 2. ilsd 2Q.Sifö3a | © a "3ja & g in 4s in the example 1 say © gaben © η Isise tr« äisrt _f wo "at älü femjasxatar iron 1 ^ 5 m £ 1 ^ ° gesjfeeigfji; ^ 4x4 * Baa ent ^ a ^ eJ & sEäe "Itee tor" firmly cSitig © Sars% ®al * st "um iiötlieii ~ 1i ^ wß iapbe" ad feaftet

You wn. lstallo- 3 er ^ eiehuagspmikt

0
lies h «i S ^^ iiÄi As ^ Hars totsttst & Lm Sgur * 8sSil foa 28,

Is something atrical? all the gemis® example 1

At B-gtel IQ ₈

lift «äcLUiffioielmlare Bisdsmng sroa

322 j

laiig im etx »& SÜ4ik» toffe $ 2! öm # ο

95 aaf 20Ö increased wirä · jÖ®s ®at "at 105 f is awake, atrohfarises wad

4 Sartre

1st 4L'® same «1« - ^ as ^ .eaaii © ® »^ game 3 tar rack tt Maa es- löt mcfe la üialtsäisK Wegbfd aot ^ fcd;

1..000

Syaj ^ eliiaom wlTd eaX eissi 'HetjedÄad ia © iis®m SIa «33 ^« 3? ^ .uer ^ t! S3cs tofjfatwc ^ pM3? ®. PURCHASED ^ WHERE! »®! «La®« Larr MhawmiJllihinis ^ fersehen is * 35ie iard -β ÖtTasdes laiig aaf I ^ θ Μ © MO ^^ geiial * tea imä fisiaa IQ ä-tenägoi lang jwdT JS ₁ O laia IfS ^ T Saeh this U-1 ^ a EntüiolclEiiSig. nreaa 'CibloiaWtseeaCitoii ^f j> j »3? fcisait S © akti..os3S-g @ fäss itod iom.si elae fakuwagiumpe an-

msaä 1 StuM © lai ^ 'iaÄfeer TeüTiBg ^ teÄ iö9x <äc on

© in © fsaperamr tos ItO Is 3SÖ g ^ fcialteän Dm «arises

in the «i3» TF gr-Sesexeä S @ sge lies »fe <$ odbi ± u 4iännea!» raictlftö'ia. Ifarfcloas « M <® SI ^^ salüL äi & 11 aaft 4La Sawsls ^ Tsasstti ^ first lies feel La Beniol" oM ¥ a & sfe ^ a. Alt Ät & m ·

al® Säurtgafel naeit äeai fiosäkasn © -oiai die

⁰ y 11 »gt 1m &I'M ψ *

12 _τ

Mtm Iiaehuag ron 47 g as

wad % _s % g mmkilstallislfrtes colorless 4

• If ia-S ^ a3irefe «^^« ^ & e in example 11 wobsi | @ ä © efc 2 £ 2iKBf olie sjugegeimn HBt the Baätempe-3? Atar usg «fitter S Stuadea laag ^ ui" 190, Ms 19S gelisl1; ea will.

Sa »ent Stehens® lara is a lmr-feer _f saer uM iaeij colorless, Ia ^ i asm && £ lös®a ia gasoline, can be filled with Ither

xater lies ¥ ei 16Q / C ^ & b -dry, traveled har »" possessed

Kohlensi © ff / 45 ^, Hydrogen V / 9 * 2 ^ * Qblor / 22, ^, The -QieoretLashes value © for oil ajJLÖ-F-Ö-iKLI P / oäer 8 ,,, HSl oil amount? Eohlensto ^ f / ^

eis® JPlasehe »welefae adt ^ eIaBr Sührroriictotuag equipped

ar & ohin ©% 5Ö0 © whether Bengol uai 5 € g i> yriäii entered «. Su dem Islaalt der Flascfe becomes one L3 @ o, ng τ on 74s5 I Thsmxf ^ m ^ Tmr ^ Iäioiil © ri4 in 2 ^ 0 oom lensia aHmiiim ^ ler QbtüIi ^ b sagagtfeeia trod daa? I ^ Siuzjäea lang geräiart * dsm ^ « ijB & l 8 © heiiei siftk ®i ^ s gelfej ^ färfete oily layer ifer I ^ jtltter flasdtis Ärd Äaim muter constant hearing 50 Ässlssa lang «f So ^« nfimt, Bi # sweat © olschioht van SexB Ben sols ehiciit as divorced and fiaiit closer together with Wsa & tr ϊρι4 lther g®wasöte.eß κιώ sdilieeslieb. "Ister rergetradfcB0t · urine srfealteBs Hars feesitst fihn-

Ä® the, gfflaäe® example 1 produced Bs feeeitBt | et © di ®iae something cteuüclere! "Arise is a bit stickier

- 15 ~

All examples of torrgesteilte Haafie Bind in Ghlorofoxm and In lensol-AlkQholäriselra & gen (BQ 120? -Q-3, "M"! G ^ m "fit) soluble * Bas optimal ratio of clay Beasol sia. Alcohol changes see 3eäOGk some Ta * öle rersehie-Harie,

Har-ge Icösasn there too-benzene or foluol aafgeläat, us fcoagentilerte iöiraiiea ra. © s * §E "b" a _s te then BEASOL-ABioliolffiis ohwog su of gew & nschtea Xoneistena

who Sen «Bg is eireekm% s £ g _f & i ^ alcohol ent iialt ende solution aiclat strlAg © E &» because toieTäa ^ sii ^ L, φ SSuresahl © AÖ & t will «you 2« gafee "roß alcohol should eiatttiiaiiiea, hewor äie solution further T «ra ^ l) Bitiet is, Se ¹ Sdsee Häfrse äer feesebri © t» en © a kind are sBEtstti iai feiylaeetat, Xtjayl * e *% at «ad 4c * ton lSslidi uHä ergetea dafesL clear solutionea ₉ other I * ostingsmi1; telmischun · - gen _? Me η A-uf loses, of teseiarieiieEen Bar se ^ earweadet ^ can be ^, sLisi Mis Ghtmgea of Butyl * or

water
aromatisöfemEolilsHstGffenj which © low proportions of ali-

phatise & en contain alcohols as they are mr dissolution -v ^ n Iitros © lliiloae.

The Hars © kiimen teduroih uasoimelgbar gssacht value that they are in the way of ¹ ^ m Y «x« ohä, eiL «) iiea metal lots, for example a llelCKylji« rwtrj * values. -Ui it has to you the we-4aeöBierdurc5h the solubility of the · Haraa la orgaaia..c> ien

is reduced ¹ * ffenm, for example, a small amount of such an oxide, for example l-5f black lead,

will -and tspsn the product at 80 to 2OQ eiae, certain long will be given ^ so w§-3% 1iiierd-arch die

According to the Erfisduag aas chlorinated: or bi? ®Äierte-TL Aryl-

Claims (1)

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