DE7743C - Process and production of iodine together with apparatus for the production of iodine and bromine - Google Patents
Process and production of iodine together with apparatus for the production of iodine and bromineInfo
- Publication number
- DE7743C DE7743C DENDAT7743D DE7743DA DE7743C DE 7743 C DE7743 C DE 7743C DE NDAT7743 D DENDAT7743 D DE NDAT7743D DE 7743D A DE7743D A DE 7743DA DE 7743 C DE7743 C DE 7743C
- Authority
- DE
- Germany
- Prior art keywords
- iodine
- production
- bromine
- liquid
- tower
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229910052740 iodine Inorganic materials 0.000 title claims description 10
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 title claims description 10
- 239000011630 iodine Substances 0.000 title claims description 10
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 title claims description 7
- WKBOTKDWSSQWDR-UHFFFAOYSA-N bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 title claims description 7
- 238000000034 method Methods 0.000 title claims description 3
- 238000004519 manufacturing process Methods 0.000 title description 5
- 239000007788 liquid Substances 0.000 claims description 9
- 238000000605 extraction Methods 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 229910052801 chlorine Inorganic materials 0.000 description 5
- 239000000460 chlorine Substances 0.000 description 5
- ZAMOUSCENKQFHK-UHFFFAOYSA-N chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- 238000009835 boiling Methods 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 229910052570 clay Inorganic materials 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/09—Bromine; Hydrogen bromide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/13—Iodine; Hydrogen iodide
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
- Physical Water Treatments (AREA)
Description
1878.1878.
Klasse 12./ 0J Class 12./ 0 J
ROBERT MÜLLER jr. und H. BÖCKEL in SCHÖNEBECK a. d. Elbe. Verfahren zur Gewinnung von Jod nebst Apparat zur Gewinnung von Jod und Brom. ROBERT MÜLLER jr. and H. BÖCKEL in SCHÖNEBECK ad Elbe. Process for the production of iodine together with an apparatus for the production of iodine and bromine.
Patentirt im Deutschen Reiche vom 12. September 1878 ab.Patented in the German Empire on September 12, 1878.
Der Apparat ist ein aus Stein, Thon, Holz oder anderem Material construirter Thurm, dessen Dimensionen sich nach den zu verarbeitenden Flüssigkeitsmengen richten.The apparatus is a tower constructed of stone, clay, wood or other material, the dimensions of which depend on the amount of liquid to be processed.
Der innere Hohlraum ist, ähnlich dem in der Schwefelsäurefabrikation angewendeten Gloverthurm, mit Stücken aus Koks, Stein oder einem anderen geeigneten Material angefüllt, jedoch nur so weit, dafs sowohl im unteren, als auch im oberen Theil des Thurmes je ein freier Raum bleibt. Die genannte Füllung ist zur Oberflächenvertheilung der Flüssigkeit bestimmt.The inner cavity is similar to the Gloverthurm used in sulfuric acid production, filled with pieces of coke, stone, or other suitable material, however only so far that there is a free one in both the lower and the upper part of the tower Space remains. The filling mentioned is intended for surface distribution of the liquid.
In den unteren Theil münden drei Rohre, von denen das eine zur Zuleitung von Chlor, das zweite zur Einleitung von Dampf und das dritte zur Ableitung der ausgenutzten Flüssigkeit dient.Three pipes open into the lower part, one of which is used to supply chlorine, the second for introducing steam and the third for discharging the used liquid serves.
In den oberen Theil des Thurmes mündet ein Rohr, welches die jod- und bromhaltige Flüssigkeit in den Thurm einleitet und in dessen Nähe befindet sich die Oeffnung, durch welche Jod- und Bromdämpfe abziehen und in beliebigen Apparaten condensirt werden.In the upper part of the tower opens a pipe which contains the iodine and bromine Introduces liquid into the tower and in its vicinity is the opening through which Extract iodine and bromine vapors and condense them in any apparatus.
Die zu verarbeitende, siedende Flüssigkeit fliefst durch das Rohr A in den Thurm ein, und, indem sie sich über die Vertheilungsvorrichtungen vertheilt, durch denselben hinab.The boiling liquid to be processed flows through pipe A into the tower, and, being distributed over the distributing devices, descends through it.
Aus den Chlorentwickelungsgefäfsen B, die abwechselnd in Betrieb gesetzt werden, strömt durch das Zuleitungsrohr Chlor in den Thurm ein und tritt mit der herabfliefsenden Flüssigkeit in Verbindung, indem es aus derselben Jod bezw. Brom frei macht.From the chlorine development vessels B, which are alternately put into operation, chlorine flows through the supply pipe into the tower and comes into contact with the downflowing liquid by being respectively iodine from the same. Makes bromine free.
Die so entwickelten Jod- und Bromgase treten auf ihrem Wege bis zum Helm C in Berührung mit immer neuen Flüssigkeitsmengen und werden dadurch vollkommen chlorfrei in den Condensationsapparaten gewonnen. Die sich im unteren Theil des Thurmes sammelnde ausgenutzte Flüssigkeit wird durch aus dem Rohr D einströmenden Dampf von mechanisch aufgelöstem Chlor befreit und fliefst durch F ab.The iodine and bromine gases developed in this way come into contact with ever new amounts of liquid on their way to the helmet C and are thus obtained in the condensation apparatus completely free of chlorine. The used liquid that collects in the lower part of the tower is freed of mechanically dissolved chlorine by steam flowing in from tube D and flows off through F.
Claims (2)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE7743C true DE7743C (en) |
Family
ID=285452
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT7743D Active DE7743C (en) | Process and production of iodine together with apparatus for the production of iodine and bromine |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE7743C (en) |
-
0
- DE DENDAT7743D patent/DE7743C/en active Active
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