DE69900736D1 - Process for the production of detergent tablets - Google Patents

Process for the production of detergent tablets

Info

Publication number
DE69900736D1
DE69900736D1 DE69900736T DE69900736T DE69900736D1 DE 69900736 D1 DE69900736 D1 DE 69900736D1 DE 69900736 T DE69900736 T DE 69900736T DE 69900736 T DE69900736 T DE 69900736T DE 69900736 D1 DE69900736 D1 DE 69900736D1
Authority
DE
Germany
Prior art keywords
phase
production
tablet
detergent tablets
mould
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69900736T
Other languages
German (de)
Other versions
DE69900736T2 (en
Inventor
Patrizio Ricci
Brenda Frances Bennie
Christopher James Binder
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Procter and Gamble Co
Original Assignee
Procter and Gamble Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=26314049&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE69900736(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority claimed from GBGB9815525.2A external-priority patent/GB9815525D0/en
Application filed by Procter and Gamble Co filed Critical Procter and Gamble Co
Publication of DE69900736D1 publication Critical patent/DE69900736D1/en
Application granted granted Critical
Publication of DE69900736T2 publication Critical patent/DE69900736T2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/0065—Solid detergents containing builders
    • C11D17/0073—Tablets
    • C11D17/0086—Laundry tablets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/62—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047—Detergents in the form of bars or tablets
    • C11D17/0065—Solid detergents containing builders
    • C11D17/0073—Tablets
    • C11D17/0078—Multilayered tablets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/126—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in solid compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/1273—Crystalline layered silicates of type NaMeSixO2x+1YH2O
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/221—Mono, di- or trisaccharides or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3707—Polyethers, e.g. polyalkyleneoxides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3769—(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines
    • C11D3/3776—Heterocyclic compounds, e.g. lactam
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/37—Polymers
    • C11D3/3792—Amine oxide containing polymers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38609—Protease or amylase in solid compositions only
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/386—Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38645—Preparations containing enzymes, e.g. protease or amylase containing cellulase
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/40—Dyes ; Pigments
    • C11D3/42—Brightening agents ; Blueing agents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Molecular Biology (AREA)
  • Emergency Medicine (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Sealing With Elastic Sealing Lips (AREA)

Abstract

A multi-phase detergent tablet for use in a washing machine, the tablet comprising: a) a first phase in the form of a shaped body having at least one mould therein; and b) a second phase in the form of a particulate solid compressed within said mould. The multi-phase tablets provide improved dissolution and cleaning characteristics together with excellent tablet integrity and strength.
DE69900736T 1998-07-17 1999-07-07 Process for the production of detergent tablets Expired - Fee Related DE69900736T2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GBGB9815525.2A GB9815525D0 (en) 1998-07-17 1998-07-17 Detergent tablet
GB9911217A GB2339790B (en) 1998-07-17 1999-05-17 Detergent tablet

Publications (2)

Publication Number Publication Date
DE69900736D1 true DE69900736D1 (en) 2002-02-28
DE69900736T2 DE69900736T2 (en) 2002-08-29

Family

ID=26314049

Family Applications (2)

Application Number Title Priority Date Filing Date
DE69900736T Expired - Fee Related DE69900736T2 (en) 1998-07-17 1999-07-07 Process for the production of detergent tablets
DE69908139T Expired - Fee Related DE69908139T2 (en) 1998-07-17 1999-07-07 Detergent tablets and their manufacture

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE69908139T Expired - Fee Related DE69908139T2 (en) 1998-07-17 1999-07-07 Detergent tablets and their manufacture

Country Status (21)

Country Link
EP (2) EP0979864B1 (en)
JP (1) JP2002520478A (en)
CN (1) CN1309693A (en)
AT (2) ATE211503T1 (en)
AU (1) AU762815B2 (en)
BR (1) BR9912834A (en)
CA (1) CA2333388C (en)
DE (2) DE69900736T2 (en)
DK (1) DK0979864T3 (en)
ES (2) ES2168835T3 (en)
FI (1) FI4406U1 (en)
FR (1) FR2782089B1 (en)
IE (1) IES990569A2 (en)
IT (2) ITMI991509A1 (en)
NL (1) NL1012583C1 (en)
PL (1) PL189558B1 (en)
PT (1) PT979864E (en)
RU (1) RU2205869C2 (en)
SK (1) SK642001A3 (en)
TR (1) TR200100094T2 (en)
WO (1) WO2000004123A2 (en)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE29911484U1 (en) * 1998-07-17 2000-02-24 The Procter & Gamble Co., Cincinnati, Ohio Detergent tablet
EP0979865B1 (en) * 1998-07-17 2002-04-10 THE PROCTER & GAMBLE COMPANY Detergent tablet
IES990570A2 (en) * 1998-07-17 2000-03-08 Procter & Gamble Detergent tablet
DE19922578C2 (en) * 1999-05-17 2003-12-24 Benckiser Nv Process for the production of a multilayer tablet, in particular detergent tablet, and product which can be produced thereafter
DE10007608A1 (en) * 2000-02-18 2001-08-30 Henkel Kgaa Particulate laundry and other detergents contain genetically modified protease of subtilisin type and coated particulate alkali percarbonate
DE10010760A1 (en) * 2000-03-04 2001-09-20 Henkel Kgaa Laundry and other detergent tablets containing enzymes, e.g. controlled release tablets, have two or more uncompressed parts containing active substances and packaging system with specified water vapor permeability
US6386462B1 (en) * 2000-07-31 2002-05-14 S. C. Johnson & Son, Inc. Method and apparatus for dispensing liquids in aerosolized form with minimum spillage
DE10243311A1 (en) * 2002-09-18 2004-04-01 Henkel Kgaa Filled tray tablets and process for their manufacture
DE10253479A1 (en) * 2002-11-16 2004-06-03 Henkel Kgaa Filled tray tablets and process for their manufacture II
DE102007059968A1 (en) * 2007-12-11 2009-06-18 Henkel Ag & Co. Kgaa cleaning supplies
RU2510662C2 (en) 2008-03-26 2014-04-10 Новозимс А/С Stabilised liquid enzyme compositions
GB0813460D0 (en) * 2008-07-23 2008-08-27 Reckitt Benckiser Nv Container
WO2010119076A1 (en) * 2009-04-16 2010-10-21 Purac Biochem Bv Cleaning with controlled release of acid
WO2011036153A1 (en) * 2009-09-25 2011-03-31 Novozymes A/S Detergent composition
EP2674475A1 (en) * 2012-06-11 2013-12-18 The Procter & Gamble Company Detergent composition
PL414778A1 (en) 2015-11-13 2017-05-22 Skorut Systemy Solarne Spółka Z Ograniczoną Odpowiedzialnością Method for modification of laminates used in manufacturing of printed circuits
CN109971562A (en) * 2019-04-23 2019-07-05 南京巨鲨显示科技有限公司 Medical manual multienzyme cleaning sheet of a kind of slow-release and preparation method thereof
CN110373287B (en) * 2019-08-15 2021-11-09 广州立白企业集团有限公司 Automatic dish-washing machine cleaning sheet with multiphase structure
CN112646672A (en) * 2019-10-10 2021-04-13 杨子凡 Cleaning block for washing machine tank and preparation method thereof

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2035622A5 (en) * 1969-02-18 1970-12-18 Lion Fat Oil Co Ltd
US4460490A (en) * 1980-12-18 1984-07-17 Jeyes Group Limited Lavatory cleansing blocks
DE3541146A1 (en) * 1985-11-21 1987-05-27 Henkel Kgaa MULTILAYERED DETERGENT TABLETS FOR MACHINE DISHWASHER
GB9015503D0 (en) * 1990-07-13 1990-08-29 Unilever Plc Detergent composition
US5133892A (en) * 1990-10-17 1992-07-28 Lever Brothers Company, Division Of Conopco, Inc. Machine dishwashing detergent tablets
GB9022724D0 (en) * 1990-10-19 1990-12-05 Unilever Plc Detergent compositions
ATE198349T1 (en) * 1995-07-13 2001-01-15 Benckiser Nv DISHWASHER DETERGENT IN THE FORM OF A TABLET
US5837663A (en) * 1996-12-23 1998-11-17 Lever Brothers Company, Division Of Conopco, Inc. Machine dishwashing tablets containing a peracid
GB9711829D0 (en) * 1997-06-06 1997-08-06 Unilever Plc Detergent compositions
GB2327949A (en) * 1997-08-02 1999-02-10 Procter & Gamble Detergent tablet
EP1032642B1 (en) * 1997-11-10 2003-07-02 The Procter & Gamble Company Process for making a detergent tablet
US6440927B1 (en) * 1997-11-10 2002-08-27 The Procter & Gamble Company Multi-layer detergent tablet having both compressed and non-compressed portions
ATE234913T1 (en) * 1997-11-10 2003-04-15 Procter & Gamble METHOD FOR PRODUCING A DETERGENT TABLET
ATE276350T1 (en) * 1997-11-26 2004-10-15 Procter & Gamble METHOD FOR PRODUCING A DETERGENT TABLET
JP2001524590A (en) * 1997-11-26 2001-12-04 ザ、プロクター、エンド、ギャンブル、カンパニー Detergent tablet
DK0960188T3 (en) * 1997-11-26 2002-09-23 Procter & Gamble Washing Procedure
WO1999027069A1 (en) * 1997-11-26 1999-06-03 The Procter & Gamble Company Detergent tablet
DE29911484U1 (en) * 1998-07-17 2000-02-24 The Procter & Gamble Co., Cincinnati, Ohio Detergent tablet
IES990570A2 (en) * 1998-07-17 2000-03-08 Procter & Gamble Detergent tablet
EP0979865B1 (en) * 1998-07-17 2002-04-10 THE PROCTER & GAMBLE COMPANY Detergent tablet
EP1144567B1 (en) * 1998-07-17 2004-09-22 The Procter & Gamble Company Detergent tablet
BR9912838A (en) * 1998-07-17 2001-05-02 Procter & Gamble Detergent tablet

Also Published As

Publication number Publication date
ITMI991568A0 (en) 1999-07-15
CA2333388A1 (en) 2000-01-27
CA2333388C (en) 2005-04-05
EP0979864B1 (en) 2002-01-02
IES990569A2 (en) 2000-07-12
CN1309693A (en) 2001-08-22
ES2194802T3 (en) 2003-12-01
FIU990320U0 (en) 1999-07-16
PL189558B1 (en) 2005-08-31
NL1012583A1 (en) 2000-01-19
FR2782089A1 (en) 2000-02-11
EP0979864A1 (en) 2000-02-16
AU762815B2 (en) 2003-07-03
ATE211503T1 (en) 2002-01-15
ITMI991509A0 (en) 1999-07-09
ATE241004T1 (en) 2003-06-15
RU2205869C2 (en) 2003-06-10
ITMI991509A1 (en) 1999-12-18
SK642001A3 (en) 2001-06-11
WO2000004123A3 (en) 2000-04-13
PT979864E (en) 2002-06-28
FI4406U1 (en) 2000-05-18
DE69908139T2 (en) 2004-04-08
ITMI991568A1 (en) 2001-01-15
AU4964299A (en) 2000-02-07
DK0979864T3 (en) 2002-04-22
EP1097191A2 (en) 2001-05-09
PL345972A1 (en) 2002-01-14
TR200100094T2 (en) 2001-05-21
ES2168835T3 (en) 2002-06-16
BR9912834A (en) 2001-05-02
NL1012583C1 (en) 2000-01-25
FR2782089B1 (en) 2004-11-05
JP2002520478A (en) 2002-07-09
WO2000004123A2 (en) 2000-01-27
DE69900736T2 (en) 2002-08-29
DE69908139D1 (en) 2003-06-26

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Legal Events

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8365 Fully valid after opposition proceedings
8339 Ceased/non-payment of the annual fee