DE69104153T2 - Process for the continuous production of reaction products. - Google Patents

Process for the continuous production of reaction products.

Info

Publication number
DE69104153T2
DE69104153T2 DE69104153T DE69104153T DE69104153T2 DE 69104153 T2 DE69104153 T2 DE 69104153T2 DE 69104153 T DE69104153 T DE 69104153T DE 69104153 T DE69104153 T DE 69104153T DE 69104153 T2 DE69104153 T2 DE 69104153T2
Authority
DE
Germany
Prior art keywords
reactor system
reaction products
products
compartment
continuous production
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69104153T
Other languages
German (de)
Other versions
DE69104153D1 (en
Inventor
Robert P Shirtum
David D Mccoy
Walter L Wernli
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Chemical Co
Original Assignee
Dow Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Chemical Co filed Critical Dow Chemical Co
Application granted granted Critical
Publication of DE69104153D1 publication Critical patent/DE69104153D1/en
Publication of DE69104153T2 publication Critical patent/DE69104153T2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/242—Tubular reactors in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1862—Stationary reactors having moving elements inside placed in series
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058—Temperature measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00067—Liquid level measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00083—Coils
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00139—Controlling the temperature using electromagnetic heating
    • B01J2219/00146—Infrared radiation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/182—Details relating to the spatial orientation of the reactor horizontal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/185—Details relating to the spatial orientation of the reactor vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Epoxy Compounds (AREA)
  • Epoxy Resins (AREA)
  • Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)

Abstract

A continuous reactor system and process for employing such a system. Embodiments of the reactor system include a horizontal (134) or vertical (312) reactor system having a cylindrical multi-compartment vessel, the compartments intercommunicating with each other, the vessel including means (156,410) for removing vapor with reaction product or by-products and means (176,318) for removing liquid effluent with reaction products or by-products and means (158,320) for flowing reactants and catalyst into each compartment and, optionally, agitators (178,370) in each compartment. The present process and reactor system may be employed for producing reaction products, for example, liquid epoxy resins. <IMAGE>
DE69104153T 1990-07-20 1991-07-16 Process for the continuous production of reaction products. Expired - Fee Related DE69104153T2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US55586390A 1990-07-20 1990-07-20
US64387791A 1991-01-18 1991-01-18

Publications (2)

Publication Number Publication Date
DE69104153D1 DE69104153D1 (en) 1994-10-27
DE69104153T2 true DE69104153T2 (en) 1995-01-19

Family

ID=27071000

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69104153T Expired - Fee Related DE69104153T2 (en) 1990-07-20 1991-07-16 Process for the continuous production of reaction products.

Country Status (12)

Country Link
EP (1) EP0467278B1 (en)
JP (1) JP3362052B2 (en)
KR (1) KR920002218A (en)
AT (1) ATE111769T1 (en)
AU (1) AU649052B2 (en)
BR (1) BR9103138A (en)
CA (1) CA2047417A1 (en)
DE (1) DE69104153T2 (en)
DK (1) DK0467278T3 (en)
ES (1) ES2061128T3 (en)
MX (1) MX9100296A (en)
PT (1) PT98384A (en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SG106098A1 (en) * 2001-09-28 2004-09-30 Dainippon Ink & Chemicals Process for preparing epoxy resin
KR20100063029A (en) * 2007-08-23 2010-06-10 다우 글로벌 테크놀로지스 인크. Brine purification
CN102753597B (en) * 2009-12-16 2014-12-17 陶氏环球技术有限责任公司 Production of epoxy resins using improved ion exchange resin catalysts
KR101092337B1 (en) * 2011-07-20 2011-12-09 (주) 라미나 Lithium battery cathode materials for manufacturing an all-in-one type of continuous reactor, and it determines the separation device that includes
GB201810380D0 (en) * 2018-06-25 2018-08-08 Rosehill Polymers Group Ltd Continuous reaction system,vessel and method
KR102267818B1 (en) * 2018-12-12 2021-06-21 주식회사 포스코 Overflow continuous reactor
CN113024797B (en) * 2021-04-27 2023-04-25 宁夏博远橡胶有限公司 Glue solution separating device for production of chloroether rubber
CN114452905B (en) * 2022-03-09 2023-01-31 技源生物制品(徐州)有限公司 Liquid raw material conveying device

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1091568B (en) * 1957-08-02 1960-10-27 Bergwerksgesellschaft Hibernia Method and device for the continuous implementation of reactions between gases and liquids
US3129232A (en) * 1961-08-08 1964-04-14 Shell Oil Co Process for condensing epoxyalkyl halides with hydroxyl group-containing compounds
BE634031A (en) * 1962-06-23
CA1293837C (en) * 1986-10-14 1991-12-31 Ha Q. Pham Preparation of epoxy resins
FR2628418B1 (en) * 1988-03-08 1991-01-04 Inst Francais Du Petrole PROCESS FOR THE PREPARATION OF A TERTIARY ALKYL ETHER BY REACTIVE DISTILLATION

Also Published As

Publication number Publication date
EP0467278A1 (en) 1992-01-22
AU649052B2 (en) 1994-05-12
DK0467278T3 (en) 1995-02-20
EP0467278B1 (en) 1994-09-21
JP3362052B2 (en) 2003-01-07
PT98384A (en) 1994-01-31
ATE111769T1 (en) 1994-10-15
AU8119691A (en) 1992-01-23
BR9103138A (en) 1992-05-05
JPH04227052A (en) 1992-08-17
CA2047417A1 (en) 1992-01-21
ES2061128T3 (en) 1994-12-01
MX9100296A (en) 1992-02-28
KR920002218A (en) 1992-02-28
DE69104153D1 (en) 1994-10-27

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee