DE59410076D1 - METHOD FOR PRODUCING CAPROLACTAM - Google Patents

METHOD FOR PRODUCING CAPROLACTAM

Info

Publication number
DE59410076D1
DE59410076D1 DE59410076T DE59410076T DE59410076D1 DE 59410076 D1 DE59410076 D1 DE 59410076D1 DE 59410076 T DE59410076 T DE 59410076T DE 59410076 T DE59410076 T DE 59410076T DE 59410076 D1 DE59410076 D1 DE 59410076D1
Authority
DE
Germany
Prior art keywords
pct
date
sec
producing caprolactam
pub
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE59410076T
Other languages
German (de)
Inventor
Eberhard Fuchs
Tom Witzel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to DE59410076T priority Critical patent/DE59410076D1/en
Application granted granted Critical
Publication of DE59410076D1 publication Critical patent/DE59410076D1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles

Landscapes

  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Hydrogenated Pyridines (AREA)
  • Cable Accessories (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Cephalosporin Compounds (AREA)
  • Polyamides (AREA)
  • Mounting Of Bearings Or Others (AREA)
  • Peptides Or Proteins (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
  • Audible-Bandwidth Dynamoelectric Transducers Other Than Pickups (AREA)

Abstract

PCT No. PCT/EP94/03782 Sec. 371 Date May 16, 1996 Sec. 102(e) Date May 16, 1996 PCT Filed Nov. 15, 1994 PCT Pub. No. WO95/14665 PCT Pub. Date Jun. 1, 1995Cyclic lactams are prepared by reacting amino carbonitriles with water in liquid phase in a fixed bed reactor in the presence of heterogeneous catalysts which have no soluble constituents under the reaction conditions.
DE59410076T 1993-11-20 1994-11-15 METHOD FOR PRODUCING CAPROLACTAM Expired - Lifetime DE59410076D1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DE59410076T DE59410076D1 (en) 1993-11-20 1994-11-15 METHOD FOR PRODUCING CAPROLACTAM

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE4339648A DE4339648A1 (en) 1993-11-20 1993-11-20 Process for the production of caprolactam
PCT/EP1994/003781 WO1995014664A1 (en) 1993-11-20 1994-11-15 Process for manufacturing caprolactam
DE59410076T DE59410076D1 (en) 1993-11-20 1994-11-15 METHOD FOR PRODUCING CAPROLACTAM

Publications (1)

Publication Number Publication Date
DE59410076D1 true DE59410076D1 (en) 2002-04-11

Family

ID=6503070

Family Applications (3)

Application Number Title Priority Date Filing Date
DE4339648A Withdrawn DE4339648A1 (en) 1993-11-20 1993-11-20 Process for the production of caprolactam
DE59410076T Expired - Lifetime DE59410076D1 (en) 1993-11-20 1994-11-15 METHOD FOR PRODUCING CAPROLACTAM
DE59408049T Expired - Fee Related DE59408049D1 (en) 1993-11-20 1994-11-15 METHOD FOR PRODUCING CAPROLACTAM

Family Applications Before (1)

Application Number Title Priority Date Filing Date
DE4339648A Withdrawn DE4339648A1 (en) 1993-11-20 1993-11-20 Process for the production of caprolactam

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE59408049T Expired - Fee Related DE59408049D1 (en) 1993-11-20 1994-11-15 METHOD FOR PRODUCING CAPROLACTAM

Country Status (25)

Country Link
US (2) US5646277A (en)
EP (2) EP0729453B1 (en)
JP (2) JP4249257B2 (en)
KR (2) KR100310508B1 (en)
CN (2) CN1070476C (en)
AT (2) ATE178318T1 (en)
AU (2) AU678643B2 (en)
BR (2) BR9408100A (en)
CA (2) CA2176741C (en)
CZ (2) CZ284795B6 (en)
DE (3) DE4339648A1 (en)
DK (1) DK0729453T3 (en)
ES (2) ES2173162T3 (en)
FI (1) FI112651B (en)
HU (1) HU218503B (en)
MY (2) MY111427A (en)
NO (1) NO304594B1 (en)
NZ (1) NZ276096A (en)
PL (2) PL314527A1 (en)
PT (1) PT729453E (en)
RU (2) RU2120437C1 (en)
SG (2) SG47102A1 (en)
TW (1) TW382624B (en)
UA (2) UA41965C2 (en)
WO (2) WO1995014664A1 (en)

Families Citing this family (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4443125A1 (en) * 1994-12-03 1996-06-05 Basf Ag Process for the production of caprolactam
DE19500041A1 (en) * 1995-01-03 1996-07-04 Basf Ag Process for the continuous purification of crude caprolactam made from 6-aminocapronitrile
FR2729949A1 (en) * 1995-01-27 1996-08-02 Rhone Poulenc Chimie LACTAM PREPARATION PROCESS
DE19517821A1 (en) * 1995-05-18 1996-11-21 Basf Ag Process for the production of caprolactam
DE19517823A1 (en) * 1995-05-18 1996-11-21 Basf Ag Process for the production of caprolactam
DE19518474A1 (en) * 1995-05-19 1996-11-21 Basf Ag Process for the preparation of carboxylic acid derivatives
FR2735471B1 (en) * 1995-06-16 1997-08-22 Rhone Poulenc Chimie LACTAM PREPARATION PROCESS
DE19623662A1 (en) * 1996-06-13 1997-12-18 Basf Ag Process for the purification of epsilon-caprolactam
DE19632006A1 (en) * 1996-08-08 1998-02-12 Bayer Ag Process for the preparation of lactams
US5877314A (en) * 1997-02-14 1999-03-02 Dsm N.V. Process to continuously prepare an aqueous mixture of episilon caprolactum and episilon caprolactum precursors
DE19718706A1 (en) * 1997-05-02 1998-11-05 Basf Ag Process for the preparation of cyclic lactams
BR9811613A (en) 1997-09-03 2000-08-08 Basf Ag Molded materials
DE19738464A1 (en) * 1997-09-03 1999-03-04 Basf Ag Use of moldings as a catalyst for the production of caprolactam
DE19738463C2 (en) 1997-09-03 1999-09-23 Basf Ag Process for the production of caprolactam
DE19804033A1 (en) 1998-02-02 1999-08-05 Basf Ag Continuous process for the production of polyamides from aminonitriles
DE19804023A1 (en) 1998-02-02 1999-08-05 Basf Ag Continuous process for the production of polyamides from aminonitriles
DE19804014A1 (en) 1998-02-02 1999-08-05 Basf Ag Batch process for the production of polyamides from aminonitriles
DE19808190A1 (en) * 1998-02-26 1999-09-02 Basf Ag Process for the production of polyamides
DE19808490A1 (en) 1998-02-27 1999-09-02 Basf Ag Process for the preparation of polyamides from aminocarboxylic acid compounds
DE19808489A1 (en) 1998-02-27 1999-09-02 Basf Ag Process for the preparation of polymer mixtures from aminonitriles and thermoplastic polymers
DE19811880A1 (en) 1998-03-18 1999-09-23 Basf Ag Preparation of lactam by gas phase cyclizing hydrolysis of aminonitrile, useful e.g. as solvent and in polyamide production
US6346641B1 (en) 1998-07-20 2002-02-12 Basf Aktiengesellschaft Method for simultaneous production of 6-aminocapronitrile and hexamethylenediamine
FR2781393B1 (en) 1998-07-22 2000-08-25 Rhone Poulenc Fibres PROCESS FOR REGENERATION OF A CYCLISTING HYDROLYSIS CATALYST OF A LACTAM AMINONITRILE AND USE OF THE REGENERATED CATALYST FOR THE MANUFACTURE OF LACTAMS
FR2781796B1 (en) * 1998-07-28 2000-09-22 Rhone Poulenc Fibres LACTAM DEHYDRATION PROCESS
DE19839338A1 (en) 1998-08-28 2000-03-02 Basf Ag Improved process for the simultaneous production of 6-aminocapronitrile and hexamethylenediamine
DE19846014A1 (en) 1998-10-06 2000-04-13 Basf Ag Accelerator for the production of polyamides from aminonitriles
DE10021201A1 (en) 2000-05-03 2001-11-08 Basf Ag Process for the preparation of cyclic lactams
DE10021191A1 (en) * 2000-05-03 2001-11-08 Basf Ag Process for producing a polymer using caprolactam
MY127068A (en) * 2000-06-05 2006-11-30 Basf Ag Removal of ammonia from solutions including caprolactam and ammonia
DE10033518A1 (en) * 2000-07-11 2002-01-24 Basf Ag Process for the separation of ammonia from 2-phase reaction mixture obtained in amide preparation, involves separating phases and extracting organic phase with aqueous medium
US6437089B1 (en) 2001-06-01 2002-08-20 E. I. Du Pont De Nemours And Company Process for the production of nylon 6
DE102004027022A1 (en) * 2004-06-02 2006-01-05 Basf Ag Process for the separation of ammonia and water from lactam-containing mixtures
FR2944791B1 (en) * 2009-04-27 2012-02-10 Rhodia Operations PROCESS FOR THE PREPARATION OF LACTAMES

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2301964A (en) * 1941-09-12 1942-11-17 Du Pont Method of preparing lactams
JPS4821958B1 (en) * 1969-01-28 1973-07-02
EP0150295A3 (en) * 1983-12-19 1988-03-30 Allied Corporation Selective production of n-substituted amides by use of cu(o)/metallic oxides catalyst compositions
US4628085A (en) * 1985-09-03 1986-12-09 Allied Corporation Use of silica catalyst for selective production of lactams
US4625023A (en) * 1985-09-03 1986-11-25 Allied Corporation Selective conversion of aliphatic and aromatic aminonitriles and/or dinitriles into lactams

Also Published As

Publication number Publication date
CZ284794B6 (en) 1999-03-17
SG55170A1 (en) 1998-12-21
DE59408049D1 (en) 1999-05-06
WO1995014665A1 (en) 1995-06-01
NO962021D0 (en) 1996-05-15
CA2176836C (en) 2004-02-10
CZ144596A3 (en) 1996-08-14
EP0729454A1 (en) 1996-09-04
HUT74976A (en) 1997-03-28
TW382624B (en) 2000-02-21
NO304594B1 (en) 1999-01-18
HU218503B (en) 2000-09-28
KR100310508B1 (en) 2002-02-19
US5739324A (en) 1998-04-14
FI962069A (en) 1996-05-15
AU8143594A (en) 1995-06-13
RU2119912C1 (en) 1998-10-10
NO962021L (en) 1996-05-15
ES2173162T3 (en) 2002-10-16
CN1070476C (en) 2001-09-05
DE4339648A1 (en) 1995-05-24
JPH09505571A (en) 1997-06-03
CN1061976C (en) 2001-02-14
PL314527A1 (en) 1996-09-16
AU678643B2 (en) 1997-06-05
SG47102A1 (en) 1998-03-20
EP0729454B1 (en) 1999-03-31
FI112651B (en) 2003-12-31
JPH09505570A (en) 1997-06-03
HU9601337D0 (en) 1996-07-29
CN1139920A (en) 1997-01-08
UA41964C2 (en) 2001-10-15
PT729453E (en) 2002-07-31
EP0729453B1 (en) 2002-03-06
EP0729453A1 (en) 1996-09-04
KR100310509B1 (en) 2002-02-19
RU2120437C1 (en) 1998-10-20
MY111427A (en) 2000-04-29
JP3824321B2 (en) 2006-09-20
ES2129791T3 (en) 1999-06-16
ATE178318T1 (en) 1999-04-15
US5646277A (en) 1997-07-08
MY111913A (en) 2001-02-28
CA2176741C (en) 2004-02-03
CA2176836A1 (en) 1995-06-01
ATE214047T1 (en) 2002-03-15
CN1141626A (en) 1997-01-29
PL314526A1 (en) 1996-09-16
KR960705776A (en) 1996-11-08
PL179509B1 (en) 2000-09-29
CA2176741A1 (en) 1995-06-01
BR9408099A (en) 1997-08-05
NZ276096A (en) 1997-05-26
WO1995014664A1 (en) 1995-06-01
AU1065095A (en) 1995-06-13
UA41965C2 (en) 2001-10-15
JP4249257B2 (en) 2009-04-02
KR960705775A (en) 1996-11-08
DK0729453T3 (en) 2002-05-21
CZ284795B6 (en) 1999-03-17
FI962069A0 (en) 1996-05-15
BR9408100A (en) 1997-08-05
CZ144696A3 (en) 1996-08-14

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: BASF SE, 67063 LUDWIGSHAFEN, DE