DE592118C - Plant for the centralized liquefaction of solid carbonic acid - Google Patents

Plant for the centralized liquefaction of solid carbonic acid

Info

Publication number
DE592118C
DE592118C DES89840D DES0089840D DE592118C DE 592118 C DE592118 C DE 592118C DE S89840 D DES89840 D DE S89840D DE S0089840 D DES0089840 D DE S0089840D DE 592118 C DE592118 C DE 592118C
Authority
DE
Germany
Prior art keywords
pressure
liquefaction
filling
container
carbonic acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DES89840D
Other languages
German (de)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Publication date
Priority to DES89840D priority Critical patent/DE592118C/en
Application granted granted Critical
Publication of DE592118C publication Critical patent/DE592118C/en
Expired legal-status Critical Current

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C9/00—Methods or apparatus for discharging liquefied or solidified gases from vessels not under pressure
    • F17C9/02—Methods or apparatus for discharging liquefied or solidified gases from vessels not under pressure with change of state, e.g. vaporisation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/50—Carbon dioxide
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2201/00—Vessel construction, in particular geometry, arrangement or size
    • F17C2201/01—Shape
    • F17C2201/0104—Shape cylindrical
    • F17C2201/0109—Shape cylindrical with exteriorly curved end-piece
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2201/00—Vessel construction, in particular geometry, arrangement or size
    • F17C2201/06—Vessel construction using filling material in contact with the handled fluid
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2203/00—Vessel construction, in particular walls or details thereof
    • F17C2203/06—Materials for walls or layers thereof; Properties or structures of walls or their materials
    • F17C2203/0602—Wall structures; Special features thereof
    • F17C2203/0612—Wall structures
    • F17C2203/0626—Multiple walls
    • F17C2203/0629—Two walls
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2205/00—Vessel construction, in particular mounting arrangements, attachments or identifications means
    • F17C2205/01—Mounting arrangements
    • F17C2205/0123—Mounting arrangements characterised by number of vessels
    • F17C2205/013—Two or more vessels
    • F17C2205/0134—Two or more vessels characterised by the presence of fluid connection between vessels
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2205/00—Vessel construction, in particular mounting arrangements, attachments or identifications means
    • F17C2205/01—Mounting arrangements
    • F17C2205/0153—Details of mounting arrangements
    • F17C2205/018—Supporting feet
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2205/00—Vessel construction, in particular mounting arrangements, attachments or identifications means
    • F17C2205/03—Fluid connections, filters, valves, closure means or other attachments
    • F17C2205/0302—Fittings, valves, filters, or components in connection with the gas storage device
    • F17C2205/0323—Valves
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2221/00—Handled fluid, in particular type of fluid
    • F17C2221/01—Pure fluids
    • F17C2221/013—Carbone dioxide
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/01—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the phase
    • F17C2223/0146—Two-phase
    • F17C2223/0153—Liquefied gas, e.g. LPG, GPL
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/01—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the phase
    • F17C2223/0146—Two-phase
    • F17C2223/0153—Liquefied gas, e.g. LPG, GPL
    • F17C2223/0161—Liquefied gas, e.g. LPG, GPL cryogenic, e.g. LNG, GNL, PLNG
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/03—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the pressure level
    • F17C2223/035—High pressure (>10 bar)
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/03—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the pressure level
    • F17C2223/036—Very high pressure (>80 bar)
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2227/00—Transfer of fluids, i.e. method or means for transferring the fluid; Heat exchange with the fluid
    • F17C2227/04—Methods for emptying or filling
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2250/00—Accessories; Control means; Indicating, measuring or monitoring of parameters
    • F17C2250/01—Intermediate tanks

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)

Description

Anlage zur zentralisierten Verflüssigung fester Kohlensäure Vorliegende Erfindung betrifft eine Anlage zur Überführung von Kohlensäure in Hochdruckbehälter, z. B. in die üblichen Stahlflaschen.Plant for the centralized liquefaction of solid carbon dioxide The invention relates to a system for transferring carbon dioxide into high-pressure containers, z. B. in the usual steel bottles.

Die Anlage arbeitet in der Weise, daß die Kohlensäure in festem Zustand zunächst nach Einfüllung meinen Niederdruckbehälter durch Zuführung von Wärme 'auf etwa den Druck des Tripelpunktes gebracht und dadurch verflüssigt wird, worauf die erhaltene flüssige Kohlensäure ,aus dem Verflüssigungsbehälter in Hochdruckbehälter abgefüllt wird.The system works in such a way that the carbonic acid is in a solid state first after filling my low-pressure tank by adding heat ' brought about the pressure of the triple point and thereby liquefied, whereupon the obtained liquid carbonic acid, from the liquefaction tank into high pressure tank is bottled.

Die Erfindung besteht darin, daß mit dem zentralen Verflüssigungsbehälter, der gleichzeitig auch als Speicher- oder Lagerungsbehälter für die Kohlensäure dienen kann, ein zweiter Behälter oder Kessel zum Abfüllen auf die üblichen Hochdruckbehälter vereinigt ist, der mit dem ersten zur Aufrechterhaltung höherer Drucke ;absperrbar verbunden ist. Aus dem zweiten Behälter, dem Abfüllbehälter, werden dann die bekannten Hochdruckbehälter, wie ;Kohlensäureflaschen o. dgl., mit der flüssigen Kohlensäure gefüllt.The invention consists in that with the central liquefaction tank, which also serve as a storage or storage container for the carbon dioxide can, a second container or boiler for filling on the usual high pressure container is united, the one with the first to maintain higher pressures; lockable connected is. The second container, the filling container, then becomes the familiar High-pressure containers, such as carbon dioxide bottles or the like, with the liquid carbon dioxide filled.

Den höheren Druck im zweiten Behälter erhält man am einfachsten in der Weise, daß eine Kohlensäureflasche bei gewöhnlicher Temperatur, also unter hohem Druck stehend, an den Abfüllbehälter angeschlossen wird, so daß man ihn durch öffnung eines Ventils jederzeit unter hohen Druck setzen kann. Wenn man die zu füllenden Flaschen unter der Temperatur der Umgebung herunterkühlt, dann kann auch der Druck zur Füllung der Flaschen niedriger gehalten werden.The easiest way to get the higher pressure in the second container is in the way that a carbonic acid bottle at normal temperature, that is, at a high temperature Pressure standing, is connected to the filling container, so that you can open it through a valve can put under high pressure at any time. When you have to fill the Bottles cools down below the ambient temperature, then the pressure can also kept lower to fill the bottles.

In dem Abfüllbehälter kann auch der Druck in anderer Weise gesteigert werden, beispielsweise durch Zuführung von Wärme.The pressure in the filling container can also be increased in other ways , for example by adding heat.

Auf der Zeichnung ist Haie Ausführungsform der Erfindung schematisch dargestellt. i bedeutet den zentralen Verflüssigungsbehälter, der durch einen Decke12 gasdicht geschlossen werden kann. Mit 3 ist ein Sicherheitsventil bezeichnet und mit q. ein Manometer, das den Druck anzeigt. Mit 5 ein Mantelraum, durch den die für die Verflüssigung notwendige Wärme beispielsweise durch erwärmte Luft zugeführt wird. Dias Zuführungsrohr ist mit 6 bezeichnet und mit 7 das Abführungsrohr. 8 bezeichnet einen zweiten kleineren von dem :ersten Behälter i getrennten Behälter. Das Verbindungsrohr zwischen dem zweiten Behälter und dem Niederdruckbehälter ist mit 9 bezeichnet, das überströmventil mit i o. Der zweite Behälter weist ebenfalls einen Mantelraum i i auf, der für die Erwärmung des Inhaltes dienen kann. Das Zuführungsrohr ist mit 12 bezeichnet, das Abführungsrohr mit 12a und mit 13 die zu füllenden Flaschen, die durch das Rohr 1 ¢ aus dem Behälter 8 gefüllt werden. In dem Behälter 8 soll ein höherer Druck als in dem Verflüssigungsbehälter i herrschen. ' Dieser höhere Druck kann durch die Zuführung von Wärme, wie bereits erwähnt, erzeugt werden oder durch den Druck :einer fremden Druckquelle, beispielsweise einer Kohlensäureflasche 15. Durch das Rohr 16 wird in diesem Falle der Behälter 8 unter Überdruck gesetzt. 17 bezeichnet eine bekannte Wägevorrichtung, auf der die zu füllenden. Flaschen abgewogen werden. 18 bezeichnet :ein Sicherheitsventil am zweiten Behälter.Haie embodiment of the invention is schematically shown in the drawing shown. i means the central condensing tank, which is covered by a ceiling12 can be closed gas-tight. With 3 a safety valve is referred to and with q. a manometer that shows the pressure. With 5 a shell space through which the Heat required for liquefaction, for example, supplied by heated air will. The feed pipe is denoted by 6 and 7 the discharge pipe. 8 designated a second smaller container separate from the first container i. The connecting pipe between the second container and the low-pressure container is denoted by 9, the overflow valve with i o. The second container also has a shell space i i, which can be used to heat the content. The feed tube is denoted by 12, the discharge pipe with 12a and with 13 the bottles to be filled, which are filled through the tube 1 [from the container 8]. In the container 8 should a higher pressure than prevail in the liquefaction tank i. 'This higher one Pressure can be generated or, as already mentioned, by the supply of heat by pressure: an external pressure source, for example a carbon dioxide bottle 15. In this case, the container 8 is pressurized through the tube 16. 17 denotes a known weighing device on which the to be filled. Bottles be weighed. 18 denotes: a safety valve on the second container.

Claims (2)

PATENTANSPRÜCHE: i. Anlage zur zentralisierten Verflüssigung fester Kohlensäure und Füllung der handelsüblichen Hochdruckbehälter, gekennzeichnet durch die Vereinigung eines ,an sich bekannten, gasdicht verschließbaren, drucksicheren und mit bekannter Erwärmungsvorrichtung [ausgerüsteten Verflüssigungskes;sels, in welchem die feste Kohlensäure etwa unter dem Druck des Tripelpunktes geschmolzen wird, mit einem zweiten Abfüllkessel zum Abfüllen auf die üblichen Hochdruckbehälter, der mit dem fersten zur Aufrechterhaltung höherer Drucke absperrbar verbunden ist. PATENT CLAIMS: i. Plant for centralized liquefaction of solids Carbon dioxide and filling of standard high-pressure containers, characterized by the union of a gas-tight lockable, pressure-proof one known per se and with a known heating device [equipped liquefaction boiler; sels, in which the solid carbonic acid melted under the pressure of the triple point is, with a second filling vessel for filling on the usual high pressure containers, which is lockably connected to the fersten to maintain higher pressures. 2. Ausführungsform der Anlage nach Anspruch i, dadurch gekennzeichnet, daß der zweite Kessel mit einer Leitung ausgerüstet ist, durch die :er von einer fremden Druckquelle her, z. B. einer Kohl:ens.äureflascht, die nach Bedarf besonders erwärmt -wird, unter Druck gesetzt werden kann.2. Embodiment of the system according to claim i, characterized in that the second The boiler is equipped with a line through which: it is supplied from an external pressure source heart. B. a cabbage: ens. Acid bottle, which is specially heated as required can be pressurized.
DES89840D Plant for the centralized liquefaction of solid carbonic acid Expired DE592118C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DES89840D DE592118C (en) Plant for the centralized liquefaction of solid carbonic acid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DES89840D DE592118C (en) Plant for the centralized liquefaction of solid carbonic acid

Publications (1)

Publication Number Publication Date
DE592118C true DE592118C (en) 1934-02-01

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DES89840D Expired DE592118C (en) Plant for the centralized liquefaction of solid carbonic acid

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