DE56574C - Apparatus equipped with steam jet devices for the decomposition of fats into fatty acids and glycerine - Google Patents
Apparatus equipped with steam jet devices for the decomposition of fats into fatty acids and glycerineInfo
- Publication number
- DE56574C DE56574C DENDAT56574D DE56574DA DE56574C DE 56574 C DE56574 C DE 56574C DE NDAT56574 D DENDAT56574 D DE NDAT56574D DE 56574D A DE56574D A DE 56574DA DE 56574 C DE56574 C DE 56574C
- Authority
- DE
- Germany
- Prior art keywords
- steam
- glycerine
- fats
- fatty acids
- decomposition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 title claims description 10
- 239000003925 fat Substances 0.000 title claims description 7
- 235000011187 glycerol Nutrition 0.000 title claims description 5
- 235000014113 dietary fatty acids Nutrition 0.000 title claims description 4
- 229930195729 fatty acid Natural products 0.000 title claims description 4
- 239000000194 fatty acid Substances 0.000 title claims description 4
- 150000004665 fatty acids Chemical class 0.000 title claims description 4
- 238000000354 decomposition reaction Methods 0.000 title claims description 3
- 238000001816 cooling Methods 0.000 claims description 5
- 229940090046 jet injector Drugs 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 239000000110 cooling liquid Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 239000011872 intimate mixture Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 210000003127 knee Anatomy 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
- C11C1/02—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils
- C11C1/04—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils by hydrolysis
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Description
KAISERLICHESIMPERIAL
PATENTAMT.PATENT OFFICE.
Bei allen bisher construirten und verwendeten Autoclaven zur Zersetzung von Fetten in Fettsäuren und Glycerin brauchte man stets eine verhältnifsmäfsig lange Zeit, um aus den zu verseifenden Stoffen und dem heifsen Wasser und Dampf ein inniges Gemisch herzustellen, und es wurde daher auch die Aufgabe, die Spaltung der Fette in Glycerin und Fettsäuren in möglichst kurzer Zeit zu bewirken, nur unvollkommen gelöst.In all autoclaves that have been constructed and used to date for the decomposition of fats in fatty acids and glycerine it always took a relatively long time to get out of the substances to be saponified and the hot water and steam to produce an intimate mixture, and it was therefore also the task of to break down the fats into glycerine and fatty acids in the shortest possible time, only incompletely resolved.
Mit dem nachstehend beschriebenen Apparat dagegen wird dies infolge einer ununterbrochenen circulirenden Bewegung und durch Zerstäubung der Masse erreicht. Während man bis jetzt zur Verseifung einer Beschickung 6 bis 7 Stunden braucht, sind bei dem neuen Apparat nur ι Y2 bis 2 Stunden erforderlich.With the apparatus described below, on the other hand, this is achieved by means of an uninterrupted circulating movement and by atomizing the mass. While up to now it took 6 to 7 hours to saponify a charge, only 2 to 2 hours are required with the new apparatus.
Der Apparat besteht aus zwei Haupttheilen, dem Cylinder A und dem Kühler B. Der verticale Cylinder A (aus Kupfer oder Eisen) ist oben und unten durch sphärische Kuppeln geschlossen. Die obere Kuppel k ist mit einem Mannloch rti mit Deckel η versehen, an welchem sich befinden: das Füllventil/,1 das Sicherheitsventil s, der Lufthahn h, das Manometer i, sowie das Knie c, an welches sich das Circulationsrohr mit Zerstäuber anschliefst.The apparatus consists of two main parts, the cylinder A and the cooler B. The vertical cylinder A (made of copper or iron) is closed above and below by spherical domes. The upper dome k is provided with a manhole rti with cover η , on which there are: the filling valve /, 1 the safety valve s, the air cock h, the manometer i, and the knee c, to which the circulation pipe with atomizer is attached.
Die untere Kuppel trägt einen Stutzen mit drei Abzweigungen:The lower dome has a socket with three branches:
1. einer Abzweigung für das Dampfventil ν mit Rückschlagventil r für den vom Hochdruckkessel kommenden Dampf,1. a branch for the steam valve ν with check valve r for the steam coming from the high pressure boiler,
2. einer Abzweigung mit Entleerungsventil e, welche zum Ablassen des Autoclaven dient,2. a branch with drain valve e, which is used to drain the autoclave,
3. einer Abzweigung für den Circulationselevator F, welcher mit Dampf betrieben wird,3. a branch for the circulation elevator F, which is operated with steam,
Der Stutzen Si, an dem sich diese Abzweigungen befinden, besitzt zwei getrennte Bohrungen, eine für den Dampf und eine für die Masse. Auf die Dampfbohrung d ist im Innern ein Dampfstrahl-Injector aufgesetzt, welcher die Masse im Apparat unten durch die Löcher ^ einsaugt und aus der Rohrmündungj-' mit Heftigkeit ausbläst. Die Bohrung α führt zum Circulations - Dampfelevator F und zum Entleerungsventil e.The nozzle Si, on which these branches are located, has two separate bores, one for the steam and one for the mass. A steam jet injector is placed on the inside of the steam hole d , which sucks the mass in the apparatus through the holes below and blows it out of the pipe mouth with force. The hole α leads to the circulation steam elevator F and to the drain valve e.
Der Kühler B ist mit Deckel, Dunstrohr u und Kühlschlange g versehen. Durch den Stutzen b tritt die Kühlflüssigkeit ein; dieselbe ist Wasser oder Glycerin wasser, welches beim Kühlen gleichzeitig concentrirt wird.The cooler B is provided with a cover, vent pipe u and cooling coil g . The cooling liquid enters through the nozzle b; it is water or glycerine water, which is concentrated at the same time as it is cooled.
Der untere Theil der Kühlschlange steht mit dem Circulationselevator F, der obere mit dem Zerstäuber ρ durch Rohre in Verbindung.The lower part of the cooling coil is connected to the circulation elevator F, the upper part to the atomizer ρ by pipes.
Die Wirkungsweise des Apparates ist folgende: Das in den Autoclaven gebrachte Fett wird durch Dampf aus einem Hochdruckkessel erhitzt, in Circulation versetzt und auf zweifache Weise zerstäubt: erstens wird die Materie durch den Dampf des Dampfstrahl-Injectors y bei ^ angesaugt und beij' ausgeschleudert und ununterbrochen erhitzt und bewegt; zweitens wird die Masse durch den Circulationselevator F bei α angesaugt und durch die Kühlschlange emporgedrückt. Durch die Kühlschlange wird die Spannung der Masse vermindert. Sodann wirkt der mit Dampf betriebene Zerstäuber inThe mode of operation of the apparatus is as follows: The fat brought into the autoclave is heated by steam from a high-pressure boiler, put into circulation and atomized in two ways: firstly, the matter is sucked in by the steam of the steam jet injector y at ^ and thrown out and continuously heated and agitated; Secondly, the mass is sucked in by the circulation elevator F at α and pushed up by the cooling coil. The tension in the mass is reduced by the cooling coil. The steam-operated atomizer then acts in
gleichem Sinne auf die Fettmasse und schleudert sie in den Autoclaven zurück.same sense on the fat mass and throws it back into the autoclave.
Claims (1)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE56574C true DE56574C (en) |
Family
ID=331005
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT56574D Expired - Lifetime DE56574C (en) | Apparatus equipped with steam jet devices for the decomposition of fats into fatty acids and glycerine |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE56574C (en) |
-
0
- DE DENDAT56574D patent/DE56574C/en not_active Expired - Lifetime
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