DE398879C - Process for making neutral, solid colloids and consistent lubricants - Google Patents
Process for making neutral, solid colloids and consistent lubricantsInfo
- Publication number
- DE398879C DE398879C DEC32665D DEC0032665D DE398879C DE 398879 C DE398879 C DE 398879C DE C32665 D DEC32665 D DE C32665D DE C0032665 D DEC0032665 D DE C0032665D DE 398879 C DE398879 C DE 398879C
- Authority
- DE
- Germany
- Prior art keywords
- solid
- solution
- magnesium
- colloids
- wool fat
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
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- C10M7/00—Solid or semi-solid compositions essentially based on lubricating components other than mineral lubricating oils or fatty oils and their use as lubricants; Use as lubricants of single solid or semi-solid substances
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Description
Verfahren zur Herstellung neutraler, fester Kolloide und konsistenter Schmiermittel. In dem Hauptpatent ist ein Verfahren zur Herstellung neutraler, fester Wachs- und Harzkolloide beschrieben, nach dem Wachs oder Harz unter Erwärmung mit oder ohne Druck mit wässerigen Lösungen von milchsauren Salzen, vornehmlich eingedickten Alkalilaktatlösungen, so lange verrührt werden, bis die homogene Vereinigung, beider @Bestandteile die Bildung des Suspensoids anzeigt.Method of making neutral, solid colloids and more consistent Lubricant. In the main patent is a process for producing more neutral, more solid Wax and resin colloids described after using the wax or resin with heating or without pressure with aqueous solutions of lactic acid salts, mainly thickened ones Alkali lactate solutions are stirred until the two are homogeneously combined @Components indicates the formation of the suspensoid.
Es hat sich nun-gezeigt, daß die Verwendbarkeit wässeriger Lösungen in der durch das Hauptpatent gekennzeichneten Weise nicht auf Laktatlösungen beschränkt ist, sondern daß auch andere wässerige Lösungen, die nicht eintrockenbar sind, als Bestandteile der Kolloide Anwendung finden können. Als solche kommen beispielsweise Lösungen von Magnesiumazetat, Magnesiumchlorid,. Chlorkalzium in Betracht. Eine verseifende Wirkung kommt bei diesen Lösungen ebensowenig wie im Hauptpatent in Frage, wie überhaupt die saure oder alkalische Reaktion der Lösung keine Rolle spielt.It has now been shown that the usability of aqueous solutions not limited to lactate solutions in the manner characterized by the main patent is, but that also other aqueous solutions that are not dryable than Components of the colloids can be used. As such come for example Solutions of magnesium acetate, magnesium chloride ,. Calcium chloride into consideration. One There is just as little saponifying effect in these solutions as in the main patent in Ask how the acidic or alkaline reaction of the solution plays no role at all.
Der Zusatz von Salzlösungen zu konsistenten Fetten ist schon wiederholt vorgeschlagen worden. So findet sich in 'einer Patentschrift ein Verfahren, um Fett durch Zusatz von Natronlauge und konzentrierten Kochsalzlösungen konsistent zu machen. Nach einer anderen wird zu einem Gemenge von, Wollfett und Antimonbutter Chlorzinklösung hinzugesetzt, um die Verschlechterung, welche die Leitfähigkeit der Antimonbutter bei höheren Temperaturen erleidet, wiederaufzuheben, also ein Gemenge zu gewinnen, das bei jeder Temperatur die Elektrizität gut leitet. In einer österreichischen Patentschrift werden hochkonzentrierte viskose Emulsionsmassen beschrieben, welche aus verschiedenen harzigen und öligen Substanzen mit Sulfitzellstoffablauge hergestellt sind. Diese Gemische können für verschiedene Zwecke mit Zusätzen wie Sägespänen, Gerbstoffen, Metallsalzen und -oxyden versehen werden. In allen diesen Fällen handelt es sich also um Massen, welche für ganz bestimmte, von dem hier vorliegenden völlig abweichende Zwecke zusammengesetzt werden, deren Eigenschaften von denen der festen Kolloide verschieden sind und die ihrer Zusammensetzung nach auch nicht geeignet wären, denselben Zwecken, wie die in dieser Anmeldung beschriebenen festen Kolloide zu dienen.The addition of salt solutions to consistent fats has already been repeated has been proposed. For example, there is a patent specification for a method to remove fat by adding caustic soda and concentrated saline solutions to make them consistent. After another, a mixture of, wool fat and antimony butter becomes a zinc chloride solution added to the deterioration affecting the conductivity of the antimony butter at higher temperatures suffers to pick up again, i.e. to win a mixture, that conducts electricity well at any temperature. In an Austrian Patent highly concentrated viscous emulsion compositions are described, which made from various resinous and oily substances with sulphite pulp waste liquor are. These mixtures can be used for various purposes with additives such as sawdust, Tanning agents, metal salts and oxides. Acts in all of these cases it is therefore a matter of masses, which are quite specific, of what is present here completely divergent purposes are composed, whose properties are from those of the fixed Colloids are different and their composition is not suitable either would be for the same purposes as the solid colloids described in this application to serve.
Gegenüber den vorgenannten Verfahren bezweckt die vorliegende Erfindung, konsistente Fette herzustellen, die neben harzigen und öligen Massen zu einem beträchtlichen Teil Wasser in Form einer Salzlösung enthalten. Es hat sich gezeigt, daß die so hergestellten Kolloidfette vorzügliche Schmiermittel sind, welche in bezug auf ihre Fähigkeit, die Reibung aneinandergleitender Metallflächen ebenso wie die hierbei auftretende 'Wärmeentwicklung ztt verringern, den nur aus Fetten und Harzen bestehenden Schmiermitteln vollkommen gleichstehen oder diese sogar übertreffen.Compared to the aforementioned method, the present invention aims to produce consistent fats, which in addition to resinous and oily masses to a considerable extent Part of water contained in the form of a saline solution. It has been shown that so produced colloidal fats are excellent lubricants, which in relation to their Ability to reduce the friction between sliding metal surfaces as well How to reduce the heat development that occurs here, that only from fats and resins are equal to or even better than existing lubricants.
Beispiele: i. io Teile Rolunontanwachs werden geschmolzen und unter Rühren mit 5o Teilen erwärmter Chlormagnesiumlösung von etwa 25 bis 3o Prozent Chlormagnesium in dünnem Strahl versetzt, bis sich die zunächst getrennt bleibenden Bestandteile homogen vereinigt haben, was äußerlich deutlich erkennbar ist. lach dein Erkalten liegt das Kolloid als fester einheitlicher Körper vor.Examples: i. io parts of Rolunontan wax are melted and under Stir with 50 parts of warmed magnesium chlorine solution of about 25 to 30 percent magnesium chlorine in a thin stream until the components that initially remain separate have united homogeneously, which is clearly recognizable from the outside. laugh your cold the colloid is present as a solid, uniform body.
Der Chlormagnesiumlösung wird vorher zweckmäßig Magnesiumoxyd oder Magnesiumhydroxyd in Menge von etwa 1:, Prozent des Gewichtes der Chlormagnesiumlösung zugeführt. Das Hydroxyd bzw.Oxyd kann dabei in der Lösung selbst erzeugt werden.The chlorine magnesium solution is expediently magnesium oxide or beforehand Magnesium hydroxide in an amount of about 1:, percent of the weight of the chlorine magnesium solution fed. The hydroxide or oxide can be generated in the solution itself.
2. An Stelle der Chlorinagnesiumlösung kann genau ebenso und mit demselben Erfolge eine etwa 25prozentige Magnesiumazetatlösung verwendet werden. Auch hier ist die Zugabe des Magnesiumoxydes oder -hydroxydes zweckmäßig.2. Instead of the chlorine-magnesium solution, exactly the same and with the same can be used Successfully use an approximately 25 percent magnesium acetate solution. Here too it is advisable to add the magnesium oxide or hydroxide.
Derartige Kolloide können weiterverarbeitet werden dadurch, daß man sie, mit Ü1 und Fett, z. B. Tran, Rüböl o. dgl., oder mit anderen organischen Lösungsmitteln zusammenbringt und darin löst, am besten unter Erwärmen und Rühren, wobei man dann noch evtl. andere organische Körper, wie Pech, Anthrazenrückstände, Gatsch, Paraffinmassen u. dgl., mit auflöst. Man erhält so konsistente Schmiermittel, Pasten und Salben.Such colloids can be further processed by they, with Ü1 and fat, z. B. Tran, rapeseed oil o. The like., Or with other organic solvents brings together and dissolves in it, preferably with heating and stirring, whereby one then possibly other organic bodies, such as pitch, anthracene residues, slack, paraffin masses and the like, with dissolves. In this way, consistent lubricants, pastes and ointments are obtained.
Matt kann auch an Stelle der Weiterverarbeitung des Kolloides, wie sie eben beschrieben ist, gleich von vornherein die Pasten usw. herstellen, indem inan die 1:i1-dung des Suspensoids in den Lösungsmitteln (öle und Fette u. dgl.) selbst vornimmt.Matt can also be used in place of further processing of the colloid, such as it has just been described, make the pastes etc. from the start by inanan the 1: i1-formation of the suspensoid in the solvents (oils and fats etc.) does it himself.
Es hat sich auch gezeigt, daß die Wachse, Harze, Peche, Kohlenwasserstofte usw. zum Teil oder ganz ersetzt werden können durch Wollfett oder zweckmäßiger durch die rohen Wollfettalkohole (das sind die Wollfettalkohole samt den unverseifbaren Anteilen des Wollfetts) und auch die gereinigten 'Vollfettalkolt o1 e.It has also been shown that the waxes, resins, pitches, hydrocarbons etc. can be partially or completely replaced by wool fat or, more appropriately, by the raw wool fat alcohols (these are the wool fat alcohols including the unsaponifiable ones Proportions of wool fat) and also the purified 'Vollfettalkolt o1 e.
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEC32665D DE398879C (en) | 1921-02-08 | 1922-10-03 | Process for making neutral, solid colloids and consistent lubricants |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEH84284D DE357378C (en) | 1921-02-08 | 1921-02-08 | Process for the production of neutral, solid wax and resin colloids |
DEC32665D DE398879C (en) | 1921-02-08 | 1922-10-03 | Process for making neutral, solid colloids and consistent lubricants |
Publications (1)
Publication Number | Publication Date |
---|---|
DE398879C true DE398879C (en) | 1924-07-15 |
Family
ID=25969851
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DEC32665D Expired DE398879C (en) | 1921-02-08 | 1922-10-03 | Process for making neutral, solid colloids and consistent lubricants |
Country Status (1)
Country | Link |
---|---|
DE (1) | DE398879C (en) |
-
1922
- 1922-10-03 DE DEC32665D patent/DE398879C/en not_active Expired
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