DE324140C - Method of preparing a detergent - Google Patents
Method of preparing a detergentInfo
- Publication number
- DE324140C DE324140C DE1917324140D DE324140DD DE324140C DE 324140 C DE324140 C DE 324140C DE 1917324140 D DE1917324140 D DE 1917324140D DE 324140D D DE324140D D DE 324140DD DE 324140 C DE324140 C DE 324140C
- Authority
- DE
- Germany
- Prior art keywords
- detergent
- preparing
- sulfuric acid
- blast furnace
- furnace slag
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003599 detergent Substances 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 6
- 239000002893 slag Substances 0.000 claims description 4
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 2
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 2
- 239000004571 lime Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- 150000007513 acids Chemical class 0.000 claims 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 4
- 239000000344 soap Substances 0.000 description 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000000292 calcium oxide Substances 0.000 description 2
- 235000012255 calcium oxide Nutrition 0.000 description 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Description
-Verfahren zur Darstellung eines Waschmittels. Die Erfindung betrifft die Herstellung eines Erzeugnisses, das infolge seiner schlüpfrigen Beschaffenheit in wäßriger Emulsion die Eigenschaft besitzt, Fette zu emulgieren, und deshalb als Waschmittel und Ersatz für Seife mit Erfolg angewendet werden kann.Method for the preparation of a detergent. The invention relates to the manufacture of a product which, due to its slippery nature in aqueous emulsion has the property of emulsifying fats, and therefore as Detergent and soap substitutes can be used with success.
Zu diesem Zweck wird Hochofenschlacke durch Behandeln mit verdünnter Schwefelsäure in der Siedehitze zerlegt und die erhaltene Masse mit gebranntem Kalk im Über-, versetzt. Es entsteht ein steifer Brei,, weicher hauptsächlich aus gefälltem Calciumsulfat, Aluminiumhydroxyd, Eisenoxyd, Manganoxyd und gallertartiger Kieselsäure besteht; außerdem sind vorhanden die etwa gleichzeitig ausgefällten Silikate der genannten Basen und überschüssiger Kalk.For this purpose, blast furnace slag is diluted by treating it with Sulfuric acid decomposed at the boiling point and the resulting mass with quick lime in over-, offset. The result is a stiff pulp, softer mainly from precipitated material Calcium sulfate, aluminum hydroxide, iron oxide, manganese oxide and gelatinous silica consists; in addition, the silicates of the precipitated at about the same time are present called bases and excess lime.
Die breiartige Masse wird auf einem Kollergang fein zerrieben, in Stücke geformt und an der Luft getrocknet.The pulpy mass is finely ground on a pan mill, in Pieces molded and air dried.
Ausführungsbcispie1: i 1 Schwefelsäure vom spezifischem Gewicht i,8 wird mit Wasser auf io 1 verdünnt und zum Sieden erhitzt; dann werden allmählich a kg feingepulverte Hochofenschlacke unter beständigem Umrühren hinzugefügt. Nach der vollständigen Zersetzung des Schlackenpulvers, welche in So Minuten erreicht ist, werden allmählich 6 kg gepulverter gebrannter Kalk unter fortwährendem Umrühren zugegeben und zu einem gleichmäßigen Brei verarbeitet. Dieser kann ohne vorhergehendes Trocknen wie Schmierseife verwendet werden; man kann ihn aber auch in Stücke formen und an der Luft trocknen, um ihn als Ersatz von Hartseifen zu verwenden, oder die getrockneten Stücke zwecks Verwendung als Waschpulver vermahlen.Execution example: i 1 sulfuric acid with a specific weight of i, 8 is diluted to 10 1 with water and heated to the boil; then will gradually a kg of finely powdered blast furnace slag added with constant stirring. To the complete decomposition of the slag powder, which reaches in so minutes is, gradually add 6 kg of powdered quick lime with constant stirring added and processed into a uniform paste. This can be done without preceding Drying can be used like soft soap; but you can also shape it into pieces and air dry to use as a substitute for hard soaps, or the Grind the dried pieces for use as washing powder.
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE324140T | 1917-03-25 |
Publications (1)
Publication Number | Publication Date |
---|---|
DE324140C true DE324140C (en) | 1920-08-23 |
Family
ID=6177668
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE1917324140D Expired DE324140C (en) | 1917-03-25 | 1917-03-25 | Method of preparing a detergent |
Country Status (1)
Country | Link |
---|---|
DE (1) | DE324140C (en) |
-
1917
- 1917-03-25 DE DE1917324140D patent/DE324140C/en not_active Expired
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