DE257826C - - Google Patents
Info
- Publication number
- DE257826C DE257826C DENDAT257826D DE257826DA DE257826C DE 257826 C DE257826 C DE 257826C DE NDAT257826 D DENDAT257826 D DE NDAT257826D DE 257826D A DE257826D A DE 257826DA DE 257826 C DE257826 C DE 257826C
- Authority
- DE
- Germany
- Prior art keywords
- alkali
- water
- chloride
- reaction
- under pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 239000003513 alkali Substances 0.000 claims description 4
- 150000001447 alkali salts Chemical class 0.000 claims description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 3
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 3
- 229910052910 alkali metal silicate Inorganic materials 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000004576 sand Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N Silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 235000012239 silicon dioxide Nutrition 0.000 claims 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N Sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 3
- 235000019353 potassium silicate Nutrition 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- AKEJUJNQAAGONA-UHFFFAOYSA-N Sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 229910052570 clay Inorganic materials 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/32—Alkali metal silicates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Silicon Compounds (AREA)
Description
KAISERLICHESIMPERIAL
PATENTAMT.PATENT OFFICE.
Zur Darstellung von Wasserglas hat man bisher Kieselsäure mit Soda bzw. Pottasche und Kohle zusammen geschmolzen.So far, silica with soda or potash has been used to represent water glass and coal melted together.
Es wurde nun gefunden, daß man in bedeutend einfacherer Weise Wasserglas erhält, wenn man Kieselsäure in fein verteilter Form, z. B. feinen Sand oder Lehm; mit entsprechenden Mengen eines Alkalisalzes, z. B. Alkalichlorid oder Alkalisulfat, zusammen im Autoklaven unter Druck auf höhere Temperaturen erhitzt. Zur Erzeugung des erforderlichen Druckes im Autoklaven kann man das Gemisch vorteilhaft mit geringen Mengen Wasser zu einem sirupförmigen Brei anrühren.It has now been found that water glass is obtained in a much simpler manner if silica is used in finely divided form, e.g. B. fine sand or clay ; with appropriate amounts of an alkali salt, e.g. B. alkali chloride or alkali sulfate, heated together in the autoclave under pressure to higher temperatures. To generate the required pressure in the autoclave, the mixture can advantageously be mixed with small amounts of water to form a syrupy paste.
Bei Temperaturen von 400 bis 600 ° bildet sich dann im Verlauf von 6 bis 8 Stunden das betreffende Alkalisilikat und bei Verwendung eines Chlorids Salzsäure- bzw. bei höherem Druck Chlorgas bzw. bei Verwendung eines Sulfats Schwefelsäureanhydrid, die nach Beendigung der Reaktion durch Ablassen aus einem oberen Ventil entfernt werden.At temperatures of 400 to 600 ° it then forms in the course of 6 to 8 hours the alkali silicate in question and, if a chloride is used, hydrochloric acid or higher Pressure chlorine gas or, if a sulphate is used, sulfuric anhydride, which after termination the reaction can be removed by draining from an upper valve.
Das im Autoklaven verbleibende Wasserglas kann beliebiger Verwendung zugeführt werden.The water glass remaining in the autoclave can be put to any use.
Claims (1)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE257826C true DE257826C (en) |
Family
ID=515704
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT257826D Active DE257826C (en) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE257826C (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7488373B2 (en) | 2002-03-05 | 2009-02-10 | Statoil Asa | Device and method for treating a gas/liquid mixture |
-
0
- DE DENDAT257826D patent/DE257826C/de active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7488373B2 (en) | 2002-03-05 | 2009-02-10 | Statoil Asa | Device and method for treating a gas/liquid mixture |
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